J. Mater. Sci. Technol. ›› 2022, Vol. 99: 193-206.DOI: 10.1016/j.jmst.2021.04.072
• Research article • Previous Articles Next Articles
Xiang Peng, Wencai Liu*(
), Guohua Wu*(), Hao Ji, Wenjiang Ding
Received:2021-03-02
Revised:2021-03-30
Accepted:2021-04-21
Published:2022-02-10
Online:2022-02-09
Contact:
Wencai Liu,Guohua Wu
About author:ghwu@sjtu.edu.cn (G. Wu).Xiang Peng, Wencai Liu, Guohua Wu, Hao Ji, Wenjiang Ding. Plastic deformation and heat treatment of Mg-Li alloys: a review[J]. J. Mater. Sci. Technol., 2022, 99: 193-206.
Fig. 1. Binary phase diagram of Mg-Li alloy [31].
Fig. 2. The comparison between experimental and predicted results at different strain rates: (a) 1 s-1, (b) 0.1 s-1, (c) 0.01 s-1 and (d) 0.001 s-1 [35].
Fig. 3. Microstructure of extruded Mg-9Li-3Al-2.5Sr alloy with different extrusion temperatures: (a-c) 250 °C; (d-f) 300 °C; (g-i) 350 °C [57].
Fig. 4. Microstructure of extruded Mg-8Li-3Al-(1, 2, 3)Sn alloys observed by (a-c) OM and (e-f) SEM [2].
Fig. 5. Pole figures of the extruded Mg-Li sheets: (a) Mg-1Li, (b) Mg-2Li, (c) Mg-3Li [62].
| Alloy | State | Yield strength (MPa) | Ultimate tensile strength (MPa) | Elongation (%) |
|---|---|---|---|---|
| Mg-8Li-3Al-1Sn | As-cast | 116 ± 3 | 176 ±7 | 15.9 ±1.2 |
| As-extruded | 251 ±2 | 275 ±4 | 17.4 ±1.4 | |
| Mg-8Li-3Al-2Sn | As-cast | 138 ±2 | 177 ±5 | 12.3 ±0.8 |
| As-extruded | 270 ±4 | 297 ±5 | 20.8 ±1.5 | |
| Mg-8Li-3Al-3Sn | As-cast | 156 ±3 | 190 ±3 | 9.9 ±2.3 |
| As-extruded | 253 ±6 | 289 ±8 | 17.9 ±2.1 |
Table 1 The effect of extrusion on tensile properties in the Mg-8Li-3Al-(1, 2, 3)Sn alloys [2].
| Alloy | State | Yield strength (MPa) | Ultimate tensile strength (MPa) | Elongation (%) |
|---|---|---|---|---|
| Mg-8Li-3Al-1Sn | As-cast | 116 ± 3 | 176 ±7 | 15.9 ±1.2 |
| As-extruded | 251 ±2 | 275 ±4 | 17.4 ±1.4 | |
| Mg-8Li-3Al-2Sn | As-cast | 138 ±2 | 177 ±5 | 12.3 ±0.8 |
| As-extruded | 270 ±4 | 297 ±5 | 20.8 ±1.5 | |
| Mg-8Li-3Al-3Sn | As-cast | 156 ±3 | 190 ±3 | 9.9 ±2.3 |
| As-extruded | 253 ±6 | 289 ±8 | 17.9 ±2.1 |
Fig. 6. SEM and EDS analysis of cast and extruded Mg-8Li-3Al-2Zn-0.5Y alloy with different ratios: (a) 4:1; (b) 9:1; (c) 16:1; (d) 25:1; (e) cast specimen; (f) typical EDS pointing analysis for the labeled-B particles [40].
| Direction | Cumulative rolling strain | Yield strength (MPa) | Ultimate tensile strength (MPa) | Elongation (%) | |||
|---|---|---|---|---|---|---|---|
| Mean | STD | Mean | STD* | Mean | STD* | ||
| As-cast | 165.1 | 5.6 | 200.3 | 4.2 | 13.9 | 2.6 | |
| RD | 10% | 169.2 | 4.1 | 209.3 | 3.7 | 10.5 | 1.2 |
| 30% | 205.3 | 3.5 | 240.2 | 4.5 | 8.2 | 1.2 | |
| 50% | 213.5 | 4.6 | 247.1 | 2.7 | 7.3 | 1.1 | |
| 60% | 224.8 | 4.4 | 247.5 | 1.6 | 7.2 | 0.5 | |
| 70% | 230.3 | 2.1 | 250.9 | 3.1 | 7.1 | 0.9 | |
| TD | 10% | 181.3 | 2.3 | 211.3 | 1.5 | 7.5 | 0.9 |
| 30% | 198.6 | 2.8 | 228.7 | 4.6 | 4.3 | 0.6 | |
| 50% | 202.6 | 2.2 | 238.2 | 3.3 | 3.2 | 0.5 | |
| 60% | 208.8 | 3.8 | 239.7 | 3.2 | 2.9 | 0.3 | |
| 70% | 210.4 | 4.2 | 248.2 | 2.5 | 2.7 | 0.2 | |
Table 2 Tensile properties of as-cast and as-rolled Mg-8Li-3Al-2Zn-0.5Y in two directions [39]
| Direction | Cumulative rolling strain | Yield strength (MPa) | Ultimate tensile strength (MPa) | Elongation (%) | |||
|---|---|---|---|---|---|---|---|
| Mean | STD | Mean | STD* | Mean | STD* | ||
| As-cast | 165.1 | 5.6 | 200.3 | 4.2 | 13.9 | 2.6 | |
| RD | 10% | 169.2 | 4.1 | 209.3 | 3.7 | 10.5 | 1.2 |
| 30% | 205.3 | 3.5 | 240.2 | 4.5 | 8.2 | 1.2 | |
| 50% | 213.5 | 4.6 | 247.1 | 2.7 | 7.3 | 1.1 | |
| 60% | 224.8 | 4.4 | 247.5 | 1.6 | 7.2 | 0.5 | |
| 70% | 230.3 | 2.1 | 250.9 | 3.1 | 7.1 | 0.9 | |
| TD | 10% | 181.3 | 2.3 | 211.3 | 1.5 | 7.5 | 0.9 |
| 30% | 198.6 | 2.8 | 228.7 | 4.6 | 4.3 | 0.6 | |
| 50% | 202.6 | 2.2 | 238.2 | 3.3 | 3.2 | 0.5 | |
| 60% | 208.8 | 3.8 | 239.7 | 3.2 | 2.9 | 0.3 | |
| 70% | 210.4 | 4.2 | 248.2 | 2.5 | 2.7 | 0.2 | |
Fig. 7. Pole figures of as-rolled (a) sheet 1, (b) sheet 2, and (c) sheet 3. Inverse pole figures of the as-rolled (d) sheet 1, (e) sheet 2, and (f) sheet 3. The alloy sheet 1 subjected the rolling deformation with the RD (rolling direction), TD (transverse direction) and ND (normal direction) are all invariable between rolling passes. The alloy sheet 2 subjected the rolling deformation with the RD deflects 180°C, while TD and ND are invariable between rolling passes deformation. As for sheet 3, TD is invariable, while RD and ND deflect 180°C [50].
Fig. 8. Microstructures of the Mg-8Li alloy after HPT processing for 5 turns: (a) bright-field image, (b) SAED pattern, (c) dark-field image and (d) appearance of HPT-processed samples after pulling to failure at different temperatures [74].
Fig. 9. The stress-strain curves of the CARB-processed Mg-5Li-1Al alloy: (a) along RD, (b) along TD [22].
Fig. 10. Mechanical properties of the LA143 alloys after various MDF passes: (a) True stress-strain curves for compression tests at 300 K, (b) yield strength and specific yield strength as a function of the total equivalent strain, (c, d) work hardening rate as a function of true strain during compression tests [1].
Fig. 11. TEM bright field micrographs of the aged Mg-8Li-3Al-2Zn-0.5Y alloy at different temperatures for 4 h: (a) 50 °C; (b) 75 °C; (c) 100 °C [16].
Fig. 12. Load vs. displacement plot of (a) α-Mg phase and (b) β-Li phase for as-cast, solutionized and aged Mg-9Li-7Al-1Sn alloy [9].
Fig. 13. (a) Scanning transmission electron microscope (STEM) images, (b) corresponding Al compositional map, and (c, d) atom probe tomography (APT) results of water-quenched Mg-11Li-3Al-1(Zr, Y) alloy [86].
Fig. 14. (a) High-resolution TEM(HRTEM) images of water-quenched Mg-11Li-3Al-1(Zr, Y) alloy, (b) the inverse fast Fourier transform (IFFT) pattern of the area marked by the yellow square in (a), (c) hardness changes in alloys during natural ageing, and (d) bright-field TEM image for Mg-11Li-3Al-1(Zr, Y) after natural aging for 1000 h [86].
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