J. Mater. Sci. Technol. ›› 2022, Vol. 113: 1-13.DOI: 10.1016/j.jmst.2021.09.011

• Research article •     Next Articles

Effect of cooling rate following β forging on texture evolution and variant selection during β → α transformation in Ti-55511 alloy

Yue Donga, Xingang Liua,*(), Junjie Zoua, Yujiao Kea, Pengwei Liua, Lan Mab, Hengjun Luoc   

  1. aCollege of Mechanical Engineering, Yanshan University, Qinhuangdao 066004, China
    bOxford Instruments (Shanghai) Co., Ltd., No.461, Hongcao Road, Shanghai 200233, China
    cDeyang Wanhang Die Forging Co., Ltd., China National Erzhong Group Co., Deyang 618000, China
  • Received:2021-06-16 Revised:2021-09-25 Accepted:2021-09-26 Published:2021-12-29 Online:2022-06-24
  • Contact: Xingang Liu
  • About author:*E-mail address: lxg@ysu.edu.cn (X. Liu).

Abstract:

The control of the post-forging cooling rate has been a key issue in the industrial production process of titanium alloys. We investigated texture evolution and variant selection (VS) during β → α transformation through high-temperature compression experiments followed by quantitative control of varying cooling rates. Results show that post-forging cooling rates affect β grains, α variants, and α / β textures. The α precipitation inhibits motions of β static recrystallization (βSRX) grain boundaries and thus leads to grain refining from 0.1 °C/s to 0.05 °C/s. Further analysis reveals that lamellae grain boundary widmanstatten α (αWGB) keeps growing rapidly within β-grain in an interface instability manner at 0.1-0.05 °C/s. Most of α-phase with 50°-60°/<-12-10> is preferentially precipitated at β-medium angle GBs between 30° and 45° and strictly follows BOR with the side of of adjacent β-grain with the same or similar {110} or {111}. Moreover, the texture type transforms gradually from RGoss {110} <1-10> to Brass {110} <1-12> from 25 °C/s to 1 °C/s. βSRX grains exhibit (102) [-201] texture, while the corresponding α has textures of <0001>//Z and <11-20>//Y from 1 °C/s to 0.05 °C/s. Our findings lay a profound theoretical foundation in microstructure evolution of near-β titanium alloy for industrial production.

Key words: Ti-55511 alloy, Cooling rate, Texture evolution, Phase transformation, Variant selection (VS)