J. Mater. Sci. Technol. ›› 2021, Vol. 87: 39-45.DOI: 10.1016/j.jmst.2021.01.052
• Research Article • Previous Articles Next Articles
Xiong Yanga, Daquan Liub, Jianbo Lia, Ruonan Mina, Huijun Kanga,c,*(
), Linwei Lia, Zongning Chena,c, Enyu Guoa,c, Tongmin Wanga,c,*()
Received:2020-12-17
Revised:2021-01-23
Accepted:2021-01-28
Published:2021-10-10
Online:2021-03-17
Contact:
Huijun Kang,Tongmin Wang
About author:tmwang@dlut.edu.cn (T. Wang).Xiong Yang, Daquan Liu, Jianbo Li, Ruonan Min, Huijun Kang, Linwei Li, Zongning Chen, Enyu Guo, Tongmin Wang. Top-down method to fabricate TiNi1+xSn half-Heusler alloy with high thermoelectric performance[J]. J. Mater. Sci. Technol., 2021, 87: 39-45.
Fig. 1. Schematics of the steps involved in the conventional preparation method and the top-down method.
Fig. 2. SEM images of the average grain sizes in TiNi2Sn powders at different ball-milling periods: (a) 30 min, (b) 5 h, and (c) 20 h. (d) Room temperature powder X-ray diffraction patterns for the TiNiSn-based HH samples.
Fig. 3. EPMA images, elemental mappings and chemical compositions of as-sintered TiNi1.05Sn samples: (a) TiNi1.05Sn-S10, (b) TiNi1.05Sn-CPP.
Fig. 4. (a) Secondary electron (SE) image of the TiNi1.05Sn-S10 alloy. The inset shows the sampling position of the focused ion beam (FIB). (b) STEM-EDS chemical maps displaying the spatial distribution of Ti, Ni, Sn for the grain interfaces of TiNi1.05Sn-S10. (c) HAADF-STEM image of the interface between TiNiSn and TiNi2Sn, with electron diffraction patterns insets from the TiNiSn and TiNi2Sn phases. (d) Inverse fast-Fourier transform image obtained from Fig. 4(c).
Fig. 5. Thermoelectric properties of the TiNi1.05Sn HH samples: (a) total thermal conductivity, (b) lattice thermal conductivity.
Fig. 6. Temperature dependence of thermoelectric properties of the TiNi1.05Sn HH samples: (a) carrier mobility, (b) carrier concentration, (c) electrical conductivity, (d) Seebeck coefficient, (e) power factor, and (f) figure of merit (ZT).
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