J. Mater. Sci. Technol. ›› 2022, Vol. 111: 152-166.DOI: 10.1016/j.jmst.2021.08.038
• Research Article • Previous Articles Next Articles
Received:2021-06-20
Revised:2021-08-29
Accepted:2021-08-29
Published:2022-06-10
Online:2021-12-01
Contact:
W.J. Kim
About author:* E-mail address: kimwj@wow.hongik.ac.kr (W.J. Kim).H.T. Jeong, W.J. Kim. Effect of roll speed ratio on the texture and microstructural evolution of an FCC high-entropy alloy during differential speed rolling[J]. J. Mater. Sci. Technol., 2022, 111: 152-166.
| Texture type | Texture component | Miller indices | Symbol |
|---|---|---|---|
| Recrystallization | Cube | {100}〈100〉 | ■ (sky blue) |
| Goss | {110}〈100〉 | ● (sky blue) | |
| P | {110}〈122〉 | ▲ (sky blue) | |
| Rolling | Brass | {110}〈112〉 | ■ (pink) |
| Copper | {112}〈111〉 | ● (pink) | |
| S | {123}〈634〉 | ▲ (pink) | |
| Shear | Shear1 | {100}〈110〉 | ■ (gray) |
| Shear2 | {111}〈112〉 | ● (gray) | |
| Shear3 | {111}〈110〉 | ▲ (gray) | |
| Shear4 | {112}〈110〉 | ▼ (gray) |
Table 1. Recrystallization, rolling, and shear texture components considered in this study.
| Texture type | Texture component | Miller indices | Symbol |
|---|---|---|---|
| Recrystallization | Cube | {100}〈100〉 | ■ (sky blue) |
| Goss | {110}〈100〉 | ● (sky blue) | |
| P | {110}〈122〉 | ▲ (sky blue) | |
| Rolling | Brass | {110}〈112〉 | ■ (pink) |
| Copper | {112}〈111〉 | ● (pink) | |
| S | {123}〈634〉 | ▲ (pink) | |
| Shear | Shear1 | {100}〈110〉 | ■ (gray) |
| Shear2 | {111}〈112〉 | ● (gray) | |
| Shear3 | {111}〈110〉 | ▲ (gray) | |
| Shear4 | {112}〈110〉 | ▼ (gray) |
Fig. 3. The IPF, kernel average misorientation (KAM), and GB maps for the microstructures of the samples rolled at SR of (a) 2 and (b) 4 with high magnification. The KAM and GB maps show the rectangular regions in the IPF maps.
Fig. 4. The orientation gradients marked along the lines (a) A, (b) B, (c) C, and (d) D in Fig. 3(a) and (b), and (e) A and (f) B in Fig. 13(b) and (d).
Fig. 6. The grain size distribution in the samples rolled with different SRs. (a) As-rolled samples and (b) the rolled samples after annealing at 973 K for 1 h.
Fig. 7. (a) The XRD curves for the samples deformed with different SRs and (b) the magnified (111) peaks in (a). (c) The dislocation density calculated based on the XRD and EBSD data.
Fig. 9. The ODF intensities of individual texture components belonging to recrystallization, rolling, and shear texture at different SRs: (a) 1, (b) 2, (c) 3, and (d) 4.
Fig. 12. The spatial relationship between the overlapped rolling texture and shear texture components: the rotation between (a) copper texture and shear1 around [$10\bar{1}$], (b) copper texture and shear2 around [$1\bar{1}0$], (c) S texture and shear3 around [$7\bar{9}11$], and (d) brass and shear4 around [$\bar{1}11$].
Fig. 13. The IPF, KAM, and GB maps for the microstructures of the samples annealed at 873 K for 1 h with different SRs: (a) 1, (b) 2, (c) 3, and (d) 4. The KAM and GB maps show the rectangular regions in the IPF maps.
Fig. 14. The φ2=0°, 45°, and 63° ODF sections of the samples annealed at 873 K for 1 h with different SRs: (a) 1, (b) 2, (c) 3, and (d) 4. The φ2=0°, 45°, and 63° ODF sections of the samples annealed at 973 K for 1 h with different SRs: (e) 1, (f) 2, (g) 3, and (h) 4.
Fig. 17. The plots for the ODF intensities of various texture components as a function of annealing temperature including the data for the initial and as-rolled samples at different SRs: (a) 1, (b) 2, (c) 3, and (d) 4. The plots of the ODF intensities of shear texture components as a function of SR for the samples prepared under different conditions: (e) as-rolled, (f) annealed at 873 K, and (g) annealed at 973 K.
Fig. 18. The sum of the area fractions for the grains with the texture components belonging to the (a) α, (b) β, and (c) γ fibers as a function of annealing temperature including the data for the initial and as-rolled samples.
Fig. 19. (a) The microhardness measurement results (along the sheet thickness direction) for the as-rolled samples at different SRs. (b) The engineering stress-engineering strain curves for the as-rolled and annealed samples at different SRs. (c) The plot of σy of the rolled and annealed materials as a function of d - 1/2. (d) The plot of strain hardening rates (and true stress) vs true strain for the rolled and annealed materials.
Fig. 20. (a) Comparison of the calculated yield stresses based on Eq. (3) with the experimental data of the as-rolled materials. (b) Comparison of the calculated yield stresses based on Eqs. (4) and (5) with the experimental data of the rolled materials annealed at 873 K.
| [1] | R.Z. Valiev, R.K. Islamgaliev, I.V. Alexandrov, Prog.Mater. Sci. 45 (2000) 103-189. |
| [2] |
Y. Estrin, A. Vinogradov, Acta Mater 61 (2013) 782-817.
DOI URL |
| [3] |
D. Orlov, G. Raab, T.T. Lamark, M. Popov, Y. Estrin, Acta Mater 59 (2011) 375-385.
DOI URL |
| [4] |
Z.J. Zheng, Y. Gao, Y. Gui, M. Zhu, Corros. Sci. 54 (2012) 60-67.
DOI URL |
| [5] | Y.J. Chen, Y.J. Li, J.C. Walmsley, S. Dumoulin, S.S. Gireeh, S. Armada, P.C. Skaret, H.J. Roven, Scr.Mater. 64 (2011) 904-907. |
| [6] |
K. Edalati, R. Miresmaeili, Z. Horita, H. Kanayama, R. Pippan, Mater. Sci. Eng. A 528 (2011) 7301-7305.
DOI URL |
| [7] |
F.A. Mohamed, S.S. Dheda, Mater. Sci. Eng. A 558 (2012) 59-63.
DOI URL |
| [8] |
B.B. Straumal, A.R. Kilmametov, Y. Ivanisenko, L. Kurmanaeva, B. Baretzky, Y.O. Kucheev, P. Zięba, A. Korneva, D.A. Molodov, Mater. Lett. 118 (2014) 111-114.
DOI URL |
| [9] |
M.R. Totoghinejad, F. Ashrafizadeh, R. Jamaati, Mater. Sci. Eng. A 561 (2013) 145-151.
DOI URL |
| [10] |
A. Fattah-alhosseini, O. Imantalab, J. Alloys Compd. 632 (2015) 48-52.
DOI URL |
| [11] |
M.M. Mahdavian, L. Chalandari, M. Reihanian, Mater. Sci. Eng. A 579 (2013) 99-107.
DOI URL |
| [12] |
A. Bahmani, W.J. Kim, Materials (Basel) 13 (2020) 4159.
DOI URL |
| [13] | W. Polkowski, V. Glebovsky (Ed.), Progress in Metallic Alloys, InTechOpen, Lon- don(2016) 111-126. |
| [14] | W.J. Kim, S.J. Yoo, J.B. Lee, Scr.Mater. 62 (2010) 451-454. |
| [15] |
Y.G. Ko, J. Suharto, J.S. Lee, B.H. Park, D.H. Shin, Met. Mater. Int. 19 (2013) 603-609.
DOI URL |
| [16] |
K. Hamad, Y.G. Ko, Mater. Lett. 160 (2015) 213-217.
DOI URL |
| [17] |
W. Polkowski, P. Jó′zwik, M. Pola ′nski, Z. Bojar, Mater. Sci. Eng. A 564 (2013) 289-297.
DOI URL |
| [18] |
W.Y. Kim, W.J. Kim, Mater. Sci. Eng. A 594 (2014) 189-192.
DOI URL |
| [19] |
W.J. Kim, S.J. Yoo, H.T. Jeong, D.M. Kim, B.H. Choe, J.B. Lee, Scr. Mater. 64 (2011) 49-52.
DOI URL |
| [20] |
W. Polkowski, P. Jó′zwik, Z. Bojar, Metall. Mater. Trans. A 46 (2015) 2216-2226.
DOI URL |
| [21] |
J.W. Yeh, JOM 65 (2013) 1759-1771.
DOI URL |
| [22] |
D.B. Miracle, J.D. Miller, O.N. Senkov, C. Woodward, M.D. Uchic, J. Tiley, Entropy 16 (2014) 494-525.
DOI URL |
| [23] |
G.D. Sathiaraj, P.P. Bhattacharjee, Mater. Charact. 109 (2015) 189-197.
DOI URL |
| [24] |
J. Hou, M. Zhang, S. Ma, P.K. Liaw, Y. Zhang, J. Qiao, Mater. Sci. Eng. A 707 (2017) 593-601.
DOI URL |
| [25] |
S.R. Reddy, M.Z. Ahmed, G.D. Sathiaraj, P.P. Bhattacharjee, Intermetallics 87 (2017) 94-103.
DOI URL |
| [26] |
X. Liang, Q. Wu, H. Li, R. Wang, L. Kang, B. Liu, L. Wang, J. Alloy. Compd. 862 (2021) 158602.
DOI URL |
| [27] |
L. Kaushik, M.S. Kim, J. Singh, J.H. Kang, Y.U. Heo, J.Y. Suh, S.H. Choi, Int. J. Plast. 141 (2021) 102989.
DOI URL |
| [28] |
J. Saha, G. Ummethala, S.R.K. Malladi, P.P. Bhattacharjee, Intermetallics 129 (2021) 107029.
DOI URL |
| [29] |
G.D. Sathiaraj, P.P. Bhattacharjee, J. Alloy. Compd. 637 (2015) 267-276.
DOI URL |
| [30] |
D.P. Field, L.T. Bradford, M.M. Nowell, T.M. Lillo, Acta Mater 55 (2007) 4233-4241.
DOI URL |
| [31] |
N. Bozzolo, M. Bernacki, Metall. Mater. Trans. A 51 (2020) 2665-2684.
DOI URL |
| [32] |
P. Asghari-Rad, R. Sathiyamoorthi, N.T.C. Nguyen, J.W. Bae, H. Shahmir, H.S. Kim, Mater. Sci. Eng. A 771 (2020) 138604.
DOI URL |
| [33] | J.W. Liu, Q.P. Cao, L.Y. Chen, X.D. Wang, J.Z. Jiang, Acta Mater 58 (2010) 4 827-4 840. |
| [34] | T. Sakai, A. Belyakov, R. Kaibyshev, H. Miura, J.J. Jonas, Prog.Mater. Sci. 60 (2014) 130-207. |
| [35] |
K. Huang, R.E. Logé, Mater. Des. 111 (2016) 548-574.
DOI URL |
| [36] |
Y.C. Lin, X.Y. Wu, X.M. Chen, J. Chen, D.X. Wen, J.L. Zhang, L.T. Li, J. Alloy. Compd. 640 (2015) 101-113.
DOI URL |
| [37] |
I.L. Dillamore, W.T. Roberts, Acta Metall 12 (1964) 281-293.
DOI URL |
| [38] |
E.A. Calnan, Acta Metall 2 (1954) 865-874.
DOI URL |
| [39] | T. Leffers, D.J. Jensen, Textures Microstruct 8-9 (1988) 467-480. |
| [40] |
F. Shen, D. Yi, Y. Jiang, B. Wang, H. Liu, C. Tang, W. Shou, Mater. Sci. Eng. A 657 (2016) 15-25.
DOI URL |
| [41] |
A. Takayama, X. Yang, H. Miura, T. Sakai, Mater. Sci. Eng. A 478 (2008) 221-228.
DOI URL |
| [42] |
A. Belyakov, T. Sakai, H. Miura, R. Kaibyshev, K. Tsuzaki, Acta Mater 50 (2002) 1547-1557.
DOI URL |
| [43] | H. Jin, S. Saimoto, Mater. Sci. Technol. 19 (2003) 1197-1206. |
| [44] |
X. Yang, Y. Okabe, H. Miura, T. Sakai, Mater. Sci. Eng. A 535 (2012) 209-215.
DOI URL |
| [45] |
Y.G. An, H. Vegter, S. Melzer, P.R. Triguero, J. Mater. Process. Technol. 213 (2013) 1419-1425.
DOI URL |
| [46] | S. Tamimi, G. Sivaswamy, I. Violatos, S. Moturu, S. Rahimi, P. Blackwell, Proce- dia Eng 207 (2017) 1-6. |
| [47] |
H. Inoue, T. Takasugi, Mater. Trans. 48 (2007) 2014-2022.
DOI URL |
| [48] |
J. Sidor, A. Miroux, R. Petrov, L. Kestens, Acta Mater 56 (2008) 2495-2507.
DOI URL |
| [49] | O. Noguchi, T. Komatsubara, T. Sakuma, R. Baba, K. Yoshida, Mater. Forum 28 (2004) 758-763. |
| [50] |
H. Jin, D.J. Lloyd, Mater. Sci. Eng. A 399 (2005) 358-367.
DOI URL |
| [51] |
H.T. Jeong, W.J. Kim, Mater. Sci. Eng. A 727 (2018) 38-42.
DOI URL |
| [52] |
D.A. Hughes, N. Hansen, Acta Mater 48 (2000) 2985-30 04.
DOI URL |
| [53] | H.T. Jeong, W.J. Kim, J. Mater. Sci.Technol. 42 (2020) 190-202. |
| [54] |
G. Laplanche, P. Gadaud, O. Horst, F. Otto, G. Eggeler, E.P. George, J. Alloy. Compd. 623 (2015) 348-353.
DOI URL |
| [55] |
R. Shi, Z. Nie, Q. Fan, F. Wang, Y. Zhou, X. Liu, Mater. Sci. Eng. A 715 (2018) 101-107.
DOI URL |
| [56] |
F.F. Lavrentev, Mater. Sci. Eng. 46 (1980) 191-208.
DOI URL |
| [57] |
J.Y. He, W.H. Liu, H. Wang, Y. Wu, X.J. Liu, T.G. Nieh, Z.P. Lu, Acta Mater 62 (2014) 105-113.
DOI URL |
| [58] |
Z. Wang, R.T. Qu, S. Scudino, D.A. Sun, K.G. Prashanth, D.V. Louzguine-Luzgin, M.W. Chen, Z.F. Zhang, J. Eckert, NPG Asia Mater 7 (2015) e229.
DOI URL |
| [59] |
S.J. Sun, Y.Z. Tian, H.R. Lin, H.J. Yang, X.G. Dong, Y.H. Wang, Z.F. Zhang, Mater. Sci. Eng. A 712 (2018) 603-607.
DOI URL |
| [60] |
S.W. Wu, G. Wang, J. Yi, Y.D. Jia, I. Hussain, Q.J. Zhai, P.K. Liaw, Mater. Res. Lett. 5 (2017) 276-283.
DOI URL |
| [1] | Hanchen Feng, Lei Cai, Linfeng Wang, Xiaodan Zhang, Feng Fang. Microstructure and strength in ultrastrong cold-drawn medium carbon steel [J]. J. Mater. Sci. Technol., 2022, 97(0): 89-100. |
| [2] | Shiyu Wu, Dongxu Qiao, Haitao Zhang, Junwei Miao, Hongliang Zhao, Jun Wang, Yiping Lu, Tongmin Wang, Tingju Li. Microstructure and mechanical properties of CxHf0.25NbTaW0.5 refractory high-entropy alloys at room and high temperatures [J]. J. Mater. Sci. Technol., 2022, 97(0): 229-238. |
| [3] | Ruifeng Dong, Xiaoyang Zhang, Chenhui Li, Yuhong Zhao, Jinzhong Tian, Li Wu, Hua Hou. Correlation between the mechanical properties and the 〈110〉 texture in a hot-rolled near β titanium alloy [J]. J. Mater. Sci. Technol., 2022, 97(0): 165-168. |
| [4] | Dong Huang, Yanxin Zhuang. Break the strength-ductility trade-off in a transformation-induced plasticity high-entropy alloy reinforced with precipitation strengthening [J]. J. Mater. Sci. Technol., 2022, 108(0): 125-132. |
| [5] | Zhong Zheng, Xuexi Zhang, Mingfang Qian, Jianchao Li, Muhammad Imran, Lin Geng. Ultra-high strength GNP/2024Al composite via thermomechanical treatment [J]. J. Mater. Sci. Technol., 2022, 108(0): 164-172. |
| [6] | Hyun Chung, Dae Woong Kim, Woo Jin Cho, Heung Nam Han, Yuji Ikeda, Shoji Ishibashi, Fritz Körmann, Seok Su Sohn. Effect of solid-solution strengthening on deformation mechanisms and strain hardening in medium-entropy V1-xCrxCoNi alloys [J]. J. Mater. Sci. Technol., 2022, 108(0): 270-280. |
| [7] | H.R. Peng, Z.Y. Jian, C.X. Liu, L.K. Huang, Y.M. Ren, F. Liu. Uncovering the softening mechanism and exploring the strengthening strategies in extremely fine nanograined metals: A molecular dynamics study [J]. J. Mater. Sci. Technol., 2022, 109(0): 186-196. |
| [8] | Xinde Huang, Yunchang Xin, Yu Cao, Guangjie Huang, Wei Li. A quantitative study on planar mechanical anisotropy of a Mg-2Zn-1Ca alloy [J]. J. Mater. Sci. Technol., 2022, 109(0): 30-48. |
| [9] | Jianwen Le, Yuanfei Han, Peikun Qiu, Shaopeng Li, Guangfa Huang, Jianwei Mao, Weijie Lu. Insight into the formation mechanism and interaction of matrix/TiB whisker textures and their synergistic effect on property anisotropy in titanium matrix composites [J]. J. Mater. Sci. Technol., 2022, 110(0): 1-13. |
| [10] | C. Yang, M.Q. Li, Y.G. Liu. Characterization of face-centered cubic structure and deformation mechanisms in high energy shot peening process of TC17 [J]. J. Mater. Sci. Technol., 2022, 110(0): 136-151. |
| [11] | Wenjie Lu, Kang Yan, Xian Luo, Yuetang Wang, Le Hou, Pengtao Li, Bin Huang, Yanqing Yang. Superb strength and ductility balance of a Co-free medium-entropy alloy with dual heterogeneous structures [J]. J. Mater. Sci. Technol., 2022, 98(0): 197-204. |
| [12] | Lei Lei, Qinyang Zhao, Cong Wu, Yongqing Zhao, Shixing Huang, Weiju Jia, Weidong Zeng. Variant selection, coarsening behavior of α phase and associated tensile properties in an α+β titanium alloy [J]. J. Mater. Sci. Technol., 2022, 99(0): 101-113. |
| [13] | Yu Liao, Junhua Bai, Fuwen Chen, Guanglong Xu, Yuwen Cui. Microstructural strengthening and toughening mechanisms in Fe-containing Ti-6Al-4V: A comparison between homogenization and aging treated states [J]. J. Mater. Sci. Technol., 2022, 99(0): 114-126. |
| [14] | Huang Chunping, Liang Renyu, Liu Fenggang, Yang Haiou, Lin Xin. Effect of dimensionless heat input during laser solid forming of high-strength steel [J]. J. Mater. Sci. Technol., 2022, 99(0): 127-137. |
| [15] | Tianyi Han, Yong Liu, Mingqing Liao, Danni Yang, Nan Qu, Zhonghong Lai, Jingchuan Zhu. Refined microstructure and enhanced mechanical properties of AlCrFe2Ni2 medium entropy alloy produced via laser remelting [J]. J. Mater. Sci. Technol., 2022, 99(0): 18-27. |
| Viewed | ||||||
|
Full text |
|
|||||
|
Abstract |
|
|||||
WeChat

