J. Mater. Sci. Technol. ›› 2021, Vol. 77: 38-46.DOI: 10.1016/j.jmst.2020.11.026
• Research Article • Previous Articles Next Articles
Y. Chewa,*(), Z.G. Zhua, F Wenga, S.B. Gaob, F.L. Nga, B.Y Leea, G.J. Bia,*()
Received:
2020-06-20
Revised:
2020-07-29
Accepted:
2020-07-31
Published:
2021-06-30
Online:
2020-11-11
Contact:
Y. Chew,G.J. Bi
About author:
gjbi@simtech.a-star.edu.sg (G.J. Bi).Y. Chew, Z.G. Zhu, F Weng, S.B. Gao, F.L. Ng, B.Y Lee, G.J. Bi. Microstructure and mechanical behavior of laser aided additive manufactured low carbon interstitial Fe49.5Mn30Co10Cr10C0.5 multicomponent alloy[J]. J. Mater. Sci. Technol., 2021, 77: 38-46.
Sample | Co | Cr | Fe | Mn | Ni | O | N | C | Al |
---|---|---|---|---|---|---|---|---|---|
Powder [ | 9.35 | 10.17 | 48.85 | 29.60 | 0.03 | 0.27 | 0.85 | 0.54 | 0.04 |
As-built | 10.09 | 9.91 | 51.29 | 26.97 | 0.03 | 0.24 | 0.86 | 0.46 | <0.02 |
Table 1. Chemical composition of powder and as-built sample (at.%).
Sample | Co | Cr | Fe | Mn | Ni | O | N | C | Al |
---|---|---|---|---|---|---|---|---|---|
Powder [ | 9.35 | 10.17 | 48.85 | 29.60 | 0.03 | 0.27 | 0.85 | 0.54 | 0.04 |
As-built | 10.09 | 9.91 | 51.29 | 26.97 | 0.03 | 0.24 | 0.86 | 0.46 | <0.02 |
Fig. 3. (a) Optical image of as-built part in the cross-sectional plane along the building direction, (b) higher magnification view of the dotted box region in (a), (c) higher magnification view of dotted box region in (b) and (d) higher magnification view of the dotted box region in (c).
Fig. 5. (a) EBSD IPF map for as-built sample along built direction showing general grain orientation angle, (b) IPF for smaller area scan along built direction, (c) KAM map along built direction, (d) High angle grain boundaries along built direction, (e) IPF map along x-y plane (within layer), and (f-i) EDX mapping of elemental distribution of boxed region in (b).
Fig. 6. (a) Engineering stress-strain results, (b) true stress-strain curves and work hardening rate curves for Fe49.5Mn30Co10Cr10C0.5 multicomponent alloy tested at 25 ℃, -40 ℃ and -130 ℃. (c) Fractured surface of the as-built multicomponent alloy at 25°C, (d) higher magnification of the dimple structures showing particles residing within the dimples. (e) EDX showing that the particle contains higher wt.% of Mn and O.
Fig. 7. The EBSD data of the fractured sample tested at 25 ℃. (a) EBSD IPF map for fractured sample along built direction, (b) Grain boundaries map showing TRIP HCP phase and twinning. (c) KAM distribution for fractured sample along built direction. (d) Close-up view grain boundaries map of boxed region in (a). HCP phase is indicated by red regions, while black and blue lines indicate HAGBs and deformation twinning, respectively in (b) and (d).
Fig. 8. All the data given are for fractured sample tested at -40 ℃. (a) EBSD IPF map for fractured sample along built direction, (b) Grain boundaries map showing TRIP HCP phase regions. (c) KAM distribution for fractured sample along built direction. (d) Close-up view grain boundaries map of boxed region in (a). HCP phase is indicated by red regions, while black and blue lines indicate HAGBs and deformation twinning respectively in (b) and (d).
σo | σGB | σDIS | σSEG | σP | Calculatedσy |
---|---|---|---|---|---|
179 | 67.3 | 196 | 113.9 | 24.1 | 580.3 |
Table 2. Calculated contributions from different strengthening components (MPa).
σo | σGB | σDIS | σSEG | σP | Calculatedσy |
---|---|---|---|---|---|
179 | 67.3 | 196 | 113.9 | 24.1 | 580.3 |
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