J. Mater. Sci. Technol. ›› 2015, Vol. 31 ›› Issue (11): 1151-1157.DOI: 10.1016/j.jmst.2015.07.004

• Orginal Article • Previous Articles     Next Articles

Healing Process of Casting Pores in a Ni-based Superalloy by Hot Isostatic Pressing

X.G. Zheng1, Y.-N. Shi1, L.H. Lou2   

  1. 1 Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China; 2 Superalloy Division, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
  • Received:2015-01-05
  • Contact: * Corresponding author. Master of Science; Tel: +86 24 23971948; Fax: +86 2423998660.E-mail address: yinongshi@imr.ac.cn (Y.-N. Shi).
  • Supported by:
    The authors are grateful for financial support from the Ministry of Science and Technology of the People's Republic of China (No. 2012CB932201), the National Natural Science Foundation of China (No. 51231006), the International Cooperation Program funded by National Natural Science Foundation of China (No. 51261130091) and the Key Research Program of Chinese Academy of Sciences (No. KGZD-EW-T06).

Abstract: Hot isostatic pressing (HIP) with a pressure of 180?MPa at a temperature of 1170?°C was introduced to an investment cast Ni-based superalloy (M91) turbocharger blade to explore the healing process of casting pores generated during investment casting. Optical micrograph and scanning electron microscopy (SEM) observations indicate that eutectic pores are the main cast defects in the as-cast blade before HIP. These pores normally locate at the solidification front of γ/γ′ eutectic with a size of a few micrometers to a few tens of micrometers. After HIP for 4?h, most of the pores were closed. Based on phase characteristics, these pores were healed by the formation of γ matrix with finer and irregular-shaped γ′ precipitates. Healing interface can be easily distinguished by SEM. Line scan by using energy dispersive X-ray spectroscopy (EDS) reveals a much higher Ti and Al concentration in the healing interface. It is proposed that solute diffusion toward the casting pores during HIP results in the formation of γ, and the much higher concentration of γ′-forming elements Al and Ti near the healing interface contributes to the precipitation of γ′ in the healed region in the succeeding cooling process after HIP.

Key words: Superalloy, Hot isostatic pressing (HIP), Healing