Catalytic Graphitization of Phenolic Resin

J Mater Sci Technol ›› 2011, Vol. 27 ›› Issue (3): 266-270.

• Regular Papers • Previous Articles Next Articles

Catalytic Graphitization of Phenolic Resin

Mu Zhao^1,2), Huaihe Song¹⁾

1) State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029, China
2) Chinergy Co., Ltd, Beijing 100084, China

Received:2009-10-28 Revised:2010-09-13 Online:2011-03-28 Published:2011-03-21
Contact: Huaihe Song
Supported by:
the National Natural Science Foundation of China (Nos. 50572003 and 50972004) and the State Key Basic Research Program of China (No. 2006CB9326022006)

Abstract

Abstract: The catalytic graphitization of thermal plastic phenolic-formaldehyde resin with the aid of ferric nitrate (FN) was studied in detail. The morphologies and structural features of the products including onion-like carbon nanoparticles and bamboo-shaped carbon nanotubes were investigated by transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), X-ray diffraction and Raman spectroscopy measurements. It was found that with the changes of loading content of FN and residence time at 1000°C, the products exhibited various morphologies. The TEM images showed that bamboo-shaped carbon nan-otube consisted of tens of bamboo sticks and onion-like carbon nanoparticle was made up of quasi-spherically
concentrically closed carbon nanocages.

Key words: Nanostructures, Polymers, Heat treatment

Mu Zhao, Huaihe Song. Catalytic Graphitization of Phenolic Resin[J]. J Mater Sci Technol, 2011, 27(3): 266-270.

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Catalytic Graphitization of Phenolic Resin

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