J. Mater. Sci. Technol. ›› 2022, Vol. 107: 43-51.DOI: 10.1016/j.jmst.2021.07.039
• Research Article • Previous Articles Next Articles
Junlei Wanga,b, Hongfang Liub,*(
), Magdy El-Said Mohamedc, Mazen A.Salehc, Tingyue Gua,*()
Received:2021-05-17
Revised:2021-05-17
Accepted:2021-05-17
Published:2022-04-30
Online:2022-04-28
Contact:
Hongfang Liu,Tingyue Gu
About author:gu@ohio.edu (T. Gu).Junlei Wang, Hongfang Liu, Magdy El-Said Mohamed, Mazen A.Saleh, Tingyue Gu. Mitigation of sulfate reducing Desulfovibrio ferrophilus microbiologically influenced corrosion of X80 using THPS biocide enhanced by Peptide A[J]. J. Mater. Sci. Technol., 2022, 107: 43-51.
| C | P | S | Si | Mn | Cr | Ni | Mo | N | Cu | Nb | Al | Ti | B | V |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 0.07 | 0.007 | 0.023 | 0.19 | 1.82 | 0.026 | 0.17 | 0.01 | 0.004 | 0.02 | 0.056 | 0.028 | 0.012 | 0.0001 | 0.002 |
Table 1 Elemental composition (wt%) of X80 carbon steel (Fe balance).
| C | P | S | Si | Mn | Cr | Ni | Mo | N | Cu | Nb | Al | Ti | B | V |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 0.07 | 0.007 | 0.023 | 0.19 | 1.82 | 0.026 | 0.17 | 0.01 | 0.004 | 0.02 | 0.056 | 0.028 | 0.012 | 0.0001 | 0.002 |
Fig. 1. Anaerobic vials with different THPS concentrations after 7-day SRB incubation: (a) 0 ppm, (b) 20 ppm, (c) 30 ppm, (d) 40 ppm, (e) 50 ppm.
| THPS (ppm) | Planktonic (× 106 cells/mL) | Sessile (× 107 cells/cm2) |
|---|---|---|
| 0 | 3.5 | 7.9 |
| 20 | 2.8 | 7.3 |
| 50 | Undetectable | Undetectable |
Table 2 D. ferrophilus planktonic cell count (hemocytometer) and sessile cell count (MPN) after 7-day incubation.
| THPS (ppm) | Planktonic (× 106 cells/mL) | Sessile (× 107 cells/cm2) |
|---|---|---|
| 0 | 3.5 | 7.9 |
| 20 | 2.8 | 7.3 |
| 50 | Undetectable | Undetectable |
| THPS (ppm) | Weight loss (mg/cm2) | Corrosion rate (mm/a) | η (%) |
|---|---|---|---|
| 0 | 19.7 | 1.31 | - |
| 20 | 17.8 | 1.18 | 10 |
| 50 | 1.65 | 0.11 | 92 |
Table 3 Weight loss after 7-day incubation and corrosion inhibition efficiency based on weight loss reduction.
| THPS (ppm) | Weight loss (mg/cm2) | Corrosion rate (mm/a) | η (%) |
|---|---|---|---|
| 0 | 19.7 | 1.31 | - |
| 20 | 17.8 | 1.18 | 10 |
| 50 | 1.65 | 0.11 | 92 |
Fig. 2. Surface profiles of X80 carbon steel after 7-day incubation with (a) 0 ppm THPS, (b) 20 ppm THPS, (c) 50 ppm THPS.
Fig. 3. Nyquist and Bode plots of X80 with different concentrations of THPS in the EASW during 7-day incubation: (a, a1) 0 ppm THPS, (b, b1) 20 ppm THPS, (c, c1) 50 ppm THPS.
| THPS(ppm) | Time (day) | Rs (Ω cm2) | Qf (Ω-1 sn1 cm-2) | n1 | Rf (Ω cm2) | Qdl (Ω-1 sn2 cm-2) | n2 | Rct (kΩ cm2) |
|---|---|---|---|---|---|---|---|---|
| 0 | 1 | 8.46 | 5.43 × 10-2 | 0.91 | 164 | 5.95 × 10-1 | 0.91 | 0.13 |
| 3 | 8.43 | 6.13 × 10-2 | 0.89 | 1.36 | 1.58 × 10-1 | 0.88 | 0.20 | |
| 5 | 8.99 | 1.89 × 10-1 | 0.85 | 1.87 | 5.29 × 10-1 | 0.95 | 0.31 | |
| 7 | 8.60 | 2.29 × 10-1 | 0.86 | 2.51 | 5.12 × 10-1 | 0.96 | 0.29 | |
| 20 | 1 | 10.1 | 1.42 × 10-3 | 0.95 | 37.4 | 5.09 × 10-4 | 0.86 | 1.04 |
| 3 | 9.86 | 3.00 × 10-4 | 0.91 | 0.13 | 6.59 × 10-2 | 0.80 | 0.33 | |
| 5 | 9.61 | 2.64 × 10-2 | 0.89 | 0.68 | 1.07 × 10-1 | 0.80 | 0.30 | |
| 7 | 9.18 | 3.86 × 10-1 | 0.89 | 2.14 | 3.91 × 10-1 | 0.91 | 0.21 | |
| 50 | 1 | 10.9 | 2.70 × 10-4 | 0.90 | 237 | 5.51 × 10-3 | 0.51 | 1.64 |
| 3 | 11.0 | 5.00 × 10-4 | 0.91 | 251 | 6.71 × 10-3 | 0.61 | 1.60 | |
| 5 | 11.2 | 6.45 × 10-4 | 0.92 | 241 | 7.06 × 10-3 | 0.66 | 1.30 | |
| 7 | 12.3 | 8.16 × 10-4 | 0.92 | 246 | 7.18 × 10-3 | 0.68 | 1.37 |
Table 4 Fitted electrochemical parameters from EIS data in Fig. 3.
| THPS(ppm) | Time (day) | Rs (Ω cm2) | Qf (Ω-1 sn1 cm-2) | n1 | Rf (Ω cm2) | Qdl (Ω-1 sn2 cm-2) | n2 | Rct (kΩ cm2) |
|---|---|---|---|---|---|---|---|---|
| 0 | 1 | 8.46 | 5.43 × 10-2 | 0.91 | 164 | 5.95 × 10-1 | 0.91 | 0.13 |
| 3 | 8.43 | 6.13 × 10-2 | 0.89 | 1.36 | 1.58 × 10-1 | 0.88 | 0.20 | |
| 5 | 8.99 | 1.89 × 10-1 | 0.85 | 1.87 | 5.29 × 10-1 | 0.95 | 0.31 | |
| 7 | 8.60 | 2.29 × 10-1 | 0.86 | 2.51 | 5.12 × 10-1 | 0.96 | 0.29 | |
| 20 | 1 | 10.1 | 1.42 × 10-3 | 0.95 | 37.4 | 5.09 × 10-4 | 0.86 | 1.04 |
| 3 | 9.86 | 3.00 × 10-4 | 0.91 | 0.13 | 6.59 × 10-2 | 0.80 | 0.33 | |
| 5 | 9.61 | 2.64 × 10-2 | 0.89 | 0.68 | 1.07 × 10-1 | 0.80 | 0.30 | |
| 7 | 9.18 | 3.86 × 10-1 | 0.89 | 2.14 | 3.91 × 10-1 | 0.91 | 0.21 | |
| 50 | 1 | 10.9 | 2.70 × 10-4 | 0.90 | 237 | 5.51 × 10-3 | 0.51 | 1.64 |
| 3 | 11.0 | 5.00 × 10-4 | 0.91 | 251 | 6.71 × 10-3 | 0.61 | 1.60 | |
| 5 | 11.2 | 6.45 × 10-4 | 0.92 | 241 | 7.06 × 10-3 | 0.66 | 1.30 | |
| 7 | 12.3 | 8.16 × 10-4 | 0.92 | 246 | 7.18 × 10-3 | 0.68 | 1.37 |
Fig. 4. Equivalent circuit model used for fitting EIS data in Fig. 3.
Fig. 5. (a) Daily Rp curves, and (b) PDP curves at the end of 7-day incubation.
| THPS (ppm) | βa (V/dec) | βc (V/dec) | Ecorr (V) vs. SCE | icorr (A/cm2) | ηi (%) |
|---|---|---|---|---|---|
| 0 | - | - 1.9 | - 0.78 | 5.0 × 10-4 | - |
| 20 | 0.98 | - | - 0.77 | 4.6 × 10-4 | 8 |
| 50 | 0.06 | - 0.53 | - 0.66 | 2.0 × 10-5 | 96 |
Table 5 Tafel parameters fitted from Fig. 5(b) PDP curves together with calculated corrosion inhibition efficiency based on icorr reduction.
| THPS (ppm) | βa (V/dec) | βc (V/dec) | Ecorr (V) vs. SCE | icorr (A/cm2) | ηi (%) |
|---|---|---|---|---|---|
| 0 | - | - 1.9 | - 0.78 | 5.0 × 10-4 | - |
| 20 | 0.98 | - | - 0.77 | 4.6 × 10-4 | 8 |
| 50 | 0.06 | - 0.53 | - 0.66 | 2.0 × 10-5 | 96 |
| 20 ppm THPS + Peptide A (ppb) | Planktonic (cells/mL) | Sessile (cells/cm2) |
|---|---|---|
| 0 | 2.8 × 106 | 7.3 × 107 |
| 10 | 2.0 × 106 | 4.5 × 105 |
| 100 | 1.7 × 106 | 5.3 × 103 |
Table 6 Planktonic and sessile cell counts after 7-day incubation for different biocide treatments.
| 20 ppm THPS + Peptide A (ppb) | Planktonic (cells/mL) | Sessile (cells/cm2) |
|---|---|---|
| 0 | 2.8 × 106 | 7.3 × 107 |
| 10 | 2.0 × 106 | 4.5 × 105 |
| 100 | 1.7 × 106 | 5.3 × 103 |
| 20 ppm THPS + Peptide A (ppb) | Weight loss (mg/cm2) | Corrosion rate (mm/a) | Enhancement (%) |
|---|---|---|---|
| 0 | 17.8 | 1.18 | - |
| 10 | 5.4 | 0.36 | 69 |
| 100 | 3.0 | 0.20 | 83 |
Table 7 Weight losses after 7-day incubation for different biocide treatments and corrosion inhibition enhancements.
| 20 ppm THPS + Peptide A (ppb) | Weight loss (mg/cm2) | Corrosion rate (mm/a) | Enhancement (%) |
|---|---|---|---|
| 0 | 17.8 | 1.18 | - |
| 10 | 5.4 | 0.36 | 69 |
| 100 | 3.0 | 0.20 | 83 |
Fig. 6. Surface profiles of X80 after 7-day incubation: (a) 20 ppm THPS (from Fig. 2(b)), (b) 20 ppm THPS + 10 ppb Peptide A, (c) 20 ppm THPS + 100 ppb Peptide A.
Fig. 7. Nyquist and Bode plots of X80 during 7-day incubation: (a, a1) 20 ppm THPS + 10 ppb Peptide A, (b, b1) 20 ppm THPS + 100 ppb Peptide A.
| 20 ppm THPS + Peptide A (ppb) | Time (day) | Rs (Ω cm2) | Qf(Ω-1 sn1 cm-2) | n1 | Rf (Ω cm2) | Qdl (Ω-1 sn2 cm-2) | n2 | Rct (kΩ cm2) |
|---|---|---|---|---|---|---|---|---|
| 10 | 1 | 9.55 | 3.25 × 10-4 | 0.89 | 222 | 7.67 × 10-4 | 0.46 | 1.11 |
| 3 | 9.34 | 5.54 × 10-3 | 0.80 | 1.41 | 3.84 × 10-2 | 0.81 | 0.67 | |
| 5 | 4.89 | 1.93 × 10-1 | 0.92 | 2.05 | 1.63 × 10-1 | 0.86 | 0.47 | |
| 7 | 4.23 | 1.03 × 10-1 | 0.98 | 1.11 | 1.89 × 10-1 | 0.84 | 0.42 | |
| 100 | 1 | 7.07 | 6.93 × 10-4 | 0.81 | 288 | 5.95 × 10-4 | 0.80 | 1.80 |
| 3 | 10.4 | 2.08 × 10-3 | 0.95 | 185 | 6.87 × 10-4 | 0.81 | 0.80 | |
| 5 | 6.21 | 2.65 × 10-2 | 0.93 | 180 | 1.11 × 10-2 | 0.66 | 1.60 | |
| 7 | 5.53 | 2.66 × 10-2 | 0.92 | 179 | 1.40 × 10-2 | 0.84 | 1.28 |
Table 8 Fitted electrochemical parameters from the EIS data in Fig. 7.
| 20 ppm THPS + Peptide A (ppb) | Time (day) | Rs (Ω cm2) | Qf(Ω-1 sn1 cm-2) | n1 | Rf (Ω cm2) | Qdl (Ω-1 sn2 cm-2) | n2 | Rct (kΩ cm2) |
|---|---|---|---|---|---|---|---|---|
| 10 | 1 | 9.55 | 3.25 × 10-4 | 0.89 | 222 | 7.67 × 10-4 | 0.46 | 1.11 |
| 3 | 9.34 | 5.54 × 10-3 | 0.80 | 1.41 | 3.84 × 10-2 | 0.81 | 0.67 | |
| 5 | 4.89 | 1.93 × 10-1 | 0.92 | 2.05 | 1.63 × 10-1 | 0.86 | 0.47 | |
| 7 | 4.23 | 1.03 × 10-1 | 0.98 | 1.11 | 1.89 × 10-1 | 0.84 | 0.42 | |
| 100 | 1 | 7.07 | 6.93 × 10-4 | 0.81 | 288 | 5.95 × 10-4 | 0.80 | 1.80 |
| 3 | 10.4 | 2.08 × 10-3 | 0.95 | 185 | 6.87 × 10-4 | 0.81 | 0.80 | |
| 5 | 6.21 | 2.65 × 10-2 | 0.93 | 180 | 1.11 × 10-2 | 0.66 | 1.60 | |
| 7 | 5.53 | 2.66 × 10-2 | 0.92 | 179 | 1.40 × 10-2 | 0.84 | 1.28 |
Fig. 8. OCP vs. time during 7-day incubation.
Fig. 9. Rp (a) and PDP curves (b) of X80 with 20 ppm THPS and various Peptide A concentrations.
| 20 ppm THPS + Peptide A (ppb) | βa (V/dec) | βc (V/dec) | Ecorr (V) vs. SCE | icorr (A/cm2) | Enhancement (%) |
|---|---|---|---|---|---|
| 0 | 0.98 | - | - 0.77 | 4.6 × 10-4 | - |
| 10 | 0.19 | - 0.36 | - 0.61 | 1.9 × 10-4 | 59 |
| 100 | 0.19 | - 0.20 | - 0.59 | 2.3 × 10-5 | 95 |
Table 9 Tafel parameters fitted from PDP curves in Fig. 9(b) and corrosion inhibition enhancements by Peptide A.
| 20 ppm THPS + Peptide A (ppb) | βa (V/dec) | βc (V/dec) | Ecorr (V) vs. SCE | icorr (A/cm2) | Enhancement (%) |
|---|---|---|---|---|---|
| 0 | 0.98 | - | - 0.77 | 4.6 × 10-4 | - |
| 10 | 0.19 | - 0.36 | - 0.61 | 1.9 × 10-4 | 59 |
| 100 | 0.19 | - 0.20 | - 0.59 | 2.3 × 10-5 | 95 |
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