Tailoring the morphology and charge transfer pathways of ultrathin Cd0.8Zn0.2S nanosheets via ionic liquid-modified Ti3C2 MXenes towards remarkable photocatalytic hydrogen evolution

doi:10.1016/j.jmst.2024.03.025

Abstract

Abstract: Small-sized Cd_xZn_1-_xS solid solution nanomaterial is an important candidate for efficient photocatalytic hydrogen evolution (PHE), but it still suffers from easy agglomeration, severe photo corrosion, and fast photogenerated electron-hole recombination. To tackle these issues, herein, we propose a new strategy to modify Cd_xZn_1-_xS nanoreactors by the simultaneous utilization of ionic-liquid)-assisted morphology engineering and MXene-incorporating method. That is, we designed and synthesized a novel hierarchical Cd_0.8Zn_0.2S/Ti₃C₂ Schottky junction composite through the in-situ deposition of ultrathin Cd_0.8Zn_0.2S nanosheets on unique IL-modified Ti₃C₂ MXenes by a one-pot solvothermal method for efficiently PHE. The unique construction strategy tailors the thickness of ultrathin Cd_0.8Zn_0.2S nanosheets and prevents them from stacking and agglomeration, and especially, optimizes their charge transfer pathways during the photocatalytic process. Compared with pristine Cd_0.8Zn_0.2S nanosheets, Cd_0.8Zn_0.2S/Ti₃C₂ has abundant photogenerated electrons available on the Ti₃C₂ surface for proton reduction reaction, owing to the absence of deep-trapped electrons, suppression of electron-hole recombination in Cd_0.8Zn_0.2S and high-efficiency charge separation at the Cd_0.8Zn_0.2S/Ti₃C₂ Schottky junction interface. Moreover, the hydrophilicity, electrical conductivity, visible-light absorption capacity, and surficial hydrogen desorption of Cd_0.8Zn_0.2S/Ti₃C₂ heterostructure are significantly improved. As a result, the heterostructure exhibits outstanding photocatalytic stability and super high apparent quantum efficiency, being rendered as one of the best noble-metal-free Cd-Zn-S-based photocatalysts. This work illustrates the mechanisms of morphology control and heterojunction construction in controlling the catalytic behavior of photocatalysts and highlights the great potential of the IL-assisted route in the synthesis of high-performance MXene-based heterostructures for photocatalytic hydrogen evolution.

Key words: Ionic liquid, Ultrathin Cd_0.8Zn_0.2S nanosheets, MXene, Schottky junction, Photoexcited charge separation, Photocatalytic H₂ evolution

Qianqian Hu, Haiyan Yin, Yifan Liu, Abdusalam Ablez, Zhuangzhuang Wang, Yue Zhan, Chengfeng Du, Xiaoying Huang. Tailoring the morphology and charge transfer pathways of ultrathin Cd_0.8Zn_0.2S nanosheets via ionic liquid-modified Ti₃C₂ MXenes towards remarkable photocatalytic hydrogen evolution[J]. J. Mater. Sci. Technol., 2025, 204: 47-59.

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Tailoring the morphology and charge transfer pathways of ultrathin Cd_0.8Zn_0.2S nanosheets via ionic liquid-modified Ti₃C₂ MXenes towards remarkable photocatalytic hydrogen evolution

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