J. Mater. Sci. Technol. ›› 2023, Vol. 166: 47-57.DOI: 10.1016/j.jmst.2023.04.055

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Homogenization on solution treatment and its effects on the precipitation-hardening of selective laser melted 17-4PH stainless steel

Sohee Ana,du-Rim Eob, Il Sohna,*, Kyunsuk Choic,*   

  1. aDepartment of Materials Science and Engineering, Yonsei University, Seoul, 03722, Republic of Korea;
    bAdvanced Joining & Additive Manufacturing R&D Department, Korea Institute of Industrial Technology (KITECH), 529 Seohaean-ro, Siheung 15014, Republic of Korea;
    cDepartment of Industry-University Convergence, Hanbat National University, Yuseong, Daejeon, 34158, Republic of Korea
  • Received:2023-01-30 Revised:2023-04-08 Accepted:2023-04-28 Published:2023-12-10 Online:2023-12-06
  • Contact: *E-mail addresses: ilsohn@yonsei.ac.kr (I. Sohn), kschoi@hanbat.ac.kr (K. Choi).

Abstract: 17-4 precipitation-hardened (PH) stainless steel (SS) exhibits high strength and good corrosion resistance via Cu-precipitation hardening. Unlike conventional wrought 17-4PH SS, Cu segregation and ε-Cu pre-cipitates are observed in additively manufactured (AM) 17-4PH SS owing to the repeated rapid cooling after heating, which characterizes the AM process. In this study, solution treatment was conducted under various temperatures (1,000, 1,050, 1,100, and 1,200 °C) and durations (1, 2, 4, and 8 h) to minimize the negative effects of Cu segregation and ε-Cu precipitates on precipitation hardening. The mechanical prop-erties and microstructures of each condition for the Cu precipitation behavior were examined. Although the ε-Cu precipitates did not disappear after solution treatment, the average diameter of the ε-Cu precipi-tates tended to decrease with increasing solution treatment temperature and duration. Therefore, solution treatment at a temperature of 1,200 °C for 8 h was the best, resulting in improved strength compared to the conventional solution treatment at 1,050 °C. Solution treatment on at least 1,100 °C is effective in AM.

Key words: Selective laser melting, Cu segregation, Solution treatment, 17-4 Precipitation-hardened stainless steel, Additive manufacturing