Microstructure Evolution of in situ (Ti3AlC D Ti5Si3)/Ti3Al Composite Sheet with a Novel Quasi-continuous Chain Reinforcement Distribution Architecture Prepared by Using Roll Bonding and Reaction Annealing

doi:10.1016/j.jmst.2013.10.020

J. Mater. Sci. Technol.

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Microstructure Evolution of in situ (Ti3AlC D Ti₅Si₃)/Ti₃Al Composite Sheet with a Novel Quasi-continuous Chain Reinforcement Distribution Architecture Prepared by Using Roll Bonding and Reaction Annealing

J.C. Pang, G.H. Fan, X.P. Cui, A.B. Li, L. Geng, Z.Z. Zheng, Q.W. Wang

School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001, China

Received:2013-04-10 Revised:2013-06-09 Online:2013-12-30 Published:2013-12-24
Contact: G.H. Fan
Supported by:
National Natural Science Foundation of China (Nos. 51071058 and 51101041), and the Fundamental Research Funds for the Central University (Contract Nos. HIT. ICRST.2010007 and HIT. NSRIF. 2010107).

Abstract

Abstract:

The Ti₃Al matrix composite sheet with a novel quasi-continuous chain reinforcement distribution was prepared by using roll bonding and subsequent reaction annealing with pure Ti and SiC_p/Al foils. The (Ti₃AlC + Ti₅Si₃) reinforcements were produced by in situ reaction of the as-rolled Ti–(SiC_p/Al) laminated composite sheet after a two-stage annealing treatment including first annealing at 660 °C and second annealing at 1250 °C. The microstructure evolution during the reaction annealing was investigated. In the first reaction annealing, TiAl₃ was formed, and the SiC particles were pushed together due to the Kirkendall effect, and after the second reaction annealing, Ti₃Al, Ti₃AlC and Ti₅Si₃ were synthesized. In addition, the reinforcement distribution presents a quasi-continuous chain microstructure in Ti₃Al matrix composite sheet.

Key words: Composite, Intermetallic, Fabrication, Reaction synthesis

J.C. Pang, G.H. Fan, X.P. Cui, A.B. Li, L. Geng, Z.Z. Zheng, Q.W. Wang. Microstructure Evolution of in situ (Ti3AlC D Ti₅Si₃)/Ti₃Al Composite Sheet with a Novel Quasi-continuous Chain Reinforcement Distribution Architecture Prepared by Using Roll Bonding and Reaction Annealing[J]. J. Mater. Sci. Technol., DOI: 10.1016/j.jmst.2013.10.020.

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Microstructure Evolution of in situ (Ti3AlC D Ti₅Si₃)/Ti₃Al Composite Sheet with a Novel Quasi-continuous Chain Reinforcement Distribution Architecture Prepared by Using Roll Bonding and Reaction Annealing

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