J. Mater. Sci. Technol. ›› 2022, Vol. 124: 76-85.DOI: 10.1016/j.jmst.2022.01.028
• Research Article • Previous Articles Next Articles
Yuanting Xua,1, Wanting Lina,b,1, Dandan Yuana, Shifan Chena, Fang Lia, Yanping Longa, Chao Hea, Weifeng Zhaoa,*(
), Changsheng Zhaoa,c,d,*()
Received:2021-10-11
Revised:2022-01-10
Accepted:2022-01-16
Published:2022-10-10
Online:2022-04-04
Contact:
Weifeng Zhao,Changsheng Zhao
About author:zhaochsh70@163.com (C. Zhao).Yuanting Xu, Wanting Lin, Dandan Yuan, Shifan Chen, Fang Li, Yanping Long, Chao He, Weifeng Zhao, Changsheng Zhao. “1+1>2”: Highly efficient removal of organic pollutants by composite nanofibrous membrane based on the synergistic effect of adsorption and photocatalysis[J]. J. Mater. Sci. Technol., 2022, 124: 76-85.
Fig. 1. (a) Schematic illustration of the fabrication process of the BAM nanofibrous membrane, corresponding optical image (b), SEM image (c) and TEM image (d) of BAM nanofibrous membrane.
| Samples | Polyethersulfone (wt%) | p(MMA-AA) copolymer (wt%) | B-C3N4(wt%) |
|---|---|---|---|
| PES | 19 | 0 | 0 |
| BCN | 19 | 0 | 1.9 |
| AM | 19 | 1.9 | 0 |
| BAM | 19 | 1.9 | 1.9 |
Table 1. Recipes of different precursor solutions for nanofibrous membrane fabrication.
| Samples | Polyethersulfone (wt%) | p(MMA-AA) copolymer (wt%) | B-C3N4(wt%) |
|---|---|---|---|
| PES | 19 | 0 | 0 |
| BCN | 19 | 0 | 1.9 |
| AM | 19 | 1.9 | 0 |
| BAM | 19 | 1.9 | 1.9 |
Fig. 2. FTIR spectra (a), TGA curves (b) and DTG curves (c) of the nanofibrous membranes.
Fig. 3. Surface zeta potentials (a), UV-vis diffuse reflectance absorption spectra (b) and plots of transformed Kubelka-Munk function versus photon energy (c) of the nanofibrous membranes.
Fig. 4. (a) Removal efficiency of RhB by the nanofibrous membranes under visible light irradiation, (b) the corresponding kinetics analysis, (c) adsorption-photocatalytic degradation performance of RhB by the nanofibrous membranes, (d) the UV-vis spectra of RhB solution contacting with BAM in dark and under visible light irradiation, (e) images of BAM membrane and RhB dye solutions before adsorption, after adsorption and after photocatalysis, (f) removal efficiency of RhB by BAM as well as the combination of AM and BCN with different mass.
Fig. 5. (a) Photocatalytic degradation of RhB by the BAM sample during 5 cycles, (b) adsorption-degradation performance of RhB by the BAM sample during 5 cycles, (c) schematic diagram of photocatalytic degradation for recycling under visible light irradiation, (d) SEM image of BAM membrane after 5 cycles, (e) FTIR spectra of BAM membrane before adsorption, after adsorption, after photocatalysis and after 5 cycles.
Fig. 6. (a) Removal efficiency of different organic dyes by BAM, (b) chemical structures of RhB, MB, MG, ST and MV dyes, (c) images of BAM membrane and RhB/MB/MG ternary mixture solution before being mixed and after photocatalysis, (d) UV-vis spectra of RhB/MB/MG ternary mixture at different stages, (e) images of BAM membrane and RhB/MB/MG/ST quaternary mixture solution before mixed and after photocatalysis, (f) UV-vis spectra of RhB/MB/MG/ST quaternary mixture solution at different stages.
Fig. 7. (a) Effect of trapping agents on removal efficiency of RhB by BAM under visible light irradiation, (b) DMPO spin-trapping EPR spectra in methyl alcohol solutions with BAM under visible light irradiation, (c) the proposed mechanism of photocatalytic degrading pollutants in the presence of BAM under visible light irradiation.
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