J. Mater. Sci. Technol. ›› 2021, Vol. 77: 117-125.DOI: 10.1016/j.jmst.2020.09.051
• Research Article • Previous Articles Next Articles
Wuyou Wanga, Xuewen Wanga,*(
), Lei Gana, Xinfei Jia, Zili Wub, Rongbin Zhanga,*()
Received:2020-08-31
Revised:2020-09-18
Accepted:2020-09-19
Published:2021-06-30
Online:2020-11-20
Contact:
Xuewen Wang,Rongbin Zhang
About author:rbzhang@ncu.edu.cn (R. Zhang).Wuyou Wang, Xuewen Wang, Lei Gan, Xinfei Ji, Zili Wu, Rongbin Zhang. All-solid-state Z-scheme BiVO4-Bi6O6(OH)3(NO3)3 heterostructure with prolonging electron-hole lifetime for enhanced photocatalytic hydrogen and oxygen evolution[J]. J. Mater. Sci. Technol., 2021, 77: 117-125.
Fig. 1. XRD patterns of the BiVO4-BBN-5 heterostructure, BiVO4, and BBN (a); SEM images of the BBN (b) and the BiVO4-BBN-5 heterostructure (c); scheme of growth process of the BiVO4-BBN developed by a one-pot hydrothermal method (d).
Fig. 2. TEM images of the BiVO4-BBN-5 heterostructure (a, b); HRTEM image of the BiVO4-BBN-5 heterostructure (c); TEM-EDX (d) and TEM-mapping (e-h) images of the BiVO4-BBN-5 heterostructure.
Fig. 3. UV-vis DRS (a), FT-IR spectra (b), Raman spectra (c), and local Raman spectra (d) of the BiVO4-BBN-5 heterostructure, BiVO4, and BBN.
Fig. 4. XPS spectra of (a) Bi 4f, (b) O 1s, (c) V 2p, and (d) N 1s in the BiVO4-BBN-5 heterostructure, BiVO4, and BBN.
Fig. 5. Hydrogen evolution for 4 h (a) over the BiVO4-BBN-5 heterostructure, BiVO4, and BBN; multiple circle of photocatalytic hydrogen evolution (b) of the BiVO4-BBN-5; oxygen average evolution rates for 4 h (c) over the BiVO4-BBN-5 heterostructure, BiVO4, and BBN; multiple circle of photocatalytic oxygen evolution (d) over the BiVO4-BBN-5; hydrogen (e) and oxygen (f) evolution for 4 h over the BiVO4-BBN heterostructure with different amounts of BBN and BiVO4.
Fig. 6. TG spectra (a) of BBN; XRD patterns and local XRD pattern of the BiVO4-BBN-5 heterostructure and the heterostructure treated at 590 °C for 3 h in air (b); hydrogen and oxygen evolutions (c) over the BiVO4-BBN-5 heterostructure and the heterostructure annealed at 590 °C for 3 h (BiVO4-BBN-5, A) in air.
Fig. 7. ESR signals of DMPO-?OH (a) and DMPO-?O2- radical adducts (b) over BiVO4-BBN-5 heterostructure, BiVO4, and BBN under UV-vis light irradiation for 10 min; scheme of the solid-state Z-scheme transfer pathway in the BiVO4-BBN heterostructure (c).
Fig. 8. Fluorescence spectra (a) and photocurrent response (b) over the BiVO4-BBN-5 heterostructure, BiVO4, and BBN; the time-resolved PL decay curves (c) and photoluminescence spectra in TA solution over the BiVO4-BBN-5 heterostructure, BiVO4, and BBN (d).
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