J. Mater. Sci. Technol. ›› 2021, Vol. 72: 132-143.DOI: 10.1016/j.jmst.2020.09.013
• Research Article • Previous Articles Next Articles
Baoguo Yuana, Xing Liub, Jiangfei Dua, Qiang Chena,c,*(
), Yuanyuan Wanc, Yunliang Xiangc, Yan Tangc, Xiaoxue Zhangd, Zhongyue Huanga
Received:2020-07-13
Revised:2020-09-12
Accepted:2020-09-14
Published:2021-05-10
Online:2021-05-10
Contact:
Qiang Chen
About author:* School of Materials Science and Engineering, HefeiUniversity of Technology, Hefei 230009, PR China. E-mail addresses: 2009chenqiang@hfut.edu.cn, 2009chenqiang@163.com (Q. Chen).Baoguo Yuan, Xing Liu, Jiangfei Du, Qiang Chen, Yuanyuan Wan, Yunliang Xiang, Yan Tang, Xiaoxue Zhang, Zhongyue Huang. Effects of hydrogenation temperature on room-temperature compressive properties of CMHT-treated Ti6Al4V alloy[J]. J. Mater. Sci. Technol., 2021, 72: 132-143.
Fig. 1. P-C isotherms of Ti6Al4V alloys hydrogenated at different hydrogenation temperatures.
Fig. 2. Hydrogen absorption rates of Ti6Al4V alloys during the process of CMHT at different hydrogenation temperatures.
Fig. 3. OM micrographs of the as-received Ti6Al4V alloy and alloys treated by four times CMHT at different hydrogenation temperatures: (a) as-received, (b) 650 °C, (c) 700 °C, (d) 750 °C, (e) 800 °C, and (f) 850 °C.
Fig. 4. OM micrographs of Ti6Al4V alloys treated by CMHT at different hydrogenation temperatures with different CMHT numbers but containing the same H/M (0.34): (a) 800 °C, seven times CMHT; and (b) 850 °C, eight times CMHT.
Fig. 5. XRD patterns of the as-received Ti6Al4V alloy and alloys treated by four times CMHT at different hydrogenation temperatures: (a) as-received, (b) 650 °C, (c) 700 °C, (d) 750 °C, (e) 800 °C, and (f) 850 °C.
Fig. 6. XRD patterns of Ti6Al4V alloys treated by CMHT at different hydrogenation temperatures with different CMHT numbers but containing the same H/M (0.34): (a) 800 °C, seven times CMHT; and (b) 850 °C, eight times CMHT.
Fig. 7. TEM images of Ti6Al4V alloy treated by four times CMHT at 700 °C: (a) α phase and δ hydride, and corresponding SAED patterns of α phase with [1 0$\overline 1$ 1]α zone axis and δ hydride with [011]δ zone axis; (b) α phase and corresponding SAED pattern of α phase with [1 $\overline 2$ 1 $\overline 3$]α zone axis; and (c) dark field image of α2 phase with [1 $\overline 2$ 1 $\overline 6$] zone axis.
Fig. 8. TEM images of Ti6Al4V alloy treated by four times CMHT at 750 °C: (a) α' martensite and α” martensite structures, and corresponding SAED patterns of α' martensite with [1 0$\overline 1$ 1]α' zone axis and α” martensite with [31 $\overline 2$]α” zone axis; and (b) parallel δ hydrides and corresponding SAED patterns of parallel δ hydrides with [112]δ zone axis and β phase with [111]β zone axis.
Fig. 9. TEM images of Ti6Al4V alloy treated by four times CMHT at 800 °C: (a) α' martensite and α” martensite structures, and corresponding SAED patterns of α' martensite with [2 $\overline 1$$\overline 1$ 1]α' zone axis and α” martensite with [001]α” zone axis; and (b) δ hydride formed in α phase and corresponding SAED pattern of δ hydride with [$\overline 1$ 12]δ zone axis.
Fig. 10. TEM images of Ti6Al4V alloy treated by four times CMHT at 850 °C: (a) α” martensite structure and corresponding SAED pattern of α” martensite with [001]α” zone axis; (b) fragmentary microstructure; and (c) δ hydride formed in α phase and corresponding SAED pattern of δ hydride with [112]δ zone axis.
Fig. 11. TEM images of Ti6Al4V alloy treated by seven times CMHT at 800 °C with a H/M of 0.34: (a) α' martensite and α” martensite structures, and corresponding SAED patterns of α' martensite with [2 $\overline 1$$\overline 1$ 1]α' zone axis and α” martensite with [100]α” zone axis; and (b) parallel δ hydrides and corresponding SAED pattern of parallel δ hydrides with [011]δ zone axis.
Fig. 12. TEM images of Ti6Al4V alloy treated by eight times CMHT at 850 °C with a H/M of 0.34: (a) α” martensite structure and corresponding SAED patterns of α” martensite with [100]α” zone axis and β phase with [001]β zone axis; and (b) α” martensite structure.
Fig. 13. True stress-true strain curves of Ti6Al4V alloys treated by CMHT at different hydrogenation temperatures: (a) 650 °C, (b) 700 °C, (c) 750 °C, (d) 800 °C, and (e) 850 °C.
Fig. 14. Yield strength of Ti6Al4V alloys treated by CMHT at different hydrogenation temperatures.
Fig. 15. Ultimate compressive strength of Ti6Al4V alloys treated by CMHT at different hydrogenation temperatures.
Fig. 16. Ultimate compression of Ti6Al4V alloys treated by CMHT at different hydrogenation temperatures.
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