Microstructure and Mechanical Properties of C/CeZrCeSiC Composites Fabricated by Reactive Melt Infiltration with Zr, Si Mixed Powders

doi:10.1016/j.jmst.2013.05.005

J. Mater. Sci. Technol. ›› 2013, Vol. 29 ›› Issue (8): 702-710.DOI: 10.1016/j.jmst.2013.05.005

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Microstructure and Mechanical Properties of C/CeZrCeSiC Composites Fabricated by Reactive Melt Infiltration with Zr, Si Mixed Powders

Xin Yang^1,2), Zhean Su²⁾, Qizhong Huang²⁾, Xiao Fang²⁾, Liyuan Chai¹⁾

1) School of Metallurgical Science and Engineering, Central South University, Changsha 410083, China
2) State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, China

Received:2012-06-10 Revised:2012-11-13 Online:2013-08-30 Published:2013-07-17
Contact: Qizhong Huang
Supported by:
China Postdoctoral Science Foundation (No. 2012M511752), the National Basic Research Program of China (No. 2011CB605801), the Fundamental Research Funds for the Central Universities (No. 2012QNZT004), the Freedom Explore Program of Central South University, the Open-End Fund for the Valuable and Precision Instruments of Central South University (No. CSUZC2012026) and the Postdoctoral Science Foundation of Central South University.

Abstract

Abstract:

To meet the increasing demand for advanced materials capable of operation over 2000 °C for future thermal protection systems application, C/C–ZrC–SiC composites were fabricated by reactive melt infiltration (RMI) with Zr, Si mixed powders as raw materials. The structural evolution and formation mechanism of the C/C–ZrC–SiC composites were discussed, and the mechanical property of the as-prepared material was investigated by compression test. The results showed that after the RMI process, a special structure with ZrC–SiC multi-coating as outer layer and ZrC–SiC–PyC ceramics as inner matrix was formed. ZrC and SiC rich areas were formed in the composites and on the coating surface due to the formation of Zr–Si intermetallic compounds in the RMI process. Mechanical tests showed that the average compression strength of the C/C–ZrC–SiC composites was 133.86 MPa, and the carbon fibers in the composites were not seriously damaged after the RMI process.

Key words: Carbon/carbon composites, Reactive melt infiltration, Coating, ZrC, SiC

Xin Yang, Zhean Su, Qizhong Huang, Xiao Fang, Liyuan Chai. Microstructure and Mechanical Properties of C/CeZrCeSiC Composites Fabricated by Reactive Melt Infiltration with Zr, Si Mixed Powders[J]. J. Mater. Sci. Technol., 2013, 29(8): 702-710.

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Microstructure and Mechanical Properties of C/CeZrCeSiC Composites Fabricated by Reactive Melt Infiltration with Zr, Si Mixed Powders

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