J. Mater. Sci. Technol. ›› 2026, Vol. 244: 80-87.DOI: 10.1016/j.jmst.2025.04.034

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Decoupling the orientation dependence of deformation-induced martensitic transformation via single-crystal micropillar compression

Guosheng Suna,b,*, Shilong Lva, Yunfei Zhanga, Lirong Xiaoa, Yong Penga, Yuntian Zhuc,d,*, Kehong Wanga,*, Jizi Liua,b,e,*   

  1. aSchool of Materials Science and Engineering, Nanjing University of Science and Technology, Nanjing 210094, China;
    bCenter of Analytical Facilities, Nanjing University of Science and Technology, Nanjing 210094, China;
    cDepartment of Materials Science and Engineering, Hong Kong Institute for Advanced Study, College of Science and Engineering, City University of Hong Kong, Kowloon 999077, Hong Kong, China;
    dMechanical Behavior Division of Shenyang National Laboratory for Materials Science, City University of Hong Kong, Kowloon 999077, Hong Kong, China;
    eNanjing Research Center for Biomedical Electron Microscopy (NRC-BEM), Nanjing Drum Tower Hospital, Medical School, Nanjing University, Nanjing 210093, China
  • Received:2024-11-28 Revised:2025-03-19 Accepted:2025-04-14 Published:2026-02-10 Online:2025-05-29
  • Contact: *E-mail addresses: gssun@njust.edu.cn (G. Sun), y.zhu@cityu.edu.hk(Y. Zhu), wkh1602@126.com (K. Wang), jzliu@njust.edu.cn (J. Liu)

Abstract: This study explores the significant orientation dependence of deformation-induced martensitic transformation. By employing single crystalline micropillar compression, three typical low-index crystallographic orientations were selected to examine their influence on the martensitic transformation of metastable austenitic stainless steel. Results demonstrate that the [011] orientation significantly inhibits the formation of α'-martensite, whereas the [001] and [111] orientations more effectively facilitate phase transformation, which is closely related to the transformation mechanisms. Specifically, the [001] orientation, which is prone to stacking fault formation, promotes martensitic transformation significantly with the aid of ε-martensite and the decreased effective stacking fault energy during compression. Meanwhile, the [111] oriented pillars demonstrate the highest yield strength, with shear deformation responsible for the relatively high fraction of α'-martensite. Additionally, the non-Schmid behavior occurred in the [011]- and [111]- oriented micropillars were found and discussed. This research advances the understanding of orientation-dependent martensitic transformation and provides an optional way to tailor the Transformation-induced plasticity effect via grain orientation engineering.

Key words: Micropillar compression, Austenitic steel, Metastable austenite, Martensitic transformation, Orientation