J Mater Sci Technol ›› 2007, Vol. 23 ›› Issue (03): 407-411.

• Research Articles • Previous Articles     Next Articles

A Novel Route to Prepare Nanocomposites in Larger Scale

Wei WU, Lailong LUO, Guangwen CHU, Shengjun BAI, Haikui ZOU, Jianfeng CHEN   

  1. Key Lab for Nanomaterials, Ministry of Education, Beijing University of Chemical Technology, Beijing 100029, China...
  • Received:2006-05-16 Revised:2006-10-16 Online:2007-05-28 Published:2009-10-10
  • Contact: Jianfeng CHEN

Abstract: A novel route to prepare nanocomposites was illustrated through preparing overbased calcium petroleum sulfonate lubricating oil detergent, where the rotating packed bed (RPB) was used as reactor in place of conventional reaction vessel. The results showed that the carbonation efficiency is improved, the raw materials consumption is reduced, and the dispersibilities, sizes and morphologies of nano-sized CaCO3 particles in overbased detergent are enhanced. It is deduced reasonably that this route can be extensively applied to nanocomposites preparation in appropriate conditions and would be a platform technology in this field.

Key words: Nanocomposite, Preparation, Rotating packed bed, Conventional reaction vessel