Impact of severe plastic deformation on kinetics and thermodynamics of hydrogen storage in magnesium and its alloys

doi:10.1016/j.jmst.2022.10.068

J. Mater. Sci. Technol. ›› 2023, Vol. 146: 221-239.DOI: 10.1016/j.jmst.2022.10.068

• Research Article • Previous Articles Next Articles

Impact of severe plastic deformation on kinetics and thermodynamics of hydrogen storage in magnesium and its alloys

Kaveh Edalati^a,*, Etsuo Akiba^b, Walter J. Botta^c, Yuri Estrin^d,e, Ricardo Floriano^f, Daniel Fruchart^g,h, Thierry Grosdidier^i,j, Zenji Horita^a,k,l,m, Jacques Huotⁿ, Hai-Wen Li^o, Huai-Jun Lin^p, Ádám Révész^q, Michael J. Zehetbauer^r

^aWPI, International Institute for Carbon-Neutral Energy Research (WPI-I2CNER), Kyushu University, Fukuoka, Japan;
^bInternational Research Center for Hydrogen Energy, Kyushu University, Fukuoka, Japan;
^cDepartamento de Engenharia de Materiais, Universidade Federal de São Carlos, Sao Carlos-SP, Brazil;
^dDepartment of Materials Science and Engineering, Monash University, Clayton, VIC 3800, Australia;
^eDepartment of Mechanical Engineering, the University of Western Australia, Crawley, WA 6009, Australia;
^fSchool of Applied Sciences, University of Campinas (UNICAMP), Limeira, São Paulo, Brazil;
^gInstitut Néel, CNRS & UGA, 38042 Grenoble, France;
^hJOMI-LEMAN SA, 74890 Fessy, France;
ⁱUniversitéde Lorraine, Laboratory of Excellence on Design of Alloy Metals for low-mass Structures (DAMAS), Metz, F-57070, France;
^jUniversitéde Lorraine, Laboratoire d’Etude des Microstructures et de Mécanique des Matériaux (LEM3 UMR 7239), Metz, F-57070, France;
^kGraduate School of Engineering, Kyushu Institute of Technology, Kitakyushu, Japan;
^lMagnesium Research Center, Kumamoto University, Kumamoto, Japan;
^mSynchrotron Light Application Center, Saga University, Saga, Japan;
ⁿHydrogen Research Institute, Universitédu Québec àTrois-Rivières, 3351 des Forges, Trois-Rivières, QCG9A5H7, Canada;
^oHefei General Machinery Research Institute, Hefei 230031, China;
^pInstitute of Advanced Wear & Corrosion Resistance and Functional Materials, Jinan University, Guangzhou 510632, China;
^qDepartment of Materials Physics, Eötvös University, Budapest, H-1518, P.O.B.32, Budapest, Hungary;
^rFaculty of Physics, University of Vienna, Boltzmanngasse 5, A-1090 Wien, Austria

Received:2022-08-11 Revised:2022-10-16 Accepted:2022-10-19 Published:2023-05-20 Online:2023-05-15
Contact: * E-mail address: kaveh.edalati@kyudai.jp (K. Edalati)

Abstract

Abstract: Magnesium and its alloys are the most investigated materials for solid-state hydrogen storage in the form of metal hydrides, but there are still unresolved problems with the kinetics and thermodynamics of hydrogenation and dehydrogenation of this group of materials. Severe plastic deformation (SPD) methods, such as equal-channel angular pressing (ECAP), high-pressure torsion (HPT), intensive rolling, and fast forging, have been widely used to enhance the activation, air resistance, and hydrogenation/dehydrogenation kinetics of Mg-based hydrogen storage materials by introducing ultrafine/nanoscale grains and crystal lattice defects. These severely deformed materials, particularly in the presence of alloying additives or second-phase nanoparticles, can show not only fast hydrogen absorption/desorption kinetics but also good cycling stability. It was shown that some materials that are apparently inert to hydrogen can absorb hydrogen after SPD processing. Moreover, the SPD methods were effectively used for hydrogen binding-energy engineering and synthesizing new magnesium alloys with low thermodynamic stability for reversible low/room-temperature hydrogen storage, such as nanoglasses, high-entropy alloys, and metastable phases including the high-pressure γ-MgH₂ polymorph. This work reviews recent advances in the development of Mg-based hydrogen storage materials by SPD processing and discusses their potential in future applications.

Key words: Severe plastic deformation (SPD), Nanostructured materials, Ultrafine-grained (UFG) materials, Magnesium hydride (MgH₂), Magnesium-based alloys, Hydrogen absorption, Hydrogenation kinetics, Hydrogen storage thermodynamics

Kaveh Edalati, Etsuo Akiba, Walter J. Botta, Yuri Estrin, Ricardo Floriano, Daniel Fruchart, Thierry Grosdidier, Zenji Horita, Jacques Huot, Hai-Wen Li, Huai-Jun Lin, Ádám Révész, Michael J. Zehetbauer. Impact of severe plastic deformation on kinetics and thermodynamics of hydrogen storage in magnesium and its alloys[J]. J. Mater. Sci. Technol., 2023, 146: 221-239.

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Impact of severe plastic deformation on kinetics and thermodynamics of hydrogen storage in magnesium and its alloys

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[2]	P.-C. Zhao, B. Guan, Y.-G. Tong, R.-Z. Wang, X. Li, X.-C. Zhang, S.-T Tu. A quasi-in-situ EBSD study of the thermal stability and grain growth mechanisms of CoCrNi medium entropy alloy with gradient-nanograined structure [J]. J. Mater. Sci. Technol., 2022, 109(0): 54-63.
[3]	Yifan Dong, Shuolei Deng, Ziting Ma, Ge Yin, Changgang Li, Xunlong Yuan, Huiyun Tan, Jing Pan, Liqiang Mai, Fan Xia. Sodium vanadium oxides: From nanostructured design to high-performance energy storage materials [J]. J. Mater. Sci. Technol., 2022, 121(0): 80-92.
[4]	H. Zhou, H.Y. Ning, X.L. Ma, D.D. Yin, L.R. Xiao, X.C. Sha, Y.D. Yu, Q.D. Wang, Y.S. Li. Microstructural evolution and mechanical properties of Mg-9.8Gd-2.7Y-0.4Zr alloy produced by repetitive upsetting [J]. J. Mater. Sci. Technol., 2018, 34(7): 1067-1075.
[5]	Opra Denis P., Gnedenkov Sergey V., Sinebryukhov Sergey L., Voit Elena I., Sokolov AlexanderA., Modin Evgeny B., Podgorbunsky Anatoly B., Sushkov Yury V., Zheleznov Veniamin V.. Characterization and Electrochemical Properties of Nanostructured Zr-Doped Anatase TiO₂ Tubes Synthesized by Sol-Gel Template Route [J]. J. Mater. Sci. Technol., 2017, 33(6): 527-534.
[6]	Han X.B.,Qian Y.,Liu W.,Chen D.M.,Yang K.. Effect of Preparation Technique on Microstructure and Hydrogen Storage Properties of LaNi_3.8Al_1.0Mn_0.2 Alloys [J]. J. Mater. Sci. Technol., 2016, 32(12): 1332-1338.
[7]	V.M. Nadutov, A.I. Ustinov, S.A. Demchenkov, Ye.O. Svystunov, V.S. Skorodzievski. Structure and Properties of Nanostructured Vacuum-Deposited Foils of Invar Fe-(35-38 wt%)Ni Alloys [J]. J. Mater. Sci. Technol., 2015, 31(11): 1079-1086.
[8]	S.N. Hosseini, T. Mousavi, F. Karimzadehy and M.H. Enayati. Thermodynamic Aspects of Nanostructured CoAl Intermetallic Compound during Mechanical Alloying [J]. J Mater Sci Technol, 2011, 27(7): 601-606.
[9]	X. He, Z.H. Wang, D.Y. Geng, Z.D. Zhang. Structure and Magnetic Properties of S-doped Mn₃O₄/S Composited Nanoparticles and Mn₃O₄ Nanoparticles [J]. J Mater Sci Technol, 2011, 27(6): 503-506.
[10]	Xiao Si,Bining Lu,Zhenbo Wang. Aluminizing Low Carbon Steel at Lower Temperatures [J]. J Mater Sci Technol, 2009, 25(04): 433-436.
[11]	Xiao Tang,Yuzhi Zhang,Meng Liu,Yan Li. Boundary Element Method (BEM) Analysis for Galvanic Corrosion of Hot Dip Galvanized Steel Immersed in Seawater [J]. J Mater Sci Technol, 2009, 25(02): 194-198.
[12]	G.X.Wang, Steve Bewlay, L.Yang, J.Z.Wang, Y.Chen, Jane Yao, H.K.Liu, S.X.Dou. Nanostructured Electrode Materials for Rechargeable Lithium-ion Battery Applications [J]. J Mater Sci Technol, 2005, 21(Supl.1): 17-19.
[13]	Wenge CHEN, Zhanying KANG, Bingjun DING. Preparation and Arc Breakdown Behavior of Nanocrystalline W-Cu Electrical Contact Materials [J]. J Mater Sci Technol, 2005, 21(06): 875-878.