J. Mater. Sci. Technol. ›› 2020, Vol. 39: 89-98.DOI: 10.1016/j.jmst.2019.08.028
• Research Article • Previous Articles Next Articles
Honggang Donga*(), Yueqing Xiaa, Xinxing Xua, Gul Jabeen Nazb, Xiaohu Haoa, Peng Lia, Jun Zhouc, Chuang Dongb
Received:
2019-07-01
Revised:
2019-08-07
Accepted:
2019-08-12
Published:
2020-02-15
Online:
2020-03-11
Contact:
Dong Honggang
Honggang Dong, Yueqing Xia, Xinxing Xu, Gul Jabeen Naz, Xiaohu Hao, Peng Li, Jun Zhou, Chuang Dong. Performance of GH4169 brazed joint using a new designed nickel-based filler metal via cluster-plus-glue-atom model[J]. J. Mater. Sci. Technol., 2020, 39: 89-98.
Material | Cr | Fe | Mo | Nb | Al | Ti | B | Si | Ni |
---|---|---|---|---|---|---|---|---|---|
GH4169 | 18.06 | 18.90 | 2.96 | 5.43 | 0.58 | 0.94 | - | 0.06 | Bal |
Filler metal | 14.31 | - | - | - | - | - | 2.98 | 1.93 | Bal |
Table 1 Chemical composition (wt. %) of GH4169 alloy and filler metal.
Material | Cr | Fe | Mo | Nb | Al | Ti | B | Si | Ni |
---|---|---|---|---|---|---|---|---|---|
GH4169 | 18.06 | 18.90 | 2.96 | 5.43 | 0.58 | 0.94 | - | 0.06 | Bal |
Filler metal | 14.31 | - | - | - | - | - | 2.98 | 1.93 | Bal |
Spot | Ni | Cr | B | Si | Fe | Mo | Nb | Ti | Al | Possible phase |
---|---|---|---|---|---|---|---|---|---|---|
1 | 72.6 | 17.3 | - | 2.8 | 4.8 | 0.3 | 1.1 | 0.7 | 0.3 | γ-(Ni) solid solution |
2 | 53.2 | 20.3 | - | 0.1 | 20.0 | 1.4 | 2.7 | 1.2 | 1.0 | Substrate in DZ |
3 | 2.2 | 1.0 | - | - | 0.8 | 1.1 | 85.5 | 9.5 | - | (Nb, Ti)-rich phase |
4 | 2.5 | 28.4 | 46.3 | - | 1.8 | 5.6 | 14.4 | 1.0 | - | (Cr, Nb, Mo)-rich borides |
5 | 8.3 | 15.1 | 43.1 | - | 5.8 | 10.5 | 16.1 | 0.9 | 0.1 | (Cr, Nb, Mo)-rich borides |
Table 2 Chemical composition (at. %) of the marked spots in Fig. 5.
Spot | Ni | Cr | B | Si | Fe | Mo | Nb | Ti | Al | Possible phase |
---|---|---|---|---|---|---|---|---|---|---|
1 | 72.6 | 17.3 | - | 2.8 | 4.8 | 0.3 | 1.1 | 0.7 | 0.3 | γ-(Ni) solid solution |
2 | 53.2 | 20.3 | - | 0.1 | 20.0 | 1.4 | 2.7 | 1.2 | 1.0 | Substrate in DZ |
3 | 2.2 | 1.0 | - | - | 0.8 | 1.1 | 85.5 | 9.5 | - | (Nb, Ti)-rich phase |
4 | 2.5 | 28.4 | 46.3 | - | 1.8 | 5.6 | 14.4 | 1.0 | - | (Cr, Nb, Mo)-rich borides |
5 | 8.3 | 15.1 | 43.1 | - | 5.8 | 10.5 | 16.1 | 0.9 | 0.1 | (Cr, Nb, Mo)-rich borides |
Fig. 8. Interfacial microstructure of joints and magnified images of DZ at brazing temperature of 1150 ℃ (a, b), 1180 ℃ (c, d), 1210 ℃ (e, f), and 1240 ℃ (g, h) for 20 min.
Spot | Ni | Cr | B | Si | Fe | Mo | Nb | Ti | Al | Possible phase |
---|---|---|---|---|---|---|---|---|---|---|
1 | 69.2 | 3.9 | - | - | 4.7 | 0.5 | 17.4 | 4.1 | 0.2 | δ phase-Ni3(Nb, Ti) |
2 | 44.5 | 14.2 | - | 1.6 | 13.3 | 3.4 | 21.8 | 1.0 | 0.2 | Laves phase |
Table 3 Chemical composition (at. %) of marked spot in Fig. 10.
Spot | Ni | Cr | B | Si | Fe | Mo | Nb | Ti | Al | Possible phase |
---|---|---|---|---|---|---|---|---|---|---|
1 | 69.2 | 3.9 | - | - | 4.7 | 0.5 | 17.4 | 4.1 | 0.2 | δ phase-Ni3(Nb, Ti) |
2 | 44.5 | 14.2 | - | 1.6 | 13.3 | 3.4 | 21.8 | 1.0 | 0.2 | Laves phase |
Fig. 12. Microstructure of joints brazed at 1150 ℃ for 10 min (a), 20 min (b), 40 min (c), magnified morphology (d-f) of the zones marked with d, e, f.
Fig. 14. Fracture path (a) and fracture morphology (b-d) of joint brazed at 1150 ℃ for 20 min; Fracture path (e) and fracture morphology (f-h) of joint brazed at 1240 ℃ for 20 min.
Spot | Ni | Cr | Fe | Mo | Nb | Si | Ti | Al | Possible phase |
---|---|---|---|---|---|---|---|---|---|
1 | 53.67 | 21.36 | 20.45 | 1.12 | 2.20 | 0.08 | 0.90 | 0.21 | Substrate in DZ |
2 | 70.05 | 18.48 | 4.09 | 0.43 | 1.07 | 4.79 | 0.41 | 0.69 | γ-Ni solid solution |
3 | 40.75 | 14.66 | 12.70 | 3.42 | 24.81 | 1.85 | 0.90 | 0.92 | Laves phase |
4 | 52.62 | 20.34 | 18.74 | 1.71 | 3.44 | 0.36 | 1.05 | 1.74 | Substrate in DZ |
Table 4 Chemical composition (at. %) of marked spots in Fig. 14.
Spot | Ni | Cr | Fe | Mo | Nb | Si | Ti | Al | Possible phase |
---|---|---|---|---|---|---|---|---|---|
1 | 53.67 | 21.36 | 20.45 | 1.12 | 2.20 | 0.08 | 0.90 | 0.21 | Substrate in DZ |
2 | 70.05 | 18.48 | 4.09 | 0.43 | 1.07 | 4.79 | 0.41 | 0.69 | γ-Ni solid solution |
3 | 40.75 | 14.66 | 12.70 | 3.42 | 24.81 | 1.85 | 0.90 | 0.92 | Laves phase |
4 | 52.62 | 20.34 | 18.74 | 1.71 | 3.44 | 0.36 | 1.05 | 1.74 | Substrate in DZ |
Fig. 15. Room-temperature shear strength and high-temperature shear strength of the joint brazed at 1240 ℃/20 min (a); Fracture surface of high-temperature shear sample (b).
Spot | Ni | Cr | Fe | Mo | Nb | Si | Ti | Al | Possible phase |
---|---|---|---|---|---|---|---|---|---|
1 | 51.62 | 20.76 | 19.27 | 1.98 | 3.40 | 0.39 | 1.16 | 1.42 | Substrate in DZ |
2 | 52.22 | 19.88 | 18.83 | 2.18 | 4.00 | 0.37 | 1.14 | 1.38 | Substrate in DZ |
Table 5 Chemical composition (at. %) of marked spots in Fig. 15.
Spot | Ni | Cr | Fe | Mo | Nb | Si | Ti | Al | Possible phase |
---|---|---|---|---|---|---|---|---|---|
1 | 51.62 | 20.76 | 19.27 | 1.98 | 3.40 | 0.39 | 1.16 | 1.42 | Substrate in DZ |
2 | 52.22 | 19.88 | 18.83 | 2.18 | 4.00 | 0.37 | 1.14 | 1.38 | Substrate in DZ |
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