J. Mater. Sci. Technol. ›› 2025, Vol. 229: 177-195.DOI: 10.1016/j.jmst.2024.12.048

• Research article • Previous Articles     Next Articles

Anomalous temperature-dependent strength and the operative slip modes in an extruded Mg-Y sheet

Yingbo Zhanga, Ran Nia, Carl J. Boehlertb, Bo Chena, Yanqin Chaia, Bo Gaoc, Hao Zhoud, Qudong Wange, Dongdi Yina,*   

  1. aKey Laboratory of Advanced Technologies of Materials, Ministry of Education, School of Materials Science and Engineering, Southwest Jiaotong University, Chengdu 610031, China;
    bDepartment of Chemical Engineering and Materials Science, Michigan State University, East Lansing, MI 48824, USA;
    cNano and Heterogeneous Materials Center, School of Materials Science and Engineering, Nanjing University of Science and Technology, Nanjing 210094, China;
    dInstitute of Materials Plainification, Liaoning Academy of Materials, Shenyang 110167, China;
    eNational Engineering Research Center of Light Alloys Net Forming and State Key Laboratory of Metal Matrix Composites, School of Materials Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240, China
  • Received:2024-11-18 Revised:2024-12-30 Accepted:2024-12-31 Published:2025-09-10 Online:2025-02-19
  • Contact: *E-mail address: ahnydd@swjtu.edu.cn (D. Yin).

Abstract: This work is intended to further understand the controversial temperature dependencies of various slip modes in Mg alloys, and their effects on the mechanical properties at high temperature (HT). A system-atical and statistical investigation on the temperature-dependent macroscopic deformation behavior and the corresponding grain-scale slip activity was performed for both an extruded Mg-10Y (wt.%) sheet and a pure Mg sheet during tension at 25-300 ℃. The alloy's strength increased by up to 44 MPa (14.0 %) at HT compared to that at 25 ℃ and this was accompanied by decreased pyramidal II ❬c + a❭ slip activ-ity; both phenomena were opposite to that for pure Mg. The critical resolved shear stress (CRSS) ratios were estimated based on the ~1700 sets of observed slip traces, and a positive temperature-dependent CRSSpyr II /CRSSbas was found in Mg-10Y. Compared to pure Mg, Mg-10Y exhibited pronounced strain hard-ening at HT due to enhanced slip-slip interactions, including multiple slip and cross slip, increased GND accumulation, and Y solute-dislocation interactions. The significant pyramidal II ❬c + a❭ slip activity (up to 30 % frequency), its thermal hardening and pronounced strain hardening nature are proposed to be the key reasons for the observed anomalous strength increase in Mg-10Y. The grain-scale experimental evidence for ❬c + a❭ dislocation activity and its correlation to mechanical properties were revealed in this study and compared to recent atomic-scale simulations.

Key words: Mg-RE alloy, Anomalous temperature dependency CRSS, Slip trace analysis, Pyramidal ❬c + a❭slip