J. Mater. Sci. Technol. ›› 2021, Vol. 95: 145-157.DOI: 10.1016/j.jmst.2021.02.074
• Research Article • Previous Articles Next Articles
S. Samat, M.Z. Omar*(
), A.H. Baghdadi*(
), I.F. Mohamed, A. Rajabi, A.M. Aziz
Received:2020-11-08
Revised:2021-02-01
Accepted:2021-02-21
Published:2021-12-30
Online:2021-05-24
Contact:
M.Z. Omar,A.H. Baghdadi
About author:baghdadi.amirhossein@gmail.com (A.H. Baghdadi).S. Samat, M.Z. Omar, A.H. Baghdadi, I.F. Mohamed, A. Rajabi, A.M. Aziz. Microstructural evolution, dislocation density and tensile properties of Al-6.5Si-2.1Cu-0.35Mg alloy produced by different casting processes[J]. J. Mater. Sci. Technol., 2021, 95: 145-157.
| Si | Mg | Cu | Fe | Mn | Al |
|---|---|---|---|---|---|
| 6.50 | 0.35 | 2.1 | 0.32 | 0.12 | Bal. |
Table 1 Chemical composition of BM used in this study (wt.%).
| Si | Mg | Cu | Fe | Mn | Al |
|---|---|---|---|---|---|
| 6.50 | 0.35 | 2.1 | 0.32 | 0.12 | Bal. |
| Element | GC | RC | Thixo | HT-Thixo | Intermetallic compound |
|---|---|---|---|---|---|
| Al | 65.4 | 71.4 | 74.3 | 83.7 | Al2Cu |
| Cu | 34.6 | 28.6 | 25.7 | 16.3 | |
| Al | 55.9 | 56.8 | 64.8 | 69.4 | β-Al5FeSi |
| Fe | 26.1 | 22.1 | 21.8 | 20.4 | |
| Si | 18.0 | 21.1 | 12.7 | 10.2 | |
| Al | 50.2 | 53.6 | 55.1 | 62.4 | Al5Cu2Mg8Si6 |
| Cu | 37.4 | 34.8 | 35.8 | 31.1 | |
| Mg | 10.3 | 9.2 | 5.3 | 4.0 | |
| Si | 2.1 | 2.4 | 3.9 | 2.6 |
Table 2 EDS point analysis results for the intermetallic compounds (wt%) of Al-Si-Cu-Mg alloy in Fig. 5.
| Element | GC | RC | Thixo | HT-Thixo | Intermetallic compound |
|---|---|---|---|---|---|
| Al | 65.4 | 71.4 | 74.3 | 83.7 | Al2Cu |
| Cu | 34.6 | 28.6 | 25.7 | 16.3 | |
| Al | 55.9 | 56.8 | 64.8 | 69.4 | β-Al5FeSi |
| Fe | 26.1 | 22.1 | 21.8 | 20.4 | |
| Si | 18.0 | 21.1 | 12.7 | 10.2 | |
| Al | 50.2 | 53.6 | 55.1 | 62.4 | Al5Cu2Mg8Si6 |
| Cu | 37.4 | 34.8 | 35.8 | 31.1 | |
| Mg | 10.3 | 9.2 | 5.3 | 4.0 | |
| Si | 2.1 | 2.4 | 3.9 | 2.6 |
| Sample | α-Al | Silicon Particle | Intermetallic | ||
|---|---|---|---|---|---|
| SF | GS (µm) | D (µm) | AR | Length (µm) | |
| GC | N/A | N/A | 13.5 ± 1.3 | 3.1 | 60 ± 4 |
| RC | 0.85 ± 0.08 | 43 ± 4 | 3.8 ± 0.3 | 2.2 | 22 ± 3 |
| Thixo | 0.82 ± 0.07 | 57 ± 4 | 3.5 ± 0.4 | 2.1 | 10 ± 3 |
| HT-Thixo | 0.84 ± 0.06 | 58 ± 2 | 2.2 ± 0.1 | 1.3 | 3 ± 2 |
Table 3 Quantitative metallographic assessment of the microstructural features of GC, RC, Thixo, and HT-Thixo Al-Si-Cu-Mg alloys.
| Sample | α-Al | Silicon Particle | Intermetallic | ||
|---|---|---|---|---|---|
| SF | GS (µm) | D (µm) | AR | Length (µm) | |
| GC | N/A | N/A | 13.5 ± 1.3 | 3.1 | 60 ± 4 |
| RC | 0.85 ± 0.08 | 43 ± 4 | 3.8 ± 0.3 | 2.2 | 22 ± 3 |
| Thixo | 0.82 ± 0.07 | 57 ± 4 | 3.5 ± 0.4 | 2.1 | 10 ± 3 |
| HT-Thixo | 0.84 ± 0.06 | 58 ± 2 | 2.2 ± 0.1 | 1.3 | 3 ± 2 |
| Sample | GC | RC | Thixo | HT-Thixo |
|---|---|---|---|---|
| Hardness (HV) | 93 ± 2 | 95 ± 3 | 100 ± 2 | 124 ± 2 |
Table 4 Hardness values of GC, RC, Thixo, and HT-Thixo Al-Si-Cu-Mg alloys.
| Sample | GC | RC | Thixo | HT-Thixo |
|---|---|---|---|---|
| Hardness (HV) | 93 ± 2 | 95 ± 3 | 100 ± 2 | 124 ± 2 |
Fig. 14. Determination of the lattice parameters of Al-Si-Cu-Mg alloys fabricated through different casting processes based on the Nelson-Riley method.
| Sample | d (nm) | ε (%) | a (Nelson-Riley Method) (Å) | b (10-10 m) | ρ × 1014 (m - 2) |
|---|---|---|---|---|---|
| GC | 231.15 | 0.22 | 4.0391 | 2.856075000 | 1.15438 |
| RC | 92.46 | 0.26 | 4.0502 | 2.863923885 | 3.40133 |
| Thixo | 69.34 | 0.30 | 4.0522 | 2.865338099 | 5.23061 |
| HT-Thixo | 66.00 | 0.28 | 4.0523 | 2.865408809 | 5.12883 |
Table 5 Dislocation density of GC, RC, Thixo, and HT-Thixo Al-Si-Cu-Mg alloys.
| Sample | d (nm) | ε (%) | a (Nelson-Riley Method) (Å) | b (10-10 m) | ρ × 1014 (m - 2) |
|---|---|---|---|---|---|
| GC | 231.15 | 0.22 | 4.0391 | 2.856075000 | 1.15438 |
| RC | 92.46 | 0.26 | 4.0502 | 2.863923885 | 3.40133 |
| Thixo | 69.34 | 0.30 | 4.0522 | 2.865338099 | 5.23061 |
| HT-Thixo | 66.00 | 0.28 | 4.0523 | 2.865408809 | 5.12883 |
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