J. Mater. Sci. Technol. ›› 2021, Vol. 75: 96-109.DOI: 10.1016/j.jmst.2020.09.042
• Invited Review • Previous Articles Next Articles
Yanrong Lva, Chao Hana, Ye Zhua, Tianao Zhanga, Shuo Yaoa, Zhangxing Hea,b,*(), Lei Daia,b,*(), Ling Wanga,b,*()
Received:
2020-07-23
Revised:
2020-09-18
Accepted:
2020-09-27
Published:
2020-11-02
Online:
2020-11-02
Contact:
Zhangxing He,Lei Dai,Ling Wang
About author:
tswling@126.com (L. Wang).Yanrong Lv, Chao Han, Ye Zhu, Tianao Zhang, Shuo Yao, Zhangxing He, Lei Dai, Ling Wang. Recent advances in metals and metal oxides as catalysts for vanadium redox flow battery: Properties, structures, and perspectives[J]. J. Mater. Sci. Technol., 2021, 75: 96-109.
Fig. 2. (a) High-resolution transmission electron microscope (TEM) images and particle size histograms, (b) anodic polarization of V(IV) oxidation on different catalysts at different electrode rotating speeds. Reprinted from Ref. [62]. (c) Schematic of the synthesis route for CF-Ir-2, (d) TEM, (e) HR-TEM images of CF-Ir-2, and (f) energy efficiency of the batteries using CF and CF-Ir-2. Reprinted from Ref. [70].
Fig. 3. FESEM images of GFs modified with Sb particles at same magnifications after cycling (a) once charge, (b) once charge and discharge and (c) several cycles, (d) EDX spectrogram of particles on the surface of GFs; (e) electrochemical performance of VRFB using electrolyte with different concentrations of Sb3+ ions. Reprinted from Ref. [77].
Fig. 4. (a) Reaction mechanism of VRFB negative half-cell: on the surface of carbon and bismuth. (b) SEM images of Bi-TTGF and Bi-TTGF after cycling obtained using a secondary electron detector. Reprinted from Ref. [73]. (c) Schematic of the electrode design strategy, (d) different graphite original surface, graphite carbonyl surface schematic diagram and surface adsorption charge difference, SEM images of (e) CC, (f) TCC, (g) BiNP-CC and (h) BiNP-TCC. Reprinted from Ref. [75].
Fig. 5. (a-j) SEM images of various electrodes, (k) EDX analysis image of the selective area of GF, (l) EDX analysis image of the selective area of 0.2 wt.% CeO2/GF, (m) XRD patterns of the GF and CeO2/GF. Reprinted from Ref. [82]. (n) Suggested catalytic mechanism on the Nd2O3-CF electrodes for VO2+/VO2+ redox reaction, (o) mapping EDX on selected image of Nd2O3-CF. Reprinted from Ref. [86].
Fig. 6. (a, b) FESEM images of TiNb2O7-rGO nanocomposites at different magnifications, (c) HRTEM image of TiNb2O7-rGO, (d) wide-scan XPS survey, (e) CV curves of the TiNb2O7, rGO, and TiNb2O7-rGO modified GC electrode. Reprinted from Ref. [98].
Fig. 7. (a) Schematic diagram of redox mechanism of VO2+/VO2+ with Ta2O5 on GF electrode surface, (b, c) SEM images of 0.75 wt.% Ta2O5-GF, (d) high-resolution TEM image and the corresponding selected area electron diffraction (SAED) pattern (the inset). Reprinted from Ref. [102]. (e) STEM image of W-doped Nb2O5 nanorods, (f) corresponding FFT of one atomic resolution image (panel e), (g) distributions of Nb and W elements in one EELS line scan (the line is shown in panel e). Reprinted from Ref. [103].
Fig. 8. (a) Illustration of the electrode preparation, (b) morphologies of HTNW electrodes, (c) XPS for N 1s spectra for HTNW electrodes, (d) Nyquist impedance plots of different carbon felt electrodes, (e) comparison of the electrochemical performance for all as-prepared electrodes, showing the voltage profiles for charge and discharge process at 200 mA cm-2. Reprinted from Ref. [107].
Fig. 9. (a, d) SEM images of CPA-05-30, (b) TEM and (e) high-resolution TEM images of CPA-05-30, cross-sectional view of the water droplet on (c) CP and (f) CPA-05-30, (g, h, i) electrochemical performance of VRFB. Reprinted from Ref. [124].
Fig. 10. (a) Preparation steps of etched graphite (EGF) felt from bare graphite felt (BF) by the redox reaction of NiO/Ni, (b) etching mechanism of graphitic surface by the redox reaction of NiO/Ni, (c) operating-temperature profiles for three cycles of the NiO/Ni redox reaction, (d) SEM images of EGF3. Reprinted from Ref. [127].
Fig. 11. (a) Schematic of the synthesis of SnO2 nanoparticle-deposited CF, (b-e) various magnifications of the SnO2 deposited onto the CF. Reprinted from Ref. [133]. (f) Process diagram of SnO2/Sb modified carbon paper, SEM images of (g) CP, (h) CP-SnO2, and (i) CP-SnO2/Sb. Reprinted from Ref. [136].
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