Synergistic inhibition to dissolution corrosion by de-twinning and precipitation in alumina-forming austenitic steel exposed to lead-bismuth eutectic with 10-8 wt.% oxygen at 600 °C

doi:10.1016/j.jmst.2024.10.009

Abstract

Abstract: This work investigated the original microstructure of cold-worked alumina-forming austenitic steel, along with its precipitation and dissolution corrosion behaviors in lead-bismuth eutectic with 10^-8 wt.% oxygen at 600 °C, using solution-annealed steel for comparison. Anomalously, cold-worked steel presented milder corrosion compared to solution-annealed steel, with average corrosion depths of 314.3 and 401.0 µm after 1700 h exposure. Cold working-induced de-twinning transformed the annealing twin boundaries into normal high-angle grain boundaries (NGBs), increasing NGBs proportion from 36% to 89%. The increased NGBs provided more nucleation sites for intergranular barriers composed of alternate NiAl and M₂₃C₆ precipitates, thus better obstructing the dissolution attack.

Key words: Alumina-forming austenitic steel, Lead-bismuth eutectic, Dissolution corrosion, De-twinning, Precipitation

Decang Zhang, Xiaoxin Zhang, Jun Zhang, Hao Ren, Zhonghui Liao, Xian Zeng, Qingzhi Yan. Synergistic inhibition to dissolution corrosion by de-twinning and precipitation in alumina-forming austenitic steel exposed to lead-bismuth eutectic with 10^-8 wt.% oxygen at 600 °C[J]. J. Mater. Sci. Technol., 2025, 222: 55-67.

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Synergistic inhibition to dissolution corrosion by de-twinning and precipitation in alumina-forming austenitic steel exposed to lead-bismuth eutectic with 10^-8 wt.% oxygen at 600 °C

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