J. Mater. Sci. Technol. ›› 2022, Vol. 110: 117-127.DOI: 10.1016/j.jmst.2021.08.025

• Research Article • Previous Articles     Next Articles

Microstructure and mechanical properties of directionally solidified Al-rich Ni3Al-based alloy under static magnetic field

Xin Liu, Sansan Shuai(), Chenglin Huang, Shijun Wu, Tao Hu, Chaoyue Chen, Jiang Wang(), Zhongming Ren()   

  1. State Key Laboratory of Advanced Special Steels, School of Materials Science and Engineering, Shanghai University, Shanghai 200444, China

Abstract:

The influence of a longitudinal static magnetic field on microstructures and mechanical properties of Ni3Al-based alloy during directional solidification at the growth speed of 25 µm/s and 100 µm/s has been experimentally investigated. Results reflected that the utilization of a 0.5 T magnetic field refines the NiAl dendrites at both speeds of growth. When applying a high magnetic field, the columnar-to-equiaxed transition (CET) occurred at growth speed of 25 µm/s and dendrite networks formed at growth speed of 100 µm/s. Tensile property results indicated that the refinement of dendrites enhanced both plasticity and ultimate tensile strength of Ni-Al alloy. The change of microstructures and mechanical properties should be attributed to the combined action of the thermoelectric magnetic convection (TEMC) in mushy zone together with the thermoelectric magnetic force (TEMF) acting on the solid. When applying a low magnetic field (0.5 T), the TEMF is too small to fragment the dendrites, and the refined dendrites is mainly due to the TEMC in the interdendritic regions. At a lower growth speed, the TEMF is supposed to strong enough to fragment the dendrites and induce the occurrence of CET under 2 or 4 T. When the growth speed increased to 100 µm/s, no obvious CET was observed, but a vertical secondary convection is induced by the circulation in the parallel plane, which promotes the growth of secondary and tertiary branches, leading to the formation of abnormally developed high order dendrites. The hierarchical dendritic structure was suggested to provide a channel for rapid crack propagation and thus degraded the mechanical properties.

Key words: Ni3Al-based alloy, Magnetic field, Directional solidification, Columnar to equiaxed transition, Mechanical properties