J. Mater. Sci. Technol. ›› 2021, Vol. 60: 44-55.DOI: 10.1016/j.jmst.2020.05.021
• Research Article • Previous Articles Next Articles
B.N. Dua, Z.Y. Hua,d, L.Y. Shenga,*(), D.K. Xub,*(), Y.X. Qiaoc, B.J. Wanga, J. Wanga, Y.F. Zhenga, T.F. Xia
Received:
2020-03-10
Revised:
2020-05-07
Accepted:
2020-05-13
Published:
2021-01-10
Online:
2021-01-22
Contact:
L.Y. Sheng,D.K. Xu
B.N. Du, Z.Y. Hu, L.Y. Sheng, D.K. Xu, Y.X. Qiao, B.J. Wang, J. Wang, Y.F. Zheng, T.F. Xi. Microstructural characteristics and mechanical properties of the hot extruded Mg-Zn-Y-Nd alloys[J]. J. Mater. Sci. Technol., 2021, 60: 44-55.
Alloys | Nominal composition | Test composition | ||
---|---|---|---|---|
Zn | Y | Nd | ||
A1 | Mg-4Zn-0.6Y-0.5Nd | 4.33 | 0.57 | 0.55 |
A2 | Mg-6Zn-0.6Y-0.5Nd | 6.60 | 0.61 | 0.61 |
A3 | Mg-4Zn-0.8Y-0.5Nd | 4.30 | 0.88 | 0.51 |
Table 1 Nominal and test composition of investigated alloys (wt.%).
Alloys | Nominal composition | Test composition | ||
---|---|---|---|---|
Zn | Y | Nd | ||
A1 | Mg-4Zn-0.6Y-0.5Nd | 4.33 | 0.57 | 0.55 |
A2 | Mg-6Zn-0.6Y-0.5Nd | 6.60 | 0.61 | 0.61 |
A3 | Mg-4Zn-0.8Y-0.5Nd | 4.30 | 0.88 | 0.51 |
Fig. 2. SEM image of the as-cast and extruded Mg-Zn-Y-Nd alloys: (a)-(c) as-cast alloy; (d)-(f) as extruded alloy; (a), (d) alloy A1; (b), (e) alloy A2; (c), (f) alloy A3.
Alloys | DRXed grains | Secondary phase | ||
---|---|---|---|---|
Volume fraction (%) | Average size (μm) | Volume fraction (%) | Average size (μm) | |
A1 | 90.44 | 15.34 | 2.15 | 2.26 |
A2 | 93.43 | 17.30 | 4.07 | 2.30 |
A3 | 68.27 | 6.65 | 2.38 | 2.23 |
Table 2 Volume fraction and average size of the DRXed grains and secondary phases of the extruded Mg-Zn-Y-Nd alloys.
Alloys | DRXed grains | Secondary phase | ||
---|---|---|---|---|
Volume fraction (%) | Average size (μm) | Volume fraction (%) | Average size (μm) | |
A1 | 90.44 | 15.34 | 2.15 | 2.26 |
A2 | 93.43 | 17.30 | 4.07 | 2.30 |
A3 | 68.27 | 6.65 | 2.38 | 2.23 |
Fig. 3. TEM analysis of the secondary phases in the hot extruded Mg-Zn-Y-Nd alloy: (a) Dark-field image of the linearly distributed secondary phase; (b) TEM-EDS result of the secondary phase in (a); (c) SADP of the secondary phase in (a); (d) Bright-field image of the fine precipitate; (e) TEM-EDS result of the secondary phase in (d); (f) SADP of the secondary phase in (d).
Fig. 4. EBSD results of alloy A1 and A3: (a) - (d) alloy A1; (e) - (h) alloy A3; (a), (e) Polar figure; (b) (f) Inverse polar figure; (c), (g) Grain boundary map; (d), (h) Twin map. (The black lines in the grain boundary maps represent high angle grain boundaries (HAGBs) and green lines represent LAGBs.).
Fig. 5. Tensile and compressive properties of the hot extruded Mg-Zn-Y-Nd alloys: (a) tensile yield strength (TYS), tensile ultimate strength (TUS) and elongation; (b) compressive yield strength (CYS) and compressive ultimate strength (CUS).
Fig. 6. SEM image of the fracture surfaces and longitudinal section of the fractured specimens after tensile tests at room temperature: (a)-(c) Fracture surfaces; (d)-(f) Longitudinal section of the fractured specimens; (a), (d) Alloy A1; (b), (e) Alloy A2; (c), (f) Alloy A3.
Fig. 7. SEM image of the longitudinal section of the fractured specimens after compressive tests at room temperature: (a) Alloy A1; (b) Alloy A2; (c) Alloy A3.
Fig. 8. EBSD of alloy A1 and A3 after tensile test at room temperature: (a)-(d) alloy A1; (e)-(h) alloy A3; (a) (e) Polar figure; (b), (f) Inverse polar figure; (c), (g) Grain boundary map; (d), (h) Twin map.
Fig. 9. EBSD of the alloy A1 and A3 after compressive test at room temperature: (a)-(d) alloy A1; (e)-(h) alloy A3; (a), (e) Polar figure; (b), (f) Inverse polar figure; (c), (g) Grain boundary map; (d), (h) Twin map.
Fig. 10. Partial region magnification of Fig. 4(b) and (c) showing the different DRXed grains: P represents parent elongated grain, and the numbers from 1 to 10 represent DRXed grains.
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