J. Mater. Sci. Technol. ›› 2022, Vol. 108: 173-185.DOI: 10.1016/j.jmst.2021.08.065
• Research Article • Previous Articles Next Articles
Lixia Maa, Min Wana, Weidong Lia,*(), Jie Shaob, Xiaoning Hanb, Jichun Zhangb
Received:
2021-05-25
Revised:
2021-08-21
Accepted:
2021-08-22
Published:
2021-10-30
Online:
2021-10-30
Contact:
Weidong Li
About author:
* E-mail address: space@buaa.edu.cn (W. Li).Lixia Ma, Min Wan, Weidong Li, Jie Shao, Xiaoning Han, Jichun Zhang. On the superplastic deformation mechanisms of near-α TNW700 titanium alloy[J]. J. Mater. Sci. Technol., 2022, 108: 173-185.
Fig. 2. SEM and EBSD analyses of the initial microstructure in as-received TNW700 alloy: (a) SEM image, (b) grain orientation map, (c) (0001) pole figure, (d) inverse pole figure.
Fig. 3. TNW700 alloy superplastic deformed at 925°C and different strain rates, (a) true stress and true strain curves, (b) effect of strain rates on elongation and peak stress, (c) specimens after superplastic, (d) strain rate sensitivity parameter.
Fig. 7. Elemental distribution in the fracture region of tensile specimen after deformation at 925°C and 0.001 s-1 obtained by EPMA, (a) corresponding SEM-BE image, elemental distribution maps (b) Ti, (c) Si, (d) Zr, (e) Al, (f) W, (h) Nb and (g) Sn.
Fig. 8. TEM characterization of α matrix and silicide in TNW700 alloy: (a) bright field image of silicide distribution; (b) magnified image of silicide at grain boundary; (c, d) SEAD pattern of primary α phase and silicide; (e) HRTEM image of silicide and primary α phase in frame Ⅰ; (f, g) The corresponding IFFT images of $\left( 20\bar{2}\bar{1} \right)$ and $\left( 11\bar{2}0 \right)$ fringes in frame Ⅱ and frame Ⅲ; (h) dislocation entanglements around silicide.
Fig. 10. EBSD IQ maps of TNW700 alloy deformed to tensile strain (a) 0.25, (b) 1.0, (c) 1.5 and (d) fracture at 925°C and 0.001 s-1 (For interpretation of the references to color in this figure, the reader is referred to the web version of this article.).
Fig. 12. The schematic diagram of β grains (a) nucleation and (e) growth. Nucleation at (b) triple junctions, (c) α grain interior and (d) α/α grain boundary (amplified image of the purple frame in Fig. 10(a). Growth at (f) triple junctions and (g) wedge into α grain interior; (h) β grains agglomeration (amplified image of the purple frame in Fig. 10(d)) (For interpretation of the references to color in this figure legend, the reader is referred to the web version of this article.).
Fig. 13. EBSD IPF maps of TNW700 alloy deformed to tensile strain (a) 0.25, (b) 1.0, (c) 1.5 and (d) fracture at 925°C and 0.001 s-1. Observation along ND was applied to IPF triangle (For interpretation of the references to color in this figure, the reader is referred to the web version of this article.).
Fig. 14. Inverse pole figures and (0001) pole figures of TNW700 alloy deformed to tensile strain (a) 0.25, (b) 1.0, (c) 1.5 and (d) fracture at 925°C and 0.001 s-1.
Fig. 16. KAM maps of TNW700 alloy deformed to tensile strain (a) 0.25, (b) 1.0, (c) 1.5 and (d) fracture at 925°C and 0.001 s-1 (For interpretation of the references to color in this figure, the reader is referred to the web version of this article.).
Fig. 17. Evolution schematic illustration of equiaxed primary α grains, LAGBs, MAGBs and HAGBs during superplastic deformation, (a) initial microstructure, (b) LAGBs generation, (c, d) LAGBs or MAGBs increase and transverse or longitudinal interfaces production, (e) HAGBs and DRX grains generation, (f) partial DRV grains and DRX grains.
Fig. 18. HRTEM bright-field micrographs of the tensile specimen deformed at 925°C and 0.001 s-1, (a) dislocation networks, (b) dislocation arrays and subgrain boundaries, (c) DRX grains (For interpretation of the references to color in this figure, the reader is referred to the web version of this article.).
Fig. 19. Schematics exhibiting five slip systems of α-Ti, (a) basal slip system, (b) prismatic <a> slip system (Pri <a>), (c) pyramidal <a> slip system (Pyr <a>), (d, e) 1st and 2nd pyramidal <c + a>slip system (Pyr-1 <c + a> and Pyr-2 <c + a>).
Fig. 20. Schematic diagrams of relationship between φ and the corresponding Schmid factor, (a) basal <a>, (b) Pri <a>, (c) Pyr-1 <c + a> and (d) Pyr-2 <c + a> (For interpretation of the references to color in this figure, the reader is referred to the web version of this article.).
Fig. 21. The Schmid factor maps of five slip modes of TNW700 alloy after tensile fracture: (a) basal <a>, (b) Pri <a>, (c) Pyr <a>, (d) Pyr-1 <c + a>, (e) Pyr-2 <c + a> and (f) the relative frequency of Schmid factor values (For interpretation of the references to color in this figure, the reader is referred to the web version of this article.).
Fig. 22. (a) The average Schmid factor values and (b) relative frequency with Schmid factor greater than 0.4 for five slip systems under different true strains.
[1] |
Z. Zhang, J. Fan, Z. Wu, D. Zhao, J. Li, J. Alloys Compd. 831 (2020) 154786.
DOI URL |
[2] |
Z. Liu, P. Li, L. Geng, T. Liu, H. gao, Mater. Sci. Eng. A 699 (2017) 71-80.
DOI URL |
[3] |
Y. Su, G. Hao, H. Fan, Y. Zhai, Y. Chen, J. Alloys Compd. 852 (2020) 156867.
DOI URL |
[4] |
C. Cai, X. Gao, Q. Teng, R. Kiran, J. Liu, Q. Wei, Y. Shi, Mater. Sci. Eng. A 802 (2021) 140426.
DOI URL |
[5] |
Z. Liu, P. Li, L. Xiong, T. Liu, L. He, Mater. Sci. Eng. A 680 (2017) 259-269.
DOI URL |
[6] |
C.J. Zhang, C.X. Guo, S.Z. Zhang, H. Feng, C.Y. Chen, H.Z. Zhang, P. Cao, Mater. Sci. Eng. A 771 (2020) 138569.
DOI URL |
[7] |
K. Yue, J. Liu, S. Zhu, L. Wang, Q. Wang, R. Yang, Materialia 1 (2018) 128-138.
DOI URL |
[8] |
C. Cheng, Z. Chen, H.E. Li, X. Wang, S. Zhu, Q. Wang, Mater. Sci. Eng. A 800 (2021) 140362.
DOI URL |
[9] |
R. Guo, B. Liu, R. Xu, Y. Cao, J. Qiu, F. Chen, Z. Yan, Y. Liu, Mater. Sci. Eng. A 777 (2020) 138993.
DOI URL |
[10] |
P. Lin, A. Feng, S. Yuan, G. Li, J. Shen, Mater. Sci. Eng. A 563 (2013) 16-20.
DOI URL |
[11] |
X. Zhang, L. Cao, Y. Zhao, Y. Chen, X. Tian, J. Deng, Mater. Sci. Eng. A 560 (2013) 700-704.
DOI URL |
[12] |
A.V. Mikhaylovskaya, A.O. Mosleh, A.D. Kotov, J.S. Kwame, T. Pourcelot, I. S. Golovin, V.K. Portnoy, Mater. Sci. Eng. A 708 (2017) 469-477.
DOI URL |
[13] |
T. Yasmeen, B. Zhao, J.H. Zheng, F. Tian, J. Lin, J. Jiang, Mater. Sci. Eng. A 788 (2020) 139482.
DOI URL |
[14] |
T. Yasmeen, Z. Shao, L. Zhao, P. Gao, J. Lin, J. Jiang, Int. J. Mech. Sci. 164 (2019) 105178.
DOI URL |
[15] |
P. Qiu, Y. Han, J. Le, G. Huang, L. Lei, L. Xiao, W. Lu, Mater. Charact. 167 (2020) 110458.
DOI URL |
[16] |
K. Shimagami, T. Ito, Y. Toda, A. Yumoto, Y. Yamabe-Mitarai, Mater. Sci. Eng. A 756 (2019) 46-53.
DOI URL |
[17] |
L. Ma, M. Wan, W. Li, J. Shao, X. Bai, J. Zhang, Mater. Sci. Eng. A 817 (2021) 141419.
DOI URL |
[18] |
E. Alabort, D. Barba, M.R. Shagiev, M.A. Murzinova, R.M. Galeyev, O.R. Valiakhmetov, A.F. Aletdinov, R.C. Reed, Acta Mater. 178 (2019) 275-287.
DOI |
[19] |
L. Ma, M. Wan, W. Li, J. Shao, X. Bai, J. Alloys Compd. 808 (2019) 151759.
DOI URL |
[20] |
K. Edalati, T. Masuda, M. Arita, M. Furui, X. Sauvage, Z. Horita, R.Z. Valiev, Sci. Rep. 7 (2017) 2662.
DOI PMID |
[21] |
P.M. Souza, P.D. Hodgson, B. Rolfe, R.P. Singh, H. Beladi, J. Alloys Compd. 793 (2019) 467-479.
DOI URL |
[22] |
W. Zhang, H. Ding, M. Cai, W. Yang, J. Li, Mater. Sci. Eng. A 727 (2018) 90-96.
DOI URL |
[23] |
E. Alabort, P. Kontis, D. Barba, K. Dragnevski, R.C. Reed, Acta Mater. 105 (2016) 449-463.
DOI URL |
[24] | J. Koike, Y. Shimoyama, T. Okamura, K. Maruyama, Mater. Sci. Forum 304-306 (1999) 183-188. |
[25] |
S. Roy, S. Suwas, Mater. Sci. Eng. A 574 (2013) 205-217.
DOI URL |
[26] |
W. Zhang, H. Liu, H. Ding, H. Fujii, Mater. Sci. Eng. A 785 (2020) 139390.
DOI URL |
[27] |
J.J. Jonas, C. Aranas, A. Fall, M. Jahazi, Mater. Des. 113 (2017) 305-310.
DOI URL |
[28] |
C. Aranas, A. Foul, B. Guo, A. Fall, M. Jahazi, J.J. Jonas, Scr. Mater. 133 (2017) 83-85.
DOI URL |
[29] |
S. Huang, J. Zhang, Y. Ma, S. Zhang, S.S. Youssef, M. Qi, H. Wang, J. Qiu, D. Xu, J. Lei, R. Yang, J. Alloys Compd. 791 (2019) 575-585.
DOI URL |
[30] |
Q. Xue, Y.J. Ma, J.F. Lei, R. Yang, C. Wang, J. Mater. Sci. Technol. 34 (2018) 2325-2330.
DOI |
[31] |
A. Madsen, E. Andrieu, H. Ghonem, Mater. Sci. Eng. A 171 (1993) 191-197.
DOI URL |
[32] |
C. Ramachandra, V. Singh, Metall. Mater. Trans. A 23 (1992) 689-690.
DOI URL |
[33] |
Z. Zheng, S. Xiao, X. Wang, Y. Guo, J. Yang, L. Xu, Y. Chen, Mater. Sci. Eng. A 803 (2021) 140487.
DOI URL |
[34] |
M.T. Whittaker, W. Harrison, P.J. Hurley, S. Williams, Mater. Sci. Eng. A 527 (2010) 4365-4372.
DOI URL |
[35] |
S. Jiang, L. Huang, Q. An, X. Gao, S. Wang, L. Geng, R. Zhang, F. Sun, Y. Jiao, J. Alloys Compd. 835 (2020) 155255.
DOI URL |
[36] |
W. Jia, W. Zeng, H. Yu, Mater. Des. 58 (2014) 108-115.
DOI URL |
[37] |
G. Seward, S. Celotto, D.J. Prior, J. Wheeler, R.C. Pond, Acta Mater. 52 (2004) 821-832.
DOI URL |
[38] |
A. Chaudhuri, A.N. Behera, A. Sarkar, R. Kapoor, R.K. Ray, S. Suwas, Acta Mater. 164 (2019) 153-164.
DOI |
[39] |
C. Yan, A. Feng, S. Qu, J.L. Sun, J. Shen, Mater. Sci. Eng. A 731 (2018) 266-277.
DOI URL |
[40] |
K. Huang, R.E. Logé, Mater. Des. 111 (2016) 548-574.
DOI URL |
[41] |
S. Gourdet, F. Montheillet, Mater. Sci. Eng. A 283 (20 0 0) 274-288.
DOI URL |
[42] |
J. Shen, Y. Sun, Y. Ning, H. Yu, Z. Yao, L. Hu, Mater. Charact. 153 (2019) 304-317.
DOI URL |
[43] |
D. Zhou, W. Zeng, J. Xu, S. Wang, W. Chen, Mater. Charact. 151 (2019) 103-111.
DOI URL |
[44] |
J.S. Kim, J.H. Kim, Y.T. Lee, C.G. Park, C.S. Lee, Mater. Sci. Eng. A 263 (1999) 272-280.
DOI URL |
[45] |
Q. Zhao, F. Yang, R. Torrens, L. Bolzoni, Mater. Des. 169 (2019) 107682.
DOI URL |
[46] |
W. Ma, S. Liu, X. Zhang, B. Chen, F. Wang, X. Zhang, M. Ma, R. Liu, Mater. Sci. Eng. A 792 (2020) 139812.
DOI URL |
[47] |
F. Wagner, N. Bozzolo, O. Van Landuyt, T. Grosdidier, Acta Mater. 50 (2002) 1245-1259.
DOI URL |
[48] |
X.Z. Ma, Z.L. Xiang, M.Z. Ma, C. Tan, Z.A. Yang, G.L. Shen, Z.Y. Chen, Q. Shu, Mater. Sci. Eng. A 772 (2020) 138749.
DOI URL |
[49] |
G. Liu, K. Wang, B. He, M. Huang, S. Yuan, Mater. Des. 86 (2015) 146-151.
DOI URL |
[50] |
H. Li, D.E. Mason, T.R. Bieler, C.J. Boehlert, M.A. Crimp, Acta Mater. 61 (2013) 7555-7567.
DOI URL |
[51] |
V. Wan, M.A. Cuddihy, J. Jiang, D.W. Maclachlan, F. Dunne, Acta Mater. 115 (2016) 45-57.
DOI URL |
[52] |
J. Zhao, L. Lv, K. Wang, G. Liu, J. Mater. Sci. Technol. 38 (2020) 125-134.
DOI |
[53] |
M.H. Yoo, Metall. Trans. A 12 (1981) 409-418.
DOI URL |
[54] |
S. Zaefferer, Mater. Sci. Eng. A 344 (2003) 20-30.
DOI URL |
[55] |
Y. Sun, C. Zhang, H. Feng, S. Zhang, J. Han, W. Zhang, E. Zhao, H. Wang, Mater. Charact. 163 (2020) 110281.
DOI URL |
[56] |
F. Bridier, P. Villechaise, J. Mendez, Acta Mater. 53 (2005) 555-567.
DOI URL |
[1] | MengCheng Deng, Shang Sui, Bo Yao, Liang Ma, Xin Lin, Jing Chen. Microstructure and room-temperature tensile property of Ti-5.7Al-4.0Sn-3.5Zr-0.4Mo-0.4Si-0.4Nb-1.0Ta-0.05C with near equiaxed β grain fabricated by laser directed energy deposition technique [J]. J. Mater. Sci. Technol., 2022, 101(0): 308-320. |
[2] | Yijing Wang, Enkang Hao, Xiaoqin Zhao, Yun Xue, Yulong An, Huidi Zhou. Effect of microstructure evolution of Ti6Al4V alloy on its cavitation erosion and corrosion resistance in artificial seawater [J]. J. Mater. Sci. Technol., 2022, 100(0): 169-181. |
[3] | Zhiyuan Liu, Dandan Zhao, Pei Wang, Ming Yan, Can Yang, Zhangwei Chen, Jian Lu, Zhaoping Lu. Additive manufacturing of metals: Microstructure evolution and multistage control [J]. J. Mater. Sci. Technol., 2022, 100(0): 224-236. |
[4] | Bijin Zhou, Leyun Wang, Jinhui Wang, Alireza Maldar, Gaoming Zhu, Hailong Jia, Peipeng Jin, Xiaoqin Zeng, Yanjun Li. Dislocation behavior in a polycrystalline Mg-Y alloy using multi-scale characterization and VPSC simulation [J]. J. Mater. Sci. Technol., 2022, 98(0): 87-98. |
[5] | Hao Guo, Shufeng Yang, Tiantian Wang, Hang Yuan, Yanling Zhang, Jingshe Li. Microstructure evolution and acicular ferrite nucleation in inclusion-engineered steel with modified MgO@C nanoparticle addition [J]. J. Mater. Sci. Technol., 2022, 99(0): 277-287. |
[6] | Jinshuo Zhang, Guohua Wu, Liang Zhang, Xiaolong Zhang, Chunchang Shi, Xin Tong. Addressing the strength-ductility trade-off in a cast Al-Li-Cu alloy—Synergistic effect of Sc-alloying and optimized artificial ageing scheme [J]. J. Mater. Sci. Technol., 2022, 96(0): 212-225. |
[7] | Zhaoxin Du, Qiwei He, Ruirun Chen, Fei Liu, Jingyong Zhang, Fei Yang, Xueping Zhao, Xiaoming Cui, Jun Cheng. Rolling reduction -dependent deformation mechanisms and tensile properties in a β titanium alloy [J]. J. Mater. Sci. Technol., 2022, 104(0): 183-193. |
[8] | Yang Bao, Lujun Huang, Shan Jiang, Rui Zhang, Qi An, Caiwei Zhang, Lin Geng, Xinxin Ma. A novel Ti cored wire developed for wire-feed arc deposition of TiB/Ti composite coating [J]. J. Mater. Sci. Technol., 2021, 83(0): 145-160. |
[9] | Dan Liu, Daoxin Liu, Junfeng Cui, Xingchen Xu, Kaifa Fan, Amin Ma, Yuting He, Sara Bagherifard. Deformation mechanism and in-situ TEM compression behavior of TB8 β titanium alloy with gradient structure [J]. J. Mater. Sci. Technol., 2021, 84(0): 105-115. |
[10] | Qingqing Li, Yong Zhang, Jie Chen, Bugao Guo, Weicheng Wang, Yuhai Jing, Yong Liu. Effect of ultrasonic micro-forging treatment on microstructure and mechanical properties of GH3039 superalloy processed by directed energy deposition [J]. J. Mater. Sci. Technol., 2021, 70(0): 185-196. |
[11] | Enkang Hao, Yulong An, Jie Chen, Xiaoqin Zhao, Guoliang Hou, Jianmin Chen, Meizhen Gao, Fengyuan Yan. In-situ formation of layer-like Ag2MoO4 induced by high-temperature oxidation and its effect on the self-lubricating properties of NiCoCrAlYTa/Ag/Mo coatings [J]. J. Mater. Sci. Technol., 2021, 75(0): 164-173. |
[12] | Jie Wang, Gaoming Zhu, Leyun Wang, Evgenii Vasilev, Jun-Sang Park, Gang Sha, Xiaoqin Zeng, Marko Knezevic. Origins of high ductility exhibited by an extruded magnesium alloy Mg-1.8Zn-0.2Ca: Experiments and crystal plasticity modeling [J]. J. Mater. Sci. Technol., 2021, 84(0): 27-42. |
[13] | Xin Zhong, Tao Zhu, Yaran Niu, Haijun Zhou, Le Zhang, Xiangyu Zhang, Qilian Li, Xuebin Zheng. Effect of microstructure evolution and crystal structure on thermal properties for plasma-sprayed RE2SiO5 (RE = Gd, Y, Er) environmental barrier coatings [J]. J. Mater. Sci. Technol., 2021, 85(0): 141-151. |
[14] | Yunsheng Wu, Xuezhi Qin, Changshuai Wang, Lanzhang Zhou. Microstructural evolution and its influence on the impact toughness of GH984G alloy during long-term thermal exposure [J]. J. Mater. Sci. Technol., 2021, 60(0): 61-69. |
[15] | Lin Yuan, Jiangtao Xiong, Yajie Du, Jin Ren, Junmiao Shi, Jinglong Li. Microstructure and mechanical properties in the TLP joint of FeCoNiTiAl and Inconel 718 alloys using BNi2 filler [J]. J. Mater. Sci. Technol., 2021, 61(0): 176-185. |
Viewed | ||||||
Full text |
|
|||||
Abstract |
|
|||||