Preparation and Characterization of Nano-silver Loaded Montmorillonite with Strong Antibacterial Activity and Slow Release Property

J Mater Sci Technol ›› 2011, Vol. 27 ›› Issue (8): 685-690.

• Novel Processing and Characterization Methods • Previous Articles Next Articles

Preparation and Characterization of Nano-silver Loaded Montmorillonite with Strong Antibacterial Activity and Slow Release Property

Guangnian Xu¹⁾, Xueliang Qiao²⁾, Xiaolin Qiu³⁾, Jianguo Chen²⁾

1) Anhui Provincial Laboratory of Biomimetic Sensing and Detection Technology, West Anhui University, Liuan 237012, China
2) State Key Laboratory of Material Processing and Die & Mould Technology, Huazhong University of Science and Technology, Wuhan 430074, China
3) Nanomaterials Research Center, Nanchang Institute of Technology, Nanchang 330013, China

Received:2009-07-24 Revised:2009-11-13 Online:2011-08-30 Published:2011-08-30
Contact: Guangnian Xu

Abstract

Abstract: Nano-silver loaded montmorillonite (Ag-MMT) was prepared by ion-exchange and then a UV-photoreduction two-step approach was applied. The silver content in Ag-MMT determined by Volhard method was about 6.4 wt%. The morphology and structure of as-synthesized Ag-MMT were characterized by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results showed that the Ag nanoparticles were spherical and their diameters were about 15−20 nm. Moreover, the structure of MMT did not change. The minimum inhibition concentration (MIC) of Ag-MMT was 100×10^-6 and the sterilizing efficiency (SE) of Ag-MMT was approximately 100% against Escherichia coli ATCC 11229 (E. coli). In addition, the slow release property of silver in Ag-MMT was also demonstrated.

Key words: Silver loaded montmorillonite, Photoreduction, Antibacterial activity, Slow release property

Guangnian Xu, Xueliang Qiao, Xiaolin Qiu, Jianguo Chen. Preparation and Characterization of Nano-silver Loaded Montmorillonite with Strong Antibacterial Activity and Slow Release Property[J]. J Mater Sci Technol, 2011, 27(8): 685-690.

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Preparation and Characterization of Nano-silver Loaded Montmorillonite with Strong Antibacterial Activity and Slow Release Property

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