J. Mater. Sci. Technol. ›› 2020, Vol. 37: 114-122.DOI: 10.1016/j.jmst.2019.06.017
• Research Article • Previous Articles Next Articles
Hao Dua*(), Chuanyu Cuiab, Housheng Liuab, Guihong Songc*(), Tianying Xionga
Received:
2019-01-01
Revised:
2019-06-25
Accepted:
2019-06-26
Published:
2020-01-15
Online:
2020-02-10
Contact:
Du Hao,Song Guihong
Hao Du, Chuanyu Cui, Housheng Liu, Guihong Song, Tianying Xiong. Improvement on compressive properties of lotus-type porous copper by a nickel coating on pore walls[J]. J. Mater. Sci. Technol., 2020, 37: 114-122.
Coating thickness (μm) | Average radius of pores (mm) | Half distance between neighbor pores (mm) | Calculated porosity (%) | Measured porosity (%) |
---|---|---|---|---|
0 | 0.2193 | 0.3043 | 47.10 | |
3.9 | 0.2154 | 0.3043 | 45.44 | 45.65 |
4.0 | 0.2153 | 0.3043 | 45.40 | 45.79 |
4.1 | 02152 | 0.3043 | 45.36 | 45.62 |
4.3 | 0.2150 | 0.3043 | 45.27 | 45.51 |
4.4 | 0.2149 | 0.3043 | 45.23 | 45.48 |
4.6 | 0.2147 | 0.3043 | 45.15 | 45.52 |
4.8 | 0.2145 | 0.3043 | 45.06 | 45.42 |
39.0 | 0.1803 | 0.3043 | 31.84 |
Table 1 Effect of coating thickness on the average radius of pores, the half distance between neighbor pores and porosity for the lotus-type porous copper.
Coating thickness (μm) | Average radius of pores (mm) | Half distance between neighbor pores (mm) | Calculated porosity (%) | Measured porosity (%) |
---|---|---|---|---|
0 | 0.2193 | 0.3043 | 47.10 | |
3.9 | 0.2154 | 0.3043 | 45.44 | 45.65 |
4.0 | 0.2153 | 0.3043 | 45.40 | 45.79 |
4.1 | 02152 | 0.3043 | 45.36 | 45.62 |
4.3 | 0.2150 | 0.3043 | 45.27 | 45.51 |
4.4 | 0.2149 | 0.3043 | 45.23 | 45.48 |
4.6 | 0.2147 | 0.3043 | 45.15 | 45.52 |
4.8 | 0.2145 | 0.3043 | 45.06 | 45.42 |
39.0 | 0.1803 | 0.3043 | 31.84 |
Fig. 2. Compressive stress-strain curve between the coated and the uncoated lotus-type porous copper (a) and the magnified part (b) in the strain range to 0.05.
Parameters | Density (g cm-3) | Compressive strength (MPa) | Specific compressive strength (MPa cm3?g-1) | Energy absorption capacity per volume (MJ m-3) | Energy absorption capacity per mass (J g-1) |
---|---|---|---|---|---|
Uncoated | 4.7081 | 22.1?±?2.0 | 4.69?±?0.42 | 48.2?±?3.0 | 10.24?±?0.64 |
Coated-3.9?μm | 4.8372 | 28.2?±?2.8 | 5.83?±?0.58 | 69.1?±?3.7 | 14.29?±?0.76 |
Coated-4.0?μm | 4.8247 | 29.3?±?2.7 | 6.07?±?0.56 | 71.6?±?3.9 | 14.84?±?0.81 |
Coated-4.1 μm | 4.8398 | 28.4?±?2.5 | 5.87?±?0.52 | 69.5?±?3.5 | 14.36?±?0.72 |
Coated-4.3 μm | 4.8496 | 29.4?±?2.8 | 6.06?±?0.58 | 72.2?±?4.0 | 14.89?±?0.82 |
Coated-4.4?μm | 4.8523 | 29.6?±?3.1 | 6.10?±?0.64 | 73.7?±?4.1 | 15.19?±?0.84 |
Coated-4.6 μm | 4.8487 | 28.8?±?2.6 | 5.94?±?0.54 | 70.1?±?3.5 | 14.46?±?0.72 |
Coated-4.8?μm | 4.8576 | 29.2?±?2.9 | 6.01?±?0.60 | 71.3?±?3.9 | 14.68?±?0.80 |
Table 2 Density, compressive strength and energy absorption capacity of both the uncoated and the coated lotus-type porous coppers.
Parameters | Density (g cm-3) | Compressive strength (MPa) | Specific compressive strength (MPa cm3?g-1) | Energy absorption capacity per volume (MJ m-3) | Energy absorption capacity per mass (J g-1) |
---|---|---|---|---|---|
Uncoated | 4.7081 | 22.1?±?2.0 | 4.69?±?0.42 | 48.2?±?3.0 | 10.24?±?0.64 |
Coated-3.9?μm | 4.8372 | 28.2?±?2.8 | 5.83?±?0.58 | 69.1?±?3.7 | 14.29?±?0.76 |
Coated-4.0?μm | 4.8247 | 29.3?±?2.7 | 6.07?±?0.56 | 71.6?±?3.9 | 14.84?±?0.81 |
Coated-4.1 μm | 4.8398 | 28.4?±?2.5 | 5.87?±?0.52 | 69.5?±?3.5 | 14.36?±?0.72 |
Coated-4.3 μm | 4.8496 | 29.4?±?2.8 | 6.06?±?0.58 | 72.2?±?4.0 | 14.89?±?0.82 |
Coated-4.4?μm | 4.8523 | 29.6?±?3.1 | 6.10?±?0.64 | 73.7?±?4.1 | 15.19?±?0.84 |
Coated-4.6 μm | 4.8487 | 28.8?±?2.6 | 5.94?±?0.54 | 70.1?±?3.5 | 14.46?±?0.72 |
Coated-4.8?μm | 4.8576 | 29.2?±?2.9 | 6.01?±?0.60 | 71.3?±?3.9 | 14.68?±?0.80 |
Fig. 3. Relationship between energy absorption per mass (a), energy absorption efficiency (b) and strain for both the uncoated and the coated lotus-type porous copper.
Fig. 4. SEM images of pore walls after being compressed to 20% (a), 40% (c) and 80% (e) of the uncoated porous copper in low magnification and their corresponding high magnification images are shown in (b), (d) and (f), respectively.
Fig. 5. SEM images of pore walls after being compressed to 20% (a), 40% (c) and 80% (e) of the coated porous copper in low magnification and their corresponding high magnification images are shown in (b), (d) and (f, g), respectively.
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