J. Mater. Sci. Technol. ›› 2020, Vol. 47: 20-28.DOI: 10.1016/j.jmst.2020.01.041
• Research Article • Previous Articles Next Articles
Praveen Sreeramagiri, Ajay Bhagavatam, Abhishek Ramakrishnan, Husam Alrehaili, Guru Prasad Dinda*()
Received:
2019-10-11
Revised:
2019-12-19
Accepted:
2020-01-07
Published:
2020-06-15
Online:
2020-06-24
Contact:
Guru Prasad Dinda
Praveen Sreeramagiri, Ajay Bhagavatam, Abhishek Ramakrishnan, Husam Alrehaili, Guru Prasad Dinda. Design and development of a high-performance Ni-based superalloy WSU 150 for additive manufacturing[J]. J. Mater. Sci. Technol., 2020, 47: 20-28.
Fig. 1. Robotic laser metal deposition (LMD) equipment developed at Wayne State University. (a) Robotic arm with a nozzle attached through the optical fiber, (b) Image demonstrating the combinatorial alloy development technique with LMD.
Fig. 2. SEM images of the as-deposited gradient samples showing the microstructural morphology of γ? particles. (a → h) Showing the increasing trend of size and volume fraction of γ? with the increase of high γ? alloy content in the sample.
Element (Wt%) | Ni | Cr | C | Mo | Co | W | Cb (Nb) | Ti | Ta | Al |
---|---|---|---|---|---|---|---|---|---|---|
WSU150 | 59.64 | 17.83 | 0.09 | 5.3 | 9.29 | 1.33 | 0.45 | 2.75 | 0.9 | 2.44 |
Table 1 Chemical composition of the new WSU 150 alloy powder.
Element (Wt%) | Ni | Cr | C | Mo | Co | W | Cb (Nb) | Ti | Ta | Al |
---|---|---|---|---|---|---|---|---|---|---|
WSU150 | 59.64 | 17.83 | 0.09 | 5.3 | 9.29 | 1.33 | 0.45 | 2.75 | 0.9 | 2.44 |
Alloy | Laser Power (Watt) | Scan Speed (mm/min) | Powder Flow Rate (gm/min) | Shaping Gas (ft3/hr) | Powder Carrier Gas (ft3/hr) |
---|---|---|---|---|---|
WSU 150 | 750 | 720 | 14.5 | 15 | 15 |
Table 2 Process parameters used for the deposition of WSU 150.
Alloy | Laser Power (Watt) | Scan Speed (mm/min) | Powder Flow Rate (gm/min) | Shaping Gas (ft3/hr) | Powder Carrier Gas (ft3/hr) |
---|---|---|---|---|---|
WSU 150 | 750 | 720 | 14.5 | 15 | 15 |
Fig. 3. (a) Block deposited for the tension test coupons, (b) Tension test sample dimensions in accordance with ASTM E8 standards, (c) Tension test sample prepared according to (b).
Fig. 4. (a) CALPHAD based solidification modeling for WSU 150, (b) Schiel based elemental segregation model for WSU 150 from start to the end of solidification.
Fig. 5. SEM analysis of as-deposited WSU 150. (a) Low magnification image showing the dendrite (gray contrast) and interdendritic region (lighter region), (b-c) Dendrite with different cores, (d) γ? particles at the center of the dendrite, (e) Transition zone of two cores with a different precipitate size distribution, and (f) Magnified view of (c) showing different cores and size distribution of γ? particles.
Fig. 6. SEM analysis of WSU 150 aged at 760 °C for 4 h, (a) Transition from one core to other core, (b) Dendrite and interdendritic region with carbides in the interdendritic region, (c) Dendrite and interdendritic region, (d) Magnified view of (a) showing different cores and size distribution of γ? particles.
(a) | |||
---|---|---|---|
Location | 1 | 2 | 3 |
Element | Wt.% | Wt.% | Wt.% |
Al | 19.59 | 2.81 | 2.73 |
Ta | 1.32 | 1.84 | 1.72 |
W | 2.98 | 2.5 | 2.79 |
Mo | 5.26 | 5.28 | 5.31 |
Ti | 2.02 | 2.32 | 2.29 |
Cr | 14.83 | 17.6 | 17.64 |
Co | 7.87 | 9.46 | 9.91 |
Ni | 46.13 | 58.18 | 57.62 |
(b) | |||
Location | 1 | 2 | 3 |
Element | Wt.% | Wt.% | Wt.% |
Al | 2.84 | 2.83 | 2.91 |
Ta | 1.91 | 1.83 | 1.98 |
W | 2.37 | 2.73 | 2.53 |
Mo | 5.02 | 5.21 | 5.43 |
Ti | 2.38 | 2.56 | 2.79 |
Cr | 17.75 | 17.81 | 17.5 |
Co | 9.24 | 9.03 | 8.97 |
Ni | 58.5 | 58.01 | 57.9 |
Table 3 The EDS analysis on the sample referenced to Fig. 7.
(a) | |||
---|---|---|---|
Location | 1 | 2 | 3 |
Element | Wt.% | Wt.% | Wt.% |
Al | 19.59 | 2.81 | 2.73 |
Ta | 1.32 | 1.84 | 1.72 |
W | 2.98 | 2.5 | 2.79 |
Mo | 5.26 | 5.28 | 5.31 |
Ti | 2.02 | 2.32 | 2.29 |
Cr | 14.83 | 17.6 | 17.64 |
Co | 7.87 | 9.46 | 9.91 |
Ni | 46.13 | 58.18 | 57.62 |
(b) | |||
Location | 1 | 2 | 3 |
Element | Wt.% | Wt.% | Wt.% |
Al | 2.84 | 2.83 | 2.91 |
Ta | 1.91 | 1.83 | 1.98 |
W | 2.37 | 2.73 | 2.53 |
Mo | 5.02 | 5.21 | 5.43 |
Ti | 2.38 | 2.56 | 2.79 |
Cr | 17.75 | 17.81 | 17.5 |
Co | 9.24 | 9.03 | 8.97 |
Ni | 58.5 | 58.01 | 57.9 |
Condition | AD | HT @760 °C/4 h | |
---|---|---|---|
Name | Units | WSU150 | |
Young’ Modulus ‘E’ | GPa | 191.32 | 201.84 |
Yield Strength | MPa | 867 | 1113.84 |
Ultimate Tensile Strength ‘UTS’ | MPa | 1188 | 1396 |
Engineering Strain at UTS | % | 27.57 | 16.05 |
% Elongation | % | 27.9 | 16.1 |
Fracture Stress | MPa | 1164.04 | 1386.32 |
Table 4 Mechanical properties of the as-deposited and the heat-treated WSU 150.
Condition | AD | HT @760 °C/4 h | |
---|---|---|---|
Name | Units | WSU150 | |
Young’ Modulus ‘E’ | GPa | 191.32 | 201.84 |
Yield Strength | MPa | 867 | 1113.84 |
Ultimate Tensile Strength ‘UTS’ | MPa | 1188 | 1396 |
Engineering Strain at UTS | % | 27.57 | 16.05 |
% Elongation | % | 27.9 | 16.1 |
Fracture Stress | MPa | 1164.04 | 1386.32 |
Fig. 9. (a) Tension test results of WSU 150 conducted in as-deposited and different heat-treated conditions, (b) Bar chart representing strength and ductility of various as-deposited and heat-treated conditions.
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