J. Mater. Sci. Technol. ›› 2025, Vol. 231: 180-192.DOI: 10.1016/j.jmst.2024.12.066

• Research article • Previous Articles     Next Articles

Effect of low-energy pulse current on the microstructure and properties of a Ni-based superalloy

Jinchao Maa,b, Jingdong Guoa,*, Jide Liub,*, Xinyi Luob,c, Zhipeng Zhangb,d, Tao Zhange,f, Jiacheng Yana,b,c, Mingkui Zhanga,e, Chuanyong Cuib, Xinfang Zhange,f, Yizhou Zhoub, Jinguo Lib   

  1. aShenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China;
    bShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China;
    cSchool of Materials Science and Engineering, Shenyang University of Technology, Shenyang 110870, China;
    dKey Laboratory for Anisotropy and Texture of Materials (MOE), School of Materials Science and Engineering, Northeastern University, Shenyang 110819, China;
    eSchool of Metallurgical and Ecological Engineering, University of Science and Technology Beijing, Beijing 100083, China;
    fKey Laboratory of Green Extraction & Efficient Utilization of Light Rare-Earth Resources (Inner Mongolia University of Science and Technology), Ministry of Education, School of Rare Earth Industry, Baotou 014010, China
  • Received:2024-08-21 Revised:2024-12-16 Accepted:2024-12-23 Published:2025-10-01 Online:2025-02-26
  • Contact: *E-mail addresses: jdguo@imr.ac.cn (J. Guo), jdliu@imr.ac.cn (J. Liu).

Abstract: This study proposes a low-energy pulse current (LEPC) rapid solution treatment method, which can dissolve more primary γ′ phase in a shorter time and effectively suppress abnormal grain growth, thereby successfully achieving microstructure optimization and property enhancement. The microstructure analysis showed that, compared with the 62.5 % dissolution rate of the standard traditional solution treatment (1100 ℃/4 h), LEPC achieved an 88.9 % dissolution of the primary γ′ phase in just 5 min at the same temperature. Furthermore, due to the rapidity of the LEPC treatment and its “targeted dissolution effect” on the γ′ phase, excessive grain growth was effectively suppressed, resulting in grain size comparable to those obtained with traditional solution treatment. Mechanical property testing indicated that the alloy treated with LEPC had a hardness of 531 HV at room temperature, while the yield strength, Ultimate strength, and maximum strain reached 994 MPa, 1030 MPa, and 5.1 % at the service temperature (750 °C). Compared to the standard traditional solution treatment, these properties were improved by 10.4 %, 11.1 %, 10.4 %, and 17.5 %, respectively. Finally, theoretical calculations revealed that the non-thermal effect of LEPC reduced the dissolution-free energy by approximately 49.4 kJ/mol and increased the diffusion coefficient by about 76 times, which was the fundamental reason for the accelerated dissolution of the primary γ' phase.

Key words: Low-energy pulse current, Solution treatment, Primary γ′ phase, Targeted dissolution effect, Microstructure, Property