J. Mater. Sci. Technol. ›› 2022, Vol. 108: 102-109.DOI: 10.1016/j.jmst.2021.08.026
• Research Article • Previous Articles Next Articles
P. Wang, X. Liu, H. Wang, J. Cao, J. Qi(), J. Feng
Received:
2021-06-02
Revised:
2021-07-29
Accepted:
2021-08-04
Published:
2021-10-08
Online:
2021-10-08
Contact:
J. Qi
About author:
* E-mail addresses: jlqi@hit.edu.cn (J. Qi).P. Wang, X. Liu, H. Wang, J. Cao, J. Qi, J. Feng. Releasing the residual stress of Cf/SiC-GH3536 joint by designing an Ag-Cu-Ti + Sc2(WO4)3 composite filler metal[J]. J. Mater. Sci. Technol., 2022, 108: 102-109.
Fig. 3. (a) SEM image of Cf/SiC-GH3536 joint, (b, c) the corresponding magnification image in (a), and (d) the corresponding elements mapping results.
Point | Ag | Cu | Ti | C | Si | Ni | Cr | Fe |
---|---|---|---|---|---|---|---|---|
A | - | - | 40.4 | 47.9 | 11.7 | - | - | - |
B | 3.1 | 95.1 | 1.8 | - | - | - | - | - |
C | 88.8 | 10.0 | 1.2 | - | - | - | - | - |
D | 12.4 | 33.5 | 25.6 | - | 10.1 | 10.9 | - | 7.5 |
E | 1.5 | 3.4 | 20.2 | - | - | 42.1 | 19.0 | 13.8 |
F | 48.6 | 2.9 | 0.7 | - | - | 7.8 | 24.5 | 15.5 |
Table 1. Element composition of the points marked at Fig. 3 (at.%).
Point | Ag | Cu | Ti | C | Si | Ni | Cr | Fe |
---|---|---|---|---|---|---|---|---|
A | - | - | 40.4 | 47.9 | 11.7 | - | - | - |
B | 3.1 | 95.1 | 1.8 | - | - | - | - | - |
C | 88.8 | 10.0 | 1.2 | - | - | - | - | - |
D | 12.4 | 33.5 | 25.6 | - | 10.1 | 10.9 | - | 7.5 |
E | 1.5 | 3.4 | 20.2 | - | - | 42.1 | 19.0 | 13.8 |
F | 48.6 | 2.9 | 0.7 | - | - | 7.8 | 24.5 | 15.5 |
Fig. 4. XRD results of (a) interface phase compositions and (b) brazing metal of Cf/SiC-GH3536 joints brazed by AgCuTi, and (c) Gibbs formation energy of (1), (2), (3).
Fig. 5. (a) SEM image of Cf/SiC-GH3536 joint brazed by Ag-Cu-Ti-6, (b-d) The corresponding magnification images in (a), and (e) the corresponding element mapping results.
Point | Ag | Cu | Ti | C | Si | Ni | Cr | Fe | Sc | W | O |
---|---|---|---|---|---|---|---|---|---|---|---|
A | - | - | 40.6 | 21.0 | 33.9 | 1.1 | 1.8 | 1.6 | - | - | - |
B | - | - | 42.7 | 51.1 | 1.8 | 1.0 | 2.0 | 1.4 | - | - | - |
C | 15.3 | 75.7 | 2.2 | - | - | 2.5 | 1.8 | 2.5 | - | - | - |
D | 76.0 | 8.9 | 7.5 | - | - | 3.3 | 1.9 | 2.4 | - | - | - |
E | 6.5 | 35.8 | 23.3 | - | - | 22.7 | 7.7 | 4.0 | - | - | - |
F | 3.2 | 8.6 | 28.5 | - | - | 43.0 | 12.6 | 4.1 | - | - | - |
G | - | - | - | - | - | - | - | - | 23.0 | 28.3 | 48.7 |
H | - | - | 56.3 | - | - | 1.7 | 0.5 | 1.9 | 2.2 | 2.3 | 35.1 |
Table 2. Element composition of these points marked at Fig. 4 (at.%).
Point | Ag | Cu | Ti | C | Si | Ni | Cr | Fe | Sc | W | O |
---|---|---|---|---|---|---|---|---|---|---|---|
A | - | - | 40.6 | 21.0 | 33.9 | 1.1 | 1.8 | 1.6 | - | - | - |
B | - | - | 42.7 | 51.1 | 1.8 | 1.0 | 2.0 | 1.4 | - | - | - |
C | 15.3 | 75.7 | 2.2 | - | - | 2.5 | 1.8 | 2.5 | - | - | - |
D | 76.0 | 8.9 | 7.5 | - | - | 3.3 | 1.9 | 2.4 | - | - | - |
E | 6.5 | 35.8 | 23.3 | - | - | 22.7 | 7.7 | 4.0 | - | - | - |
F | 3.2 | 8.6 | 28.5 | - | - | 43.0 | 12.6 | 4.1 | - | - | - |
G | - | - | - | - | - | - | - | - | 23.0 | 28.3 | 48.7 |
H | - | - | 56.3 | - | - | 1.7 | 0.5 | 1.9 | 2.2 | 2.3 | 35.1 |
Fig. 8. Simulation results of residual stress in the Cf/SiC-GH3536 joints. (a, b) Mises stress distribution on the cross-section of the joints brazed by Ag-Cu-Ti and Ag-Cu-Ti-6, (c) Mises-stress distribution curves along the selected lines marked in (a, b), (d, e) X-stress distribution on the cross-section of the joints brazed by Ag-Cu-Ti and Ag-Cu-Ti-6, and (f) X-stress distribution curves along the selected lines marked in (d, e).
Materials | Density (g cm-3) | Poisson's ratio | Temperature (°C) | Elastic modulus (GPa) | CTE ( × 10-6 K-1) | Yield stress (MPa) |
---|---|---|---|---|---|---|
Ag-Cu-Ti | 9.76 | 0.363 | 20 | 111 | 16.7 | 230 |
200 | 90 | 17.2 | 170 | |||
400 | 80 | 17.8 | 98 | |||
600 | 67 | 19.4 | 25 | |||
800 | 58 | 20.5 | 20 | |||
GH3536 | 8.3 | 0.33 | 20 | 206 | 12.1 | - |
Sc2(WO4)3 | 4.46 | 0.19 | - | 57.7 | -5.6 | - |
Cf/SiC | 3 | 0.32 | - | 122 | 3 | - |
Table 3. Physical and mechanical properties of used materials [[21], [22], [23]].
Materials | Density (g cm-3) | Poisson's ratio | Temperature (°C) | Elastic modulus (GPa) | CTE ( × 10-6 K-1) | Yield stress (MPa) |
---|---|---|---|---|---|---|
Ag-Cu-Ti | 9.76 | 0.363 | 20 | 111 | 16.7 | 230 |
200 | 90 | 17.2 | 170 | |||
400 | 80 | 17.8 | 98 | |||
600 | 67 | 19.4 | 25 | |||
800 | 58 | 20.5 | 20 | |||
GH3536 | 8.3 | 0.33 | 20 | 206 | 12.1 | - |
Sc2(WO4)3 | 4.46 | 0.19 | - | 57.7 | -5.6 | - |
Cf/SiC | 3 | 0.32 | - | 122 | 3 | - |
Fig. 10. (a-e) Different magnification images of the fracture morphologies and (f) corresponding shear strengths of Cf/SiC-GH3536 joints brazed by Ag-Cu-Ti-x.
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