J. Mater. Sci. Technol. ›› 2021, Vol. 66: 64-73.DOI: 10.1016/j.jmst.2020.05.028
• Research Article • Previous Articles Next Articles
Xiaofei Cuia,b, Wei Fua,*(), Daqing Fanga,*(
), Guangli Bic, Zijun Rena, Shengwu Guoa, Suzhi Lia, Xiangdong Dinga, Jun Suna,*(
)
Received:
2020-01-21
Revised:
2020-05-01
Accepted:
2020-05-13
Published:
2021-03-10
Online:
2021-04-01
Contact:
Wei Fu,Daqing Fang,Jun Sun
About author:
junsun@mail.xjtu.edu.cn (J. Sun).Xiaofei Cui, Wei Fu, Daqing Fang, Guangli Bi, Zijun Ren, Shengwu Guo, Suzhi Li, Xiangdong Ding, Jun Sun. Mechanical properties and deformation mechanisms of a novel fine-grained Mg-Gd-Y-Ag-Zr-Ce alloy with high strength-ductility synergy[J]. J. Mater. Sci. Technol., 2021, 66: 64-73.
Fig. 1. (a) SEM image and (b) EBSD orientation map with inverse pole figure colouring scheme of coarse-grained Mg-Gd-Y-Ag-Zr-Ce alloy. (c) EBSD orientation map and (d) TEM-BF image of fine-grained Mg-Gd-Y-Ag-Zr-Ce alloy. (e, f) Grain size distribution histogram of coarse-grained and fine-grained Mg-Gd-Y-Ag-Zr-Ce alloy, respectively. (g) Mg (Gd, Y, Ag, Ce) particle size distribution histogram of the fine-grained Mg-Gd-Y-Ag-Zr-Ce alloy.
Fig. 2. Bright-field TEM images of the CG alloys aged for 30 h observed from (a) <10$\bar{1}$0>α, (b) <0001>α zone axis. Bright-field TEM images of the CG alloy aged for 300 h observed from (c) <10$\bar{1}$0>α, (d) <0001>α zone axis. (e-l) The statistical results of precipitate size.
Fig. 3. (a) Bright-field TEM images of the Mg-Gd-Y-Ag-Zr-Ce alloy during the cooling process after extrusion. (b) A magnified TEM image of the square area in (a). (c) A high-resolution TEM image of the basal precipitate γ′′.
Fig. 4. (a) Low magnification bright-field TEM images of as-extruded Mg-Gd-Y-Ag-Zr-Ce alloy aged for 60 h. The bright-field TEM images of the nanoscale basal plate-shaped γ′′ precipitates observed from [0001]α zone axis (b), and the prismatic plate-shaped precipitate β′ observed from [11$\bar{2}$0]α zone axis (c).
Fig. 5. TEM identification of the Mg (Gd, Y, Ce, Ag) particles for (a) bright-field image, (b) HRTEM images with the Fourier transform embedded. (c) EDX-STEM spectrum acquired from one of the areas marked with a circle in (a).
Fig. 7. Schematic diagrams of microstructures in (a) solutionized, (b) aged at 200 °C for 300 h, (c) extruded and (d) extruded following by ageing at 200 °C for 60 h.
Fig. 8. (a) The variation of strength as a function of ageing time at 200 °C in CG and FG alloys. (b) Engineering stress-strain curves of FG and CG alloys. (c) Room temperature true stress-strain curves showing strain-rate jump tests of FG specimens at different strain rates ranging from 10-4 to 10-2 s-1.
Fig. 9. Representative SEM images of the fracture surface in CG and FG alloys. (a) Secondary electron (SE) images and (b) backscattered electron (BSE) images of CG alloys. (d) SE images and (e) BSE images of FG alloys. Side view of SEM images of fractured tensile CG (c) and FG (f) specimens.
Fig. 10. Typical microstructure images of the FG alloys. (a) weak-beam dark-field image with diffracting vector of g =$\bar{2}$110α and (b) two-beam bright-field image. Electron beam direction is close to [0$\bar{1}$10]α.
[1] | S.R. Agnew, J.F. Nie, Scr. Mater. 63 (2010) 671-673. |
[2] | C. Dharmendra, K.P. Rao, Y.V.R.K. Prasad, N. Hort, K.U. Kainer, J. Mater. Sci. 48 (2013) 5236-5246. |
[3] | C. Bettles, M. Barnett, Advances in Wrought Magnesium Alloys: Fundamentals of Processing, Properties and Applications, Elsevier, 2012, pp. 20-21. |
[4] | C. Guo, R. Xin, Y. Xiao, G. Liu, Q. Liu, Mater. Des. 102 (2016) 196-201. |
[5] | X. Guo, A. Chapuis, P. Wu, Q. Liu, X. Mao, Mater. Des. 98 (2016) 333-343. |
[6] | R. Kocich, L. Kunčická, P. Král, T.C. Lowe, Mater. Des. 90 (2016) 1092-1099. |
[7] | W.B. Hutchinson, M.R. Barnett, Scr. Mater. 63 (2010) 737-740. |
[8] | D.D. Yin, Q.D. Wang, C.J. Boehlert, Z. Chen, A. Chakkedath, Metall. Mater. Trans. A 47 (2016) 1-15. |
[9] | T. Honma, T. Ohkubo, S. Kamado, K. Hono, Acta Mater. 55 (2007) 4137-4150. |
[10] | W. Fu, R. Wang, K. Wu, J. Kuang, J. Zhang, G. Liu, J. Sun, J. Mater. Sci. 54 (2019) 2628-2647. |
[11] | Z.R. Zeng, Y.M. Zhu, R.L. Liu, S.W. Xu, C.H.J. Davies, J.F. Nie, N. Birbilis, Acta Mater. 160 (2018) 97-108. |
[12] |
Z. Wu, R. Ahmad, B. Yin, S. Sandlöbes, W.A. Curtin, Science 359 (2018) 447-452.
DOI URL PMID |
[13] |
Z. Wu, W.A. Curtin, Proc. Natl. Acad. Sci. U.S.A. 113 (2016) 11137-11142.
URL PMID |
[14] | H.S. Jiang, X.G. Qiao, C. Xu, M.Y. Zheng, K. Wu, S. Kamado, Mater. Des. 108 (2016) 391-399. |
[15] | L. Zhang, J. Zhang, Z. Leng, S. Liu, Q. Yang, R. Wu, M. Zhang, Mater. Des. 54 (2014) 256-263. |
[16] | Z. Su, C. Liu, Y. Wan, Mater. Des. 45 (2013) 466-472. |
[17] | J. Zhang, S. Liu, R. Wu, L. Hou, M. Zhang, J. Magnes. Alloys 6 (2018) 277-291. |
[18] | F. Zhong, H. Wu, Y. Jiao, R. Wu, J. Zhang, L. Hou, M. Zhang, J. Mater. Sci. Technol. 39 (2020) 124-134. |
[19] | H.R.J. Nodooshan, G.H. Wu, W.C. Liu, G.L. Wei, Y.L. Li, S. Zhang, Mater. Sci. Eng. A 651 (2016) 840-847. |
[20] | Q. Wang, J. Chen, Z. Zhao, S. He, Mater. Sci. Eng. A 528 (2010) 323-328. |
[21] | J. Miao, W. Sun, A.D. Klarner, A.A. Luo, Scr. Mater. 154 (2018) 192-196. |
[22] | R.K. Sabat, R.K. Mishra, A.K. Sachdev, S. Suwas, Mater. Lett. 153 (2015) 158-161. |
[23] | Y. Chino, M. Kado, M. Mabuchi, Acta Mater. 56 (2008) 387-394. |
[24] | T. Al-Samman, X. Li, Mater. Sci. Eng. A 528 (2011) 3809-3822. |
[25] | A. Kula, X. Jia, R.K. Mishra, M. Niewczas, Int. J. Plasticity 92 (2017) 96-121. |
[26] | L. Mackenzie, M. Pekguleryuz, Scr. Mater. 59 (2008) 665-668. |
[27] | I.P. Moreno, T.K. Nandy, J.W. Jones, J.E. Allison, T.M. Pollock, Scr. Mater. 48 (2003) 1029-1034. |
[28] | A. Deschamps, F. Bley, F. Livet, D. Fabregue, L. David, Philos. Mag. 83 (2003) 677-692. |
[29] | S. Xu, N. Matsumoto, S. Kamado, T. Honma, Y. Kojima, Scr. Mater. 61 (2009) 249-252. |
[30] | S. Xu, S. Kamado, T. Honma, Scr. Mater. 63 (2010) 293-296. |
[31] | K. Huang, K. Marthinsen, Q. Zhao, R.E. Logé, Prog. Mater. Sci. 92 (2018) 284-359. |
[32] | T. Mohri, M. Mabuchi, M. Nakamura, T. Asahina, H. Iwasaki, T. Aizawa, K. Higashi, Mater. Sci. Eng. A 290 (2000) 139-144. |
[33] | S.W. Xu, K. Oh-ishi, S. Kamado, F. Uchida, T. Homma, K. Hono, Scr. Mater. 65 (3) (2011) 269-272. |
[34] | H. Yu, S.H. Park, B.S. You, Mater. Sci. Eng. A 610 (2014) 445-449. |
[35] | Y. Zhang, Y. Wu, L. Peng, P. Fu, W. Ding, J. Alloys Compd. 615 (2014) 703-711. |
[36] | J.F. Nie, K. Oh-ishi, X. Gao, K. Hono, Acta Mater. 56 (2008) 6061-6076. |
[37] | C.R. Hutchinson, J.F. Nie, S. Gorsse, Metall. Mater. Trans. A 36 (2005) 2093-2105. |
[38] | C. Caceres, C. Davidson, J. Griffiths, C. Newton, Mater. Sci. Eng. A 325 (2002) 344-355. |
[39] | J.F. Nie, Scr. Mater. 48 (2003) 1009-1015. |
[40] | J.F. Nie, B.C. Muddle, I.J. Polmear, Mater. Sci. Forum Trans.Tech. Publ. 217 (1996) 1257-1262. |
[41] | N. Stanford, D. Atwell, Metall. Mater. Trans. A 44 (2013) 4830-4843. |
[42] | Z. Zeng, Y. Zhu, R. Liu, S. Xu, C. Davies, J. Nie, N. Birbilis, Acta Mater. 160 (2018) 97-108. |
[43] | H. Somekawa, T. Inoue, K. Tsuzaki, Philos. Mag. 93 (2013) 4582-4592. |
[44] | H. Somekawa, H. Watanabe, T. Mukai, Philos. Mag. 94 (2014) 1345-1360. |
[45] | T.H. Hyde, K.A. Yehia, A.A. Becker, High Temperature Technol. 13 (1995) 133-138. |
[46] | Y. Wang, E. Ma, Mater. Sci. Eng A 375 (2004) 46-52. |
[47] | J. Chen, L. Lu, K. Lu, Scr. Mater. 54 (2006) 1913-1918. |
[48] | H. Choi, Y. Kim, J. Shin, D. Bae, Mater. Sci. Eng. A 527 (2010) 1565-1570. |
[49] | C. Cepeda-Jiménez, J. Molina-Aldareguia, M. Pérez-Prado, Acta Mater. 88 (2015) 232-244. |
[50] | N. Tsuchida, Y. Tomota, K. Nagai, K. Fukaura, Scr. Mater. 54 (2006) 57-60. |
[51] | A.H. Cottrell, B. Bilby, Proc. Phys. Soc. Section A 62 (1949) 49. |
[52] |
D.H. Johnson, M.R. Edwards, P. Chard-Tuckey, Mater. Sci. Eng. A 625 (2015) 36-45.
DOI URL |
[53] | G.T. Hahn, Acta Metall. 10 (1962) 727-738. |
[54] | O. Muránsky, M.R. Barnett, V. Luzin, S. Vogel, Mater. Sci. Eng. A 527 (2010) 1383-1394. |
[55] | M. Ashby, Philos. Mag. 21 (1970) 399-424. |
[56] | D. Johnson, M. Edwards, P. Chard-Tuckey, Mater. Sci. Eng. A 625 (2015) 36-45. |
[57] | J.P. Bailon, A. Loyer, J.M. Dorlot, Mater. Sci. Eng. A 8 (1971) 288-298. |
[58] | M. Barnett, Z. Keshavarz, A. Beer, D. Atwell, Acta Mater. 52 (2004) 5093-5103. |
[1] | Yuhui Zhang, Yuling Liu, Shuhong Liu, Hai-Lin Chen, Qing Chen, Shiyi Wen, Yong Du. Assessment of atomic mobilities and simulation of precipitation evolution in Mg-X (X=Al, Zn, Sn) alloys [J]. J. Mater. Sci. Technol., 2021, 62(0): 70-82. |
[2] | Yifan Wang, Yanli Lu, Jing Zhang, Wenchao Yang, Changlin Yang, Pan Wang, Xiaoqing Song, Zheng Chen. Investigation of the 12 orientations variants of nanoscale Al precipitates in eutectic Si of Al-7Si-0.6Mg alloy [J]. J. Mater. Sci. Technol., 2021, 67(0): 186-196. |
[3] | Qianqian Jin, Xiaohong Shao, Shijian Zheng, Yangtao Zhou, Bo Zhang, Xiuliang Ma. Interfacial dislocations dominated lateral growth of long-period stacking ordered phase in Mg alloys [J]. J. Mater. Sci. Technol., 2021, 61(0): 114-118. |
[4] | Shenbao Jin, Zhenjiao Luo, Xianghai An, Xiaozhou Liao, Jiehua Li, Gang Sha. Composition-dependent dynamic precipitation and grain refinement in Al-Si system under high-pressure torsion [J]. J. Mater. Sci. Technol., 2021, 68(0): 199-208. |
[5] | Xiaoxiao Wei, Li Jin, Fenghua Wang, Jing Li, Nan Ye, Zhenyan Zhang, Jie Dong. High strength and ductility Mg-8Gd-3Y-0.5Zr alloy with bimodal structure and nano-precipitates [J]. J. Mater. Sci. Technol., 2020, 44(0): 19-23. |
[6] | Weiyi Wang, Qinglin Pan, Geng Lin, Xiaoping Wang, Yuqiao Sun, Xiangdong Wang, Ji Ye, Yuanwei Sun, Yi Yu, Fuqing Jiang, Jun Li, Yaru Liu. Microstructure and properties of novel Al-Ce-Sc, Al-Ce-Y, Al-Ce-Zr and Al-Ce-Sc-Y alloy conductors processed by die casting, hot extrusion and cold drawing [J]. J. Mater. Sci. Technol., 2020, 58(0): 155-170. |
[7] | Xiao-Yuan Wang, Yu-Fei Wang, Cheng Wang, Shun Xu, Jian Rong, Zhi-Zheng Yang, Jin-Guo Wang, Hui-Yuan Wang. A simultaneous improvement of both strength and ductility by Sn addition in as-extruded Mg-6Al-4Zn alloy [J]. J. Mater. Sci. Technol., 2020, 49(0): 117-125. |
[8] | Shuo Wang, Chi Zhang, Xin Li, Houbing Huang, Junsheng Wang. First-principle investigation on the interfacial structure evolution of the δ'/θ'/δ' composite precipitates in Al-Cu-Li alloys [J]. J. Mater. Sci. Technol., 2020, 58(0): 205-214. |
[9] | Sang-Hoon Kim, Sang Won Lee, Byoung Gi Moon, Ha Sik Kim, Sung Hyuk Park. Variation in dynamic deformation behavior and resultant yield asymmetry of AZ80 alloy with extrusion temperature [J]. J. Mater. Sci. Technol., 2020, 46(0): 225-236. |
[10] | Pengfei Zhang, Yunchang Xin, Ling Zhang, Shiwei Pan, Qing Liu. On the texture memory effect of a cross-rolled Mg-2Zn-2Gd plate after unidirectional rolling [J]. J. Mater. Sci. Technol., 2020, 41(0): 98-104. |
[11] | Qiang Lu, Kai Li, Haonan Chen, Mingjun Yang, Xinyue Lan, Tong Yang, Shuhong Liu, Min Song, Lingfei Cao, Yong Du. Simultaneously enhanced strength and ductility of 6xxx Al alloys via manipulating meso-scale and nano-scale structures guided with phase equilibrium [J]. J. Mater. Sci. Technol., 2020, 41(0): 139-148. |
[12] | Xiru Hua, Qiang Yang, Dongdong Zhang, Fanzhi Meng, Chong Chen, Zihao You, Jinghuai Zhang, Shuhui Lv, Jian Meng. Microstructures and mechanical properties of a newly developed high-pressure die casting Mg-Zn-RE alloy [J]. J. Mater. Sci. Technol., 2020, 53(0): 174-184. |
[13] | Tao Yuan, Xin Song, Xianglong Zhou, Wentao Jia, Munzali Musa, Jingdong Wang, Tianyu Ma. Role of primary Zr-rich particles on microstructure and magnetic properties of 2:17-type Sm-Co-Fe-Cu-Zr permanent magnets [J]. J. Mater. Sci. Technol., 2020, 53(0): 73-81. |
[14] | Qiuyan Huang, Yang Liu, Aiyue Zhang, Haoxin Jiang, Hucheng Pan, Xiaohui Feng, Changlin Yang, Tianjiao Luo, Yingju Li, Yuansheng Yang. Age hardening responses of as-extruded Mg-2.5Sn-1.5Ca alloys with a wide range of Al concentration [J]. J. Mater. Sci. Technol., 2020, 38(0): 39-46. |
[15] | Maryam Jamalian, David P.Field. Gradient microstructure and enhanced mechanical performance of magnesium alloy by severe impact loading [J]. J. Mater. Sci. Technol., 2020, 36(0): 45-49. |
Viewed | ||||||
Full text |
|
|||||
Abstract |
|
|||||