J. Mater. Sci. Technol. ›› 2020, Vol. 45: 157-161.DOI: 10.1016/j.jmst.2019.10.035
• Research Article • Previous Articles Next Articles
W. Zhaia, L.H. Niea, X.D. Huib, Y. Xiaoa, T. Wangb, B. Weia,*()
Received:
2019-08-12
Revised:
2019-09-10
Accepted:
2019-10-12
Published:
2020-05-15
Online:
2020-05-27
Contact:
B. Wei
W. Zhai, L.H. Nie, X.D. Hui, Y. Xiao, T. Wang, B. Wei. Ultrasonic excitation induced nanocrystallization and toughening of Zr46.75Cu46.75Al6.5 bulk metallic glass[J]. J. Mater. Sci. Technol., 2020, 45: 157-161.
Fig. 1. XRD and DSC analyses of the as-cast and ultrasound-processed Zr46.75Cu46.75Al6.5 BMG samples: (a) XRD patterns; (b) DSC traces on heating in temperature range from 500 to 850 K.
Fig. 2. Microstructures of Zr46.75Cu46.75Al6.5 BMG: (a) TEM and (b) HRTEM images for the as-cast sample; (c) TEM and (d) HRTEM images for the UST-2 h sample. The insets of (a) and (c) show the corresponding SAED patterns; (e) HRTEM image showing nanocrystals embedded in amorphous matrix; (f) Fast Fourier Transformation (FFT) pattern of yellow frame area in (e).
Fig. 3. Effects of ultrasound excitation on the macroscopic mechanical behavior of Zr46.75Cu46.75Al6.5 BMG: (a) strain-stress curves in quasi-static compression test; SEM views of the fracture surface appearance for (b) the as-cast sample with primary shear bands and (c) the UST-2 h sample with multiple shear bands.
Fig. 4. Nanoindentation tests on Zr46.75Cu46.75Al6.5 BMG: (a) typical nanoindentation load-displacement curves of the samples in as-cast state and subjected to ultrasonic vibration; (b) cumulative distributions of the critical load at the first pop-in event.
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