J. Mater. Sci. Technol. ›› 2022, Vol. 107: 82-91.DOI: 10.1016/j.jmst.2021.07.052
• Research Article • Previous Articles Next Articles
Y.J. Duana,b, L.T. Zhanga, T. Wadac, H. Katoc, E. Pined b, D. Crespob, J.M. Pelletierd, J.C. Qiaoa,*()
Received:
2021-05-25
Revised:
2021-05-25
Accepted:
2021-05-25
Published:
2022-04-30
Online:
2022-04-28
Contact:
J.C. Qiao
About author:
*E-mail address: qjczy@nwpu.edu.cn(J.C. Qiao).Y.J. Duan, L.T. Zhang, T. Wada, H. Kato, E. Pined, D. Crespo, J.M. Pelletier, J.C. Qiao. Analysis of the anelastic deformation of high-entropy Pd20Pt20Cu20Ni20P20 metallic glass under stress relaxation and recovery[J]. J. Mater. Sci. Technol., 2022, 107: 82-91.
Fig. 1. (a) XRD curve of the as-cast Pd20Pt20Cu20Ni20P20 HE-MG. (b) Normalized loss modulus E″/Eu of Pd20Pt20Cu20Ni20P20 HE-MG ribbon as a function of temperature. The heating rate is 5 K/min, and the driving frequency is 2 Hz. Eu denotes the value of the storage modulus at room temperature. (c) Stress-strain curves of Pd20Pt20Cu20Ni20P20 HE-MG as a function of temperature with a strain rate of 3×10-4s-1. (d) As a function of strain rate at 508 K.
Fig. 2. (a) Stress relaxation of Pd20Pt20Cu20Ni20P20 HE-MG containing 20 stress relaxation curves measured at stepping strain from 1% to 10%. Initial stress σonset and terminal stress σend trend lines. The inset graph is one enlarged typical stress relaxation curve measured at 1%. (b) The fitting parameters βKWW and τc of the phenomenological KWW fittings as a function of stepping strain, and the evolution of measured stress drop Δσ with strain.
Fig. 3. (a) Schematic illustration of the corresponding constitutive model. (b) Comparison of experimental (symbols) and corresponding constitutive model (black solid lines) for stress relaxation of Pd20Pt20Cu20Ni20P20 HE-MG at different step strains.
Fig. 5. The Schematic diagram of (a) stress and (b) strain response versus time during loading and unloading stages of the stress relaxation and recovery tests.
Fig. 6. (a) The anelastic strain εan/εan0 response of Pd20Pt20Cu20Ni20P20 HE-MG versus time for different initial strain level (0.4%, 0.6%…7%) during recovery tests at 508 K. εan0 is the strain at the beginning of the recovery experiments, i.e. after the instantaneous elastic drop. (b) The elastic strain εel/ε0, (c) anelastic strain εan/ε0 and (d) viscoplastic strain εvp/ε0 behavior of Pd20Pt20Cu20Ni20P20 HE-MG during recovery experiments as a function of the applied strain, ε0, during the loading stage.
Fig. 7. (a) The schematic diagram of the linear constitutive model: n anelastic processes act in series. (b) Recovery-time spectra of Pd20Pt20Cu20Ni20P20 HE-MG with different initial strain levels (0.4%, 0.6%…7%). The peaks of the time spectra are indicated by the arrows.
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