C-doped BiOCl/Bi2S3 heterojunction for highly efficient photoelectrochemical detection and photocatalytic reduction of Cr(VI)

doi:10.1016/j.jmst.2023.03.066

Abstract

Abstract: Novel C-BiOCl/Bi₂S₃ composites are prepared by hydrothermal C doping in BiOCl and in-situ growth of Bi₂S₃ on C-BiOCl. Compared with BiOCl, C-BiOCl has a larger exposed surface area and can effectively absorb visible light. The construction of a heterojunction in C-BiOCl/Bi₂S₃ further promotes the separation and transfer of photogenerated carriers. With improved photoelectric properties, the optimized 5C-BiOCl/5Bi₂S₃ is applied as a dual-functional composite for photoelectrochemical (PEC) detection and photocatalytic (PC) reduction of Cr(VI). The 5C-BiOCl/5Bi₂S₃ shows a linear range of 0.02-80 μM for PEC cathodic detection of Cr(VI) with a detection limit of 0.01628 μM. Additionally, 99.5% of Cr(VI) can be removed via absorption and PC reduction by 5C-BiOCl/5Bi₂S₃, with the reduction rate constant (k) 336 times higher than that of BiOCl.

Key words: C-BiOCl/Bi2S3, Dual-functional, Photoelectrochemical detection, Photocatalytic reduction, Cr(VI)

Chunli Wang, Nazhen Liu, Xia Zhao, Yong Tian, Xuwei Chen, Yanfeng Zhang, Liang Fan, Baorong Hou. C-doped BiOCl/Bi₂S₃ heterojunction for highly efficient photoelectrochemical detection and photocatalytic reduction of Cr(VI)[J]. J. Mater. Sci. Technol., 2023, 164: 188-197.

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C-doped BiOCl/Bi₂S₃ heterojunction for highly efficient photoelectrochemical detection and photocatalytic reduction of Cr(VI)

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