J. Mater. Sci. Technol. ›› 2022, Vol. 106: 70-76.DOI: 10.1016/j.jmst.2021.06.078
• Research Article • Previous Articles Next Articles
Xianglong Zhoua, Tao Yuana,b, Tianyu Maa,*()
Received:
2021-04-10
Revised:
2021-06-01
Accepted:
2021-06-17
Published:
2022-04-20
Online:
2021-09-22
Contact:
Tianyu Ma
About author:
*E-mail address: matianyu@xjtu.edu.cn (T. Ma).Xianglong Zhou, Tao Yuan, Tianyu Ma. Shortened processing duration of high-performance Sm-Co-Fe-Cu-Zr magnets by stress-aging[J]. J. Mater. Sci. Technol., 2022, 106: 70-76.
Magnet | Aging condition | (BH)max(MGOe) | Hcj(kOe) | Br(kG) | Hk(kOe) | Hk/Hcj(%) | FWHM(204)(°) |
---|---|---|---|---|---|---|---|
A | 10 h@90 MPa | 30.02 | 35.62 | 11.40 | 28.57 | 80.21 | 0.227 |
B | 10 h@0 MPa | 29.44 | 28.46 | 11.40 | 14.38 | 50.53 | 0.335 |
C | 20 h@0 MPa | 30.19 | 35.14 | 11.37 | 26.50 | 75.41 | 0.239 |
D | 15 h@50 MPa | 29.26 | 35.64 | 11.38 | 26.89 | 75.45 | 0.235 |
Table 1. Aging condition, magnetic properties and structural parameters of the present magnets.
Magnet | Aging condition | (BH)max(MGOe) | Hcj(kOe) | Br(kG) | Hk(kOe) | Hk/Hcj(%) | FWHM(204)(°) |
---|---|---|---|---|---|---|---|
A | 10 h@90 MPa | 30.02 | 35.62 | 11.40 | 28.57 | 80.21 | 0.227 |
B | 10 h@0 MPa | 29.44 | 28.46 | 11.40 | 14.38 | 50.53 | 0.335 |
C | 20 h@0 MPa | 30.19 | 35.14 | 11.37 | 26.50 | 75.41 | 0.239 |
D | 15 h@50 MPa | 29.26 | 35.64 | 11.38 | 26.89 | 75.45 | 0.235 |
Fig. 1. Heat-treatment procedure, initial magnetization curves and magnetization hysteresis loops of the Sm25Co50.2Fe16.2Cu5.6Zr3.0 (wt.%) magnets. Aged for 10 h under 90 MPa (magnet A) and stress-free condition (magnet B) (a, b), aged for 20 h (magnet C) under stress-free condition (c, d). The inset in Fig. 1(a) schematically shows the application of external stress using Mo pressing dies and the utilization of BN powders to avoid possible bonding between magnets and Mo dies.
Fig. 4. HR-TEM images for stress-aged magnet A (a1) and isothermally-aged magnet B (b1). Enlarged view of 1:5H/2:17R phase interface (a2) and [210] projection of 1:5H phase (a3). FFT patterns of 2:17R’ phase (b2) and 2:17R phase (b3).
Fig. 7. Bright-field TEM images, SAED patterns and intensity profiles for the 0.5 h-aged sample under 50 MPa (a-c) and for the 0.5 h-aged sample under stress-free condition (d-f).
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