J. Mater. Sci. Technol. ›› 2021, Vol. 92: 214-224.DOI: 10.1016/j.jmst.2021.04.005
• Research Article • Previous Articles Next Articles
Yiming Jina,b,*(
), Carsten Blawertc, Hong Yangd,e,*(), Björn Wiesea, Jan Bohlenc, Di Meic, Min Dengc, Frank Feyerabenda, Regine Willumeita,f
Received:2020-07-24
Revised:2021-04-11
Accepted:2021-04-13
Published:2021-11-30
Online:2021-05-09
Contact:
Yiming Jin,Hong Yang
About author:hong.yang@cqu.edu.cn (H. Yang).Yiming Jin, Carsten Blawert, Hong Yang, Björn Wiese, Jan Bohlen, Di Mei, Min Deng, Frank Feyerabend, Regine Willumeit. Deteriorated corrosion performance of micro-alloyed Mg-Zn alloy after heat treatment and mechanical processing[J]. J. Mater. Sci. Technol., 2021, 92: 214-224.
| Alloy (wt.%) | T4 heat treatment | Corrosion rate | Ref. |
|---|---|---|---|
| as-extruded Mg-5Zn | 450 °C / 2 h, quenching | WL (g/m2/h) and icorr (μA/cm2) in 3.5% NaCl solution T4 (2.6; 23) < as-extruded (3.2; 26) | [ |
| as-cast Mg-5Zn | 300 °C / 6 h + 500 °C / 42 h, quenching | WL (mm/year), icorr (μA/cm2) and H2 (mm/year) in 3.5% NaCl solution saturated with Mg(OH)2 T4 (6.5; 117; 5.7) < as-cast (15.2; 340; 18.8) | [ |
| as-cast Mg-(3, 6)Zn | 340 °C / 6, 12, 18 h, hot water quenching | WL (mm/year) and icorr (μA/cm2) in Kokubo solution As-cast: Mg-3 Zn > Mg-6 Zn Mg-3 Zn T4 (1.9; 210-224) ≈ as-cast (2.0; 228) Mg-6 Zn T4 (1.4; 191-205) < as-cast (3.5; 270) | [ |
| as-cast Mg-3Zn | 320 °C / 10 h, hot water quenching | H2 (mL/cm2) and icorr (μA/cm2) in 0.1 mol/L NaCl solution T4 (2.4; 16) < as-cast (3.0; 24) | [ |
| Sintered and then extruded Mg-(6, 14.5, 25.3, 40.3)Zn | 450 °C / 12 h, quenching | H2 (mL/cm2) and icorr (μA/cm2) in Ringer's solution as-extruded (8; 15.9) < T4 (34; 19.9) | [ |
| as-cast Mg-6Zn | 350 °C / 6, 12, 18, 24, 48 h, quenching | WL (mm/a) and icorr (μA/cm2) in SBF with TRIS 48 h (14.1; 180) < 24 h (14.9; 230) < 18 h (18.3; 360) < 12 h (21.4; 390) < 6 h(23.1; 630) < as-cast (35.9; 810) | [ |
| as-extruded Mg-6Zn | 320 °C / 8, 16, 24 h, quenching | H2 (mL/cm2) in 0.9% NaCl solution T4 (6) < as-extruded (17) | [ |
| as-extruded Mg-6Zn | 350 °C / 2 h | icorr (μA/cm2) in SBF T4 (3.5) < as-extruded (8.0) | [ |
Table 1 Literature review on the effect of heat treatment on the corrosion performance of binary Mg-Zn systems. WL: weight loss, H2: hydrogen evolution, icorr: corrosion current density from potentiodynamic polarisation test.
| Alloy (wt.%) | T4 heat treatment | Corrosion rate | Ref. |
|---|---|---|---|
| as-extruded Mg-5Zn | 450 °C / 2 h, quenching | WL (g/m2/h) and icorr (μA/cm2) in 3.5% NaCl solution T4 (2.6; 23) < as-extruded (3.2; 26) | [ |
| as-cast Mg-5Zn | 300 °C / 6 h + 500 °C / 42 h, quenching | WL (mm/year), icorr (μA/cm2) and H2 (mm/year) in 3.5% NaCl solution saturated with Mg(OH)2 T4 (6.5; 117; 5.7) < as-cast (15.2; 340; 18.8) | [ |
| as-cast Mg-(3, 6)Zn | 340 °C / 6, 12, 18 h, hot water quenching | WL (mm/year) and icorr (μA/cm2) in Kokubo solution As-cast: Mg-3 Zn > Mg-6 Zn Mg-3 Zn T4 (1.9; 210-224) ≈ as-cast (2.0; 228) Mg-6 Zn T4 (1.4; 191-205) < as-cast (3.5; 270) | [ |
| as-cast Mg-3Zn | 320 °C / 10 h, hot water quenching | H2 (mL/cm2) and icorr (μA/cm2) in 0.1 mol/L NaCl solution T4 (2.4; 16) < as-cast (3.0; 24) | [ |
| Sintered and then extruded Mg-(6, 14.5, 25.3, 40.3)Zn | 450 °C / 12 h, quenching | H2 (mL/cm2) and icorr (μA/cm2) in Ringer's solution as-extruded (8; 15.9) < T4 (34; 19.9) | [ |
| as-cast Mg-6Zn | 350 °C / 6, 12, 18, 24, 48 h, quenching | WL (mm/a) and icorr (μA/cm2) in SBF with TRIS 48 h (14.1; 180) < 24 h (14.9; 230) < 18 h (18.3; 360) < 12 h (21.4; 390) < 6 h(23.1; 630) < as-cast (35.9; 810) | [ |
| as-extruded Mg-6Zn | 320 °C / 8, 16, 24 h, quenching | H2 (mL/cm2) in 0.9% NaCl solution T4 (6) < as-extruded (17) | [ |
| as-extruded Mg-6Zn | 350 °C / 2 h | icorr (μA/cm2) in SBF T4 (3.5) < as-extruded (8.0) | [ |
| Mg-0.5Zn | Term |
| as-cast | as-cast |
| solution-treated 2 h | HT-2 h |
| solution-treated 16 h | HT-16 h |
| as-cast and then extruded | as cast-extruded |
| solution-treated 16 h and then extruded | HT16 h-extruded |
Table 2 Terminology used to describe the different treated Mg-0.5 Zn alloy in this work.
| Mg-0.5Zn | Term |
| as-cast | as-cast |
| solution-treated 2 h | HT-2 h |
| solution-treated 16 h | HT-16 h |
| as-cast and then extruded | as cast-extruded |
| solution-treated 16 h and then extruded | HT16 h-extruded |
| Composition (wt.%) | ||||
|---|---|---|---|---|
| Zn | Mn | Si | Al | Ca |
| 0.49 ± 0.02 0.49 ± 0.02 | 0.0177 ± 0.0005 0.0169 ± 0.0005 | 0.0076 ± 0.0004 0.0067 ± 0.0004 | 0.0047 ± 0.0005 0.0032 ± 0.0005 | 0.0019 ± 0.0005 0.0019 ± 0.0005 |
| Fe | Cu | Ni | Be | Mg |
| 0.0014 ± 0.0006 0.0013 ± 0.0006 | < 0.0003 < 0.0003 | < 0.0003 < 0.0003 | < 0.0003 < 0.0003 | Bal. Bal. |
Table 3 Chemical compositions of the as-cast and as-extruded Mg-0.5 Zn alloy determined by ICP-OES.
| Composition (wt.%) | ||||
|---|---|---|---|---|
| Zn | Mn | Si | Al | Ca |
| 0.49 ± 0.02 0.49 ± 0.02 | 0.0177 ± 0.0005 0.0169 ± 0.0005 | 0.0076 ± 0.0004 0.0067 ± 0.0004 | 0.0047 ± 0.0005 0.0032 ± 0.0005 | 0.0019 ± 0.0005 0.0019 ± 0.0005 |
| Fe | Cu | Ni | Be | Mg |
| 0.0014 ± 0.0006 0.0013 ± 0.0006 | < 0.0003 < 0.0003 | < 0.0003 < 0.0003 | < 0.0003 < 0.0003 | Bal. Bal. |
Fig. 1. (a-c) OM images of as-cast, HT-2 h and HT-16 h Mg-0.5 Zn; BSE SEM images and EDS element mappings of the (d) as-cast and (e) HT-16 h samples.
Fig. 2. BSE SEM images of the precipitates in (a) as-cast, (b) HT-2 h and (c) HT-16 h Mg-0.5 Zn samples; (a1-c1) (a2-c2) corresponding compositions of the precipitates and the matrix indicated by EDS.
Fig. 3. Fe and Si concentrations of the particles found in the (a) as-cast, (b) HT-2 h and (c) HT-16 h Mg-0.5 Zn samples.
Fig. 4. Corrosion morphologies of (a-f) as-cast, (e-h) HT-2 h and (i-l) HT-16 h Mg-0.5 Zn samples after immersion for 5 min, 0.5 h, 2 h and 6 h, respectively.
Fig. 5. Corrosion morphologies of the (a) as-cast and (b-c) HT-16 h Mg-0.5 Zn samples after immersion for 2 min; (a1-c1) the corresponding particle compositions indicated by EDS.
Fig. 6. Corrosion morphologies and EDS element mapping of (a) as-cast and (b) HT-16 h Mg-0.5 Zn samples after immersion for 5 min.
Fig. 7. (a) PDP curves of as-cast, HT-2 h and HT-16 h Mg-0.5 Zn samples; (b) corresponding corrosion potential and corrosion current density.
Fig. 8. EIS Nyquist plots of the (a) as-cast, (b) HT-2 h and (c) HT-16 h Mg-0.5 Zn samples.
Fig. 9. BSE-SEM images of the characteristic corrosion morphologies of (a) as-cast, (b) HT-2 h and (c) HT-16 h samples after 3 days immersion. Images a1 and a2 are the zoomed-in areas of image a.
Fig. 10. OM images of (a) as cast-extruded and (b) HT16 h-extruded Mg-0.5 Zn samples.
Fig. 11. EIS Nyquist plots of (a) as cast-extruded and (b) HT16 h-extruded Mg-0.5 Zn samples; (a1-b1) corresponding corrosion morphologies after 72 h immersion.
Fig. 12. Thermodynamic calculation of the formation enthalpies of Mg-Zn, Mg-Si, Mg-Fe, Zn-Si, Zn-Fe, Si-Fe binary systems (A-B binary systems).
Fig. 13. (a) Calculated phase diagrams of Mg0.5Zn-Fe system via Pandat; (b1-b5) schematics of the microstructure and Fe particles change during solidification and solution treatment. The red line in (a) represents the exact Fe content in the system (14 ppm). The red dots in (b) stand for the Fe particles and the bigger and darker dots depict the Fe particles are getting bigger and more concentrated during heat treatment.
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