J. Mater. Sci. Technol. ›› 2021, Vol. 67: 197-210.DOI: 10.1016/j.jmst.2020.06.038
• Research article • Previous Articles Next Articles
A.C. Boualia,*(), N.M. Andréb, M.R. Silva Camposa, M. Serdechnovaa, J.F. dos Santosb, S.T. Amancio-Filhoc, M.L. Zheludkevicha,d
Received:
2020-05-09
Revised:
2020-06-29
Accepted:
2020-06-30
Published:
2021-03-20
Online:
2021-04-15
Contact:
A.C. Bouali
About author:
* E-mail address: anissa.bouali@hzg.de (A.C. Bouali).A.C. Bouali, N.M. André, M.R. Silva Campos, M. Serdechnova, J.F. dos Santos, S.T. Amancio-Filho, M.L. Zheludkevich. Influence of LDH conversion coatings on the adhesion and corrosion protection of friction spot-joined AA2024-T3/CF-PPS[J]. J. Mater. Sci. Technol., 2021, 67: 197-210.
Fig. 1. (A) Tool used to produce the samples (dimensions in mm), (B) Steps of the FSpJ process: (a) overlapping of parts and tool, (b) plunging of the sleeve into the metal, (c) keyhole refilling with plasticized metal, and (d) joint consolidation (Adapted from [40]), (C) dimension of the final joint.
Fig. 4. Galvanic corrosion measurements of the galvanic couple AA2024-T3/CF-PPS at different conditions; representing the current density (a) and mixed potential (b) between AA2024-T3 and CF-PPS when exposed to 0.5% NaCl, 0.5% NaCl + 10-3 M NaNO3 and 0.5% NaCl + 10-3 M NaVO3.
Fig. 5. (a) Optical micrograph of the cell at t = 0; SVET maps of the coupled system (AA2024-T3/CFRP) after 2 h and 12 h immersion followed by an optical micrograph of the cell at the different solutions of 0.05 M NaCl (b), 0.05 M NaCl + 10-3 M NaNO3 (c) and 0.05 M NaCl + 10-3 M NaVO3 (d).
Fig. 6. ZRA measurement representing the current density (a) and the mixed potential (b) between the reference AA2024-T3, AA2024-T3-LDH-N and AA2024-T3-LDH-V when coupled with CF-PPS and exposed to 0.5% NaCl solution.
Fig. 8. Photographs of the top surface of the bonding area with definition of the main microstructural zones produced by the FSpJ process on the AA2024-T3 part (a), reference without any treatment (b), treated with LDH-NO3 (c) and treated with LDH-VOx (d).
Samples | Before SST (%) | 3 week SST (%) | 6 week SST (%) |
---|---|---|---|
LDH-NO3 | 19.66 | 42.79 | 36.75 |
LDH-VOx | 24.55 | 16.79 | -6.75 |
Table 1 Percentage of improvement of the average ULSF in comparison to the reference joint AA2024-T3/CF-PPS.
Samples | Before SST (%) | 3 week SST (%) | 6 week SST (%) |
---|---|---|---|
LDH-NO3 | 19.66 | 42.79 | 36.75 |
LDH-VOx | 24.55 | 16.79 | -6.75 |
Fig. 10. Photographs of the bonding zone for the couple (metal part on the left and CF-PPS on the right) after separation by lap shear tensile test with; (a) delimitation of the borders between the main regions defining the FSpJ process [39]; (b) the reference couple AA2024-T3/ CF-PPS, (c) AA2024-T3-LDH-N/ CF-PPS and (d) AA2024-T3-LDH-V/ CF-PPS, before SST and after 3 and 6 weeks of SST.
Fig. 11. SEM fracture analysis of a region of the PDZ on the AA2024-T3 part of the joints with (a) reference AA2024-T3, (b) AA2024-T3-LDH-N, (c) AA2024-T3-LDH-V before SST; and (d) reference AA2024-T3, (e) AA2024-T3-LDH-N and (f) AA2024-T3-LDH-V after 6 weeks of SST.
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