J. Mater. Sci. Technol. ›› 2020, Vol. 59: 107-116.DOI: 10.1016/j.jmst.2020.04.042
• Research Article • Previous Articles Next Articles
Pingli Jianga,*(), Carsten Blawerta, Jan Bohlena, Mikhail L. Zheludkevicha,b
Received:
2020-01-27
Revised:
2020-04-15
Accepted:
2020-04-16
Published:
2020-12-15
Online:
2020-12-18
Contact:
Pingli Jiang
Pingli Jiang, Carsten Blawert, Jan Bohlen, Mikhail L. Zheludkevich. Corrosion performance, corrosion fatigue behavior and mechanical integrity of an extruded Mg4Zn0.2Sn alloy[J]. J. Mater. Sci. Technol., 2020, 59: 107-116.
Fig. 1. Microstructure of Mg4Zn0.2Sn alloy examined by OM (a) and SEM (b, c) in BSE mode along the extrusion direction. (d) The inverse pole figure parallel to the extrusion direction of Mg4Zn0.2Sn alloy (left: <0001 >, upper right: <11 2ˉ 0 >, lower right: <10 1ˉ 0 >).
Fig. 5. XRD analysis for the compositions of corrosion products formed on Mg4Zn0.2Sn alloy surface after immersion in NaCl-DIW and NaCl-ATW solutions for 48 h.
Tensile property | Compressive property | TYS/CYS | |||
---|---|---|---|---|---|
0.2 % TYS (MPa) | UTS (MPa) | Elongation (%) | 0.2 % CYS (MPa) | UCS (MPa) | |
157 ± 0 | 254 ± 1 | 16 ± 1 | 80 ± 0 | 357 ± 2 | 2.0 |
Table 1 Mechanical properties of Mg4Zn0.2Sn alloy at room temperature.
Tensile property | Compressive property | TYS/CYS | |||
---|---|---|---|---|---|
0.2 % TYS (MPa) | UTS (MPa) | Elongation (%) | 0.2 % CYS (MPa) | UCS (MPa) | |
157 ± 0 | 254 ± 1 | 16 ± 1 | 80 ± 0 | 357 ± 2 | 2.0 |
Fig. 7. Tensile stress-strain curves of Mg4Zn0.2Sn alloy after pre-corrosion in salt spray for different time (a) and variation of tensile mechanical properties with pre-corrosion duration (b).
Salt spray duration (day) | Tensile property | ||
---|---|---|---|
0.2 % TYS (MPa) | UTS (MPa) | Elongation (%) | |
0 | 157 ± 0 | 254 ± 1 | 16 ± 1 |
3 | 156 ± 1 | 248 ± 2 | 11 ± 1 |
7 | 153 ± 2 | 237 ± 7 | 10 ± 3 |
14 | 149 ± 2 | 216 ± 10 | 7 ± 1 |
28 | 136 ± 5 | 189 ± 2 | 4 ± 1 |
Table 2 Mechanical properties of pre-corroded Mg4Zn0.2Sn alloy at room temperature.
Salt spray duration (day) | Tensile property | ||
---|---|---|---|
0.2 % TYS (MPa) | UTS (MPa) | Elongation (%) | |
0 | 157 ± 0 | 254 ± 1 | 16 ± 1 |
3 | 156 ± 1 | 248 ± 2 | 11 ± 1 |
7 | 153 ± 2 | 237 ± 7 | 10 ± 3 |
14 | 149 ± 2 | 216 ± 10 | 7 ± 1 |
28 | 136 ± 5 | 189 ± 2 | 4 ± 1 |
Fig. 9. SEM fracture surfaces of Mg4Zn0.2Sn alloy after tensile tests at room temperature (a, b, c) without exposure to salt spray and with exposure to salt spray for 3 days (d, e, f), 14 days (g, h, i) and 28 days (j, k, l).
Fig. 11. Fatigue fractography of Mg4Zn0.2Sn alloy after fatigue tests under stress amplitude of 155 MPa (27476.5 cycles) in air (a, b, c, d), 120 MPa (2620869 cycles) in NaCl-DIW solution (e, f, g, h) and 125 MPa (1976289 cycles) in NaCl-ATW solution (i, j, k, l).
Fig. 13. Fracture surfaces of Mg4Zn0.2Sn alloy after corrosion fatigue tests in NaCl-DIW solution under stress amplitude of 120 MPa (failed after different cycles).
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