J. Mater. Sci. Technol. ›› 2022, Vol. 129: 1-14.DOI: 10.1016/j.jmst.2022.03.029

• Research Article •     Next Articles

Dynamic microstructure evolution and mechanical properties of dilute Mg-Al-Ca-Mn alloy during hot rolling

Shiwei Xua,b,*(), Congcong Zhua,*(), Zhanhong Linc, Chen Jinc, S. Kamadod, K. Oh-ishie, Yun Qinf   

  1. aCollege of Materials Science and Engineering, Hunan University, Changsha 410082, China
    bState Key Laboratory of Advanced Design and Manufacturing for Vehicle Body, Hunan University, Changsha 410082, China
    cQinghai Salt Lake Teli Magnesium Co. Ltd., Xining 810000, China
    dDepartment of Mechanical Engineering, Nagaoka University of Technology, Nagaoka 940-2188, Japan
    eToyota Central R&D Labs., Inc., 41-1 Yokomichi, Nagakute, Aichi 480-1192, Japan
    fResearch Institute (R&D Centre), Baowu Steel Group Corporation, Shanghai 201900, China
  • Received:2021-12-26 Revised:2022-03-02 Accepted:2022-03-02 Published:2022-05-15 Online:2022-05-15
  • Contact: Shiwei Xu,Congcong Zhu
  • About author:congcongzhu@hnu.edu.cn (C.Zhu).
    * E-mail addresses: xushiwei@hnu.edu.cn (S. Xu),

Abstract:

The dynamic microstructure and texture of dilute Mg-0.50Al-0.71Ca-0.33Mn (wt.%) during hot rolling at two slab temperatures were investigated by electron backscattered diffraction (EBSD) and high resolution transmission electron microscopy (HRTEM). The results show that the development of the rolling microstructures is to first form {10-12} extension twins in the original grains, thereby forming the extension-twinned regions, and then to further form {10-11} - {10-12} double twins and kinks in the extension-twinned regions, and finally to form continuous dynamic recrystallized (continuous DRXed) grains in the double twins and the cross parts of the shear-deformed coarse extension-twinned regions. These extension twins, double twins and kinks show a decisive effect on the formation of rolling texture. The number of {10-11} - {10-12} double twins and resultant the continuous DRX process are strongly affected by the rolling slab temperature and the reduction thickness per pass. By optimizing the rolling conditions, texture and microstructures of the multi-pass rolled Mg-Al-Ca-Mn alloy sheets are successfully modified. Although the total alloy content is only 1.5 wt.%, these Mg-Al-Ca-Mn alloy sheets show much higher strength than the commercial Mg-3Al-1 Zn (wt.%) (AZ31B) sheet.

Key words: Mg-Al-Ca-Mn alloy, Hot rolling, Dynamic recrystallization, Texture control, Mechanical properties