J. Mater. Sci. Technol. ›› 2021, Vol. 67: 211-225.DOI: 10.1016/j.jmst.2020.06.034
• Research article • Previous Articles Next Articles
Shuai-Feng Chena,b, Hong-Wu Songa, Ming Chenga, Ce Zhenga,c, Shi-Hong Zhanga,*(), Myoung-Gyu Leeb,*()
Received:
2020-05-05
Revised:
2020-06-04
Accepted:
2020-06-04
Published:
2021-03-20
Online:
2021-04-15
Contact:
Shi-Hong Zhang,Myoung-Gyu Lee
About author:
myounglee@snu.ac.kr(M.-G. Lee).Shuai-Feng Chen, Hong-Wu Song, Ming Cheng, Ce Zheng, Shi-Hong Zhang, Myoung-Gyu Lee. Texture modification and mechanical properties of AZ31 magnesium alloy sheet subjected to equal channel angular bending[J]. J. Mater. Sci. Technol., 2021, 67: 211-225.
Fig. 2. Schematic of ECAB process: (a) key die geometry and processing parameters; (b) single pass at various temperatures and different routes at 200 °C (Route A and Route C).
Fig. 3. The accumulation of shear strain during ECAB: (a) specimen meshes after RA-P1 (e.g. single pass); (b) measured and calculated shear strain ${{\gamma }_{13}}$ for RA-P1; (c) specimen meshes after RA-P3 (e.g. three monotonic passes); (d) measured and calculated shear strain ${{\gamma }_{13}}$ for RA-P2 and RA-P3. Here, t/t0 equal to 0 and 1 indicates upper and lower sheet surface, respectively.
Fig. 4. EBSD measured IPF maps, twinning on band contrast maps, and (0001) PFs of ECAB specimens processed under different temperatures: (a)-(c) ECAB-RT; (d)-(f) ECAB-150; (g)-(i) ECAB-200 Region 1 (R1); (j)-(l) ECAB-250.
Fig. 5. (a) Schematic of EBSD region selection (boundary region, R1 and center region, R2); (b) IPF map and (c) (0001) PF for ECAB-200 R2. The boundary region can be distinguished with the center region by the slight differences in sheet thickness.
Fig. 7. EBSD measured twinning on band contrast and tilted angles between c-axis and ND: (a), (d) twinning map, (b), (e) titled angles ranging from 0° to 90°, and (c), (f) tilted angles within 30° with (a)-(c) for RA-P3 and (d)-(f) for RC-P3.
Fig. 8. EBSD measured IPF maps, twinning on band contrast maps, and (0001) PFs of annealed ECAB specimens: (a)-(c) ECAB-150; (d)-(f) RA-P3 R1; (g)-(i) RA-P3 R2; (j)-(l) RC-P3.
Fig. 9. Distributions of (a) tilted angles between c-axis and ND and (b) grain size of initial and annealed ECAB specimens extracted from Fig. 1, Fig. 8.
Fig. 10. True stress-train curves of annealed samples during tension along RD: (a) single ECAB pass and (b) different router ECAB; (c) necking features. Note that the tension test of ECAB-RT sheet was not performed since ECAB-RT sheet was fractured.
Samples | Strength (MPa) | Elongation (%) | Swift hardening law | ||
---|---|---|---|---|---|
${{\sigma }_{0.2}}$ | ${{\sigma }_{UTS}}$ | ${{\delta }_{u}}$ | ${{\delta }_{f}}$ | $\bar{\sigma }=k{{\left( {{\varepsilon }_{0}}+\bar{\varepsilon } \right)}^{n}}$ | |
Initial sheet | 150.3 | 248.8 | 14.94 | 17.12 | $464.4{{\left( 0.010+\bar{\varepsilon } \right)}^{0.245}}$ |
ECAB-150 | 121.5 | 246.5 | 24.07 | 25.76 | $559.3{{\left( 0.016+\bar{\varepsilon } \right)}^{0.394}}$ |
ECAB-200 | 116.2 | 241.4 | 19.45 | 21.08 | $513.7{{\left( 0.011+\bar{\varepsilon } \right)}^{0.316}}$ |
ECAB-250 | 143.7 | 251.3 | 15.88 | 16.23 | $463.1{{\left( 0.007+\bar{\varepsilon } \right)}^{0.241}}$ |
RA-P3 | 103.0 | 236.6 | 20.99 | 22.15 | $536.4{{\left( 0.011+\bar{\varepsilon } \right)}^{0.376}}$ |
RC-P3 | 100.8 | 238.5 | 25.83 | 27.43 | $573.6{{\left( 0.008+\bar{\varepsilon } \right)}^{0.426}}$ |
Table 1 The yield stress (${{\sigma }_{0.2}}$), ultimate tension stress (${{\sigma }_{UTS}}$), uniform (${{\delta }_{u}}$) and final (${{\delta }_{f}}$) elongations, Swift hardening law fitting of the initial and annealed ECAB sheets.
Samples | Strength (MPa) | Elongation (%) | Swift hardening law | ||
---|---|---|---|---|---|
${{\sigma }_{0.2}}$ | ${{\sigma }_{UTS}}$ | ${{\delta }_{u}}$ | ${{\delta }_{f}}$ | $\bar{\sigma }=k{{\left( {{\varepsilon }_{0}}+\bar{\varepsilon } \right)}^{n}}$ | |
Initial sheet | 150.3 | 248.8 | 14.94 | 17.12 | $464.4{{\left( 0.010+\bar{\varepsilon } \right)}^{0.245}}$ |
ECAB-150 | 121.5 | 246.5 | 24.07 | 25.76 | $559.3{{\left( 0.016+\bar{\varepsilon } \right)}^{0.394}}$ |
ECAB-200 | 116.2 | 241.4 | 19.45 | 21.08 | $513.7{{\left( 0.011+\bar{\varepsilon } \right)}^{0.316}}$ |
ECAB-250 | 143.7 | 251.3 | 15.88 | 16.23 | $463.1{{\left( 0.007+\bar{\varepsilon } \right)}^{0.241}}$ |
RA-P3 | 103.0 | 236.6 | 20.99 | 22.15 | $536.4{{\left( 0.011+\bar{\varepsilon } \right)}^{0.376}}$ |
RC-P3 | 100.8 | 238.5 | 25.83 | 27.43 | $573.6{{\left( 0.008+\bar{\varepsilon } \right)}^{0.426}}$ |
Fig. 11. Mechanical properties of initial and annealed ECAB sheets: (a) yield stress ${{\sigma }_{0.2}}$, ultimate tension stress ${{\sigma }_{UTS}}$; (b) elongations ${{\delta }_{u}}$ and ${{\delta }_{f}}$, n values for Swift hardening law.
Samples | Prismatic < a > slip | Basal < a > slip | ETW 10$\bar{1}$2 |
---|---|---|---|
Initial sheet | 17.1 % | 79.7 % | 3.2 % |
ECAB-150 | 17.2 % | 65 .1 % | 17.7 % |
RA-P3 R1 | 13.7 % | 63.7 % | 22.6 % |
RA-P3 R2 | 27.3 % | 63.9 % | 8.8 % |
RC-P3 | 17.4 % | 53.9 % | 28.7 % |
Table 2 The area fractions of grains favoring prismatic and basal < a > slips, and ETW for initial and annealed EBSD sheets during tension along RD.
Samples | Prismatic < a > slip | Basal < a > slip | ETW 10$\bar{1}$2 |
---|---|---|---|
Initial sheet | 17.1 % | 79.7 % | 3.2 % |
ECAB-150 | 17.2 % | 65 .1 % | 17.7 % |
RA-P3 R1 | 13.7 % | 63.7 % | 22.6 % |
RA-P3 R2 | 27.3 % | 63.9 % | 8.8 % |
RC-P3 | 17.4 % | 53.9 % | 28.7 % |
Fig. 14. The strain hardening rates of (a) single ECAB pass and (b) different ECAB routes derived from the true strain-stress curves in Fig. 11 (a) and (b) respectively.
Fig. 18. EBSD measured IPF and twinning maps: (a) ECAB-150; (b) RC-P3 at the vicinity of sample fracture; (c) schematic of the strain accommodation mechanism for mixture of basal and non-basal orientation grains.
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