J. Mater. Sci. Technol. ›› 2024, Vol. 192: 28-41.DOI: 10.1016/j.jmst.2023.12.023

• Research Article • Previous Articles     Next Articles

Principle and in-situ observation on discrete solidification

Xiaoping Maa, Dianzhong Lia,*, Zhuo Zhaob, Hongwei Liua, Yanfei Caoa, Paixian Fua, Pei Wanga   

  1. aShenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China;
    bDepartment of Materials Science and Engineering, University of Science and Technology Liaoning, Anshan 114051, China
  • Received:2023-09-22 Revised:2023-12-04 Accepted:2023-12-06 Published:2024-09-01 Online:2024-01-20
  • Contact: * E-mail address: dzli@imr.ac.cn (D. Li).

Abstract: Solidification is an important branch of material science. By model calculation and in-situ observation in this work, distinct from traditional solidification of continuous solid growth, the evolution of discrete solidification was investigated, and a new principle for discrete solidification is established based on segregation evolution in a semi-solid matrix. The solidification evolution of Al-2 wt.%Cu alloy was investigated by model calculation under different initial undercooling and cooling rates, under superimposed multi-scale temperature fluctuations, and under variable temperature fluctuations. The initiation and propagation of segregation fluctuations in semi-solid matrix were verified within a traditional dendritic arm. The alternate solid elements evolved from semi-solid matrix act as periodic dams inhibiting serious segregation. Based on the new solidification principle, a multi-scale dendritic pattern was reproduced in a two-dimensional calculation. The new solidification principle reveals the essence of multi-scale microstructures as multi-scale segregation patterns and highlights the feasibility of controlling multi-scale microstructures and segregations.

Key words: Solidification principle, Dendrite, Segregation, Semi-solid matrix