J. Mater. Sci. Technol. ›› 2021, Vol. 60: 70-76.DOI: 10.1016/j.jmst.2020.04.051
• Research Article • Previous Articles Next Articles
Weiwei Xiaoa, Na Nia,b,*(), Xiaohui Fanb, Xiaofeng Zhaob, Yingzheng Liua, Ping Xiaob
Received:
2020-02-25
Revised:
2020-04-07
Accepted:
2020-04-27
Published:
2021-01-10
Online:
2021-01-22
Contact:
Na Ni
Weiwei Xiao, Na Ni, Xiaohui Fan, Xiaofeng Zhao, Yingzheng Liu, Ping Xiao. Ambient flash sintering of reduced graphene oxide/zirconia composites: Role of reduced graphene oxide[J]. J. Mater. Sci. Technol., 2021, 60: 70-76.
Fig. 1. SEM images of (a) 24h-rGO aerogel and (b) green body of the 5.5 vol.% rGO/3YSZ composites. (c) TG and DSC curves of rGO aerogel. (d) and (e) Change of field strength, current density, power density, linear shrinkage and surface temperature vs. time for a typical sintering experiment used to prepare the 5.5 vol.% rGO/3YSZ composites at room temperature in air under an initial field strength of 60 V/cm and a current limit of 160 mA/mm2. Photographs of (f) the samples in the different stages of the FS experiment and (e) the cross-section of the samples.
Fig. 2. (a) Raman spectra from the black and white parts in the 5.5 vol.% rGO/3YSZ sample sintered under 60 V/cm and 160 mA/mm2 for 20 s. The characteristic graphene ID peak is marked in green. Raman mapping using the graphene ID signal for (b1) a black area and (b2) a black/white interface area in the specimen. (c) BSE image of the polished surface and (d) SE image of the surface after hydrofluoric acid in the composite area.
Fig. 3. (a1)-(b3) SEM images, (c) the porosity and relative density and (d) the grain size distribution of black and white parts of the 5.5 vol.% rGO/3YSZ sample sintered for different holding times.
Fig. 4. Mechanical properties measured by nanoindentation for the 5.5 vol.% rGO/3YSZ sample sintered with the holding time of 20 s. In situ scanning probe imaging of indents formed after the application of 10 mN load in the region of (a) white 3YSZ and (b) black rGO/YSZ composites. (c) Modulus and hardness measured in the black and white regions.
rGO (vol.%) | 0 | 0.6 | 5.5 | 10.0 |
---|---|---|---|---|
Conductivity (S/m) | 1 × 10-7 | 3 × 10-6 | 0.2 | 13 |
Table 1 Green body electrical conductivity of the rGO/YSZ composite.
rGO (vol.%) | 0 | 0.6 | 5.5 | 10.0 |
---|---|---|---|---|
Conductivity (S/m) | 1 × 10-7 | 3 × 10-6 | 0.2 | 13 |
Fig. 5. (a) FS of 0.6 vol.% rGO/YSZ composite at the elevated furnace temperature. (b) FS behavior of the 10.0 vol.% rGO/3YSZ composites at RT. (c) Plot of ln R vs. 10,000/T for the 5.5 vol.% rGO/3YSZ composite sample.
Fig. 6. (a) Electrical response and (b) surface temperature of rGO aerogel under different field strengths. (c) Comparison of the FS behavior of rGO aerogel and 5.5 vol.% rGO/3YSZ composite under the same field strength of 40 V/cm.
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