J. Mater. Sci. Technol. ›› 2022, Vol. 99: 277-287.DOI: 10.1016/j.jmst.2021.02.033
• Research article • Previous Articles
Hao Guoa,b,d, Shufeng Yangb,c,*(), Tiantian Wangb,c, Hang Yuanb,c, Yanling Zhanga, Jingshe Lib,c
Received:
2020-12-28
Revised:
2021-02-08
Accepted:
2021-02-28
Published:
2022-02-10
Online:
2022-02-09
Contact:
Shufeng Yang
About author:
* Beijing Key Laboratory of Special Melting and Prepa- ration of High-end Metals, University of Science and Technology Beijing, Beijing 100083, China. E-mail address: yangshufeng@ustb.edu.cn (S. Yang).Hao Guo, Shufeng Yang, Tiantian Wang, Hang Yuan, Yanling Zhang, Jingshe Li. Microstructure evolution and acicular ferrite nucleation in inclusion-engineered steel with modified MgO@C nanoparticle addition[J]. J. Mater. Sci. Technol., 2022, 99: 277-287.
Fig. 1. Typical TEM images, (d) and (e) XRD patterns, (f) and (g) NP size distributions of the original and surface-modified NPs, and (h) schematic diagram of NP surface treatment process [32].
C | Mn | Si | P | S | Als | T.O. | Fe |
---|---|---|---|---|---|---|---|
0.17 | 0.84 | 0.2 | 0.035 | 0.023 | 0.008 | 0.0032 | Bal. |
Table 1 Chemical composition of steel material (wt.%).
C | Mn | Si | P | S | Als | T.O. | Fe |
---|---|---|---|---|---|---|---|
0.17 | 0.84 | 0.2 | 0.035 | 0.023 | 0.008 | 0.0032 | Bal. |
No NP addition | 0.01% NP addition | 0.03% NP addition | |
---|---|---|---|
Water cooling | S0 | S1 | S2 |
Air cooling | A0 | A1 | A2 |
Table 2 Groups with different mass fractions of NPs addition (wt.%) and cooling conditions.
No NP addition | 0.01% NP addition | 0.03% NP addition | |
---|---|---|---|
Water cooling | S0 | S1 | S2 |
Air cooling | A0 | A1 | A2 |
Low cooling rate (-5°C s-1) | S0-l | S2-l |
---|---|---|
High cooling rate (-15°C s-1) | S0-h | S2-h |
Table 3 S0/S2 steel samples for in-situ observation under LSCM.
Low cooling rate (-5°C s-1) | S0-l | S2-l |
---|---|---|
High cooling rate (-15°C s-1) | S0-h | S2-h |
Fig. 8. Typical microstructures of the steel samples with (a) no; (c) 0.01%; (e) 0.03% NP addition under air cooling and the steel samples with (b) no; (d) 0.01%; (f) 0.03% NP addition under water quenching.
Fig. 10. Typical morphology and energy spectrum analysis of (a) the ferrite induced by MgAl2O4 spinel in S2 steel sample, (b) the Al2O3 in S0 steel sample, typical SEM image (c) and EDS analysis (d) of the TiN inclusion.
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