Metal-organic framework [NH2-MIL-53(Al)] functionalized TiO2 nanotube photoanodes for highly stable and efficient photoelectrochemical cathodic protection of nickel-coated Mg alloy

doi:10.1016/j.jmst.2023.09.038

Abstract

Abstract: Metal-organic framework [MOF, i.e., NH₂-MIL-53(Al)] modified TiO₂ (NMT) composite photoanodes were successfully prepared by hydrothermal synthesis and were used for the photoelectrochemical cathodic protection (PECCP) of nickel-plated magnesium alloy (Mg/Ni). Results showed that the synthesis temperature significantly impacted the morphology and PECCP performance of the NMT photoanodes. The NMT@150 photoanode prepared at a reaction temperature of 150 °C exhibited the best PECCP performance and produced a current density of 1980 μA cm^-2 under visible light irradiation, which was 19.8 times higher than that of a single TiO₂ photoanode. The composite photoanode could polarize the open circuit potential of the coupled Mg/Ni electrode to -876 mV and remain relatively stable within 35 h. XPS and EPR tests showed that a Z-scheme heterojunction was formed between the NH₂-MIL-53(Al) and TiO₂ nanotubes, allowing the photogenerated electrons to accumulate mainly on the conduction band of NH₂-MIL-53(Al). The heterojunction greatly promoted the separation and transfer of photogenerated electron-hole in the NMT composite photoanode, significantly enhancing the PECCP performance for Mg/Ni.

Key words: Magnesium alloy, Corrosion, Nickel coating, Electroless, Photoelectrochemical cathodic protection

Huan Yao, Ruifeng Zhang, Yu Wen, Yue Liu, Gang Yu, Zhi-Hui Xie. Metal-organic framework [NH₂-MIL-53(Al)] functionalized TiO₂ nanotube photoanodes for highly stable and efficient photoelectrochemical cathodic protection of nickel-coated Mg alloy[J]. J. Mater. Sci. Technol., 2024, 182: 67-78.

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Metal-organic framework [NH₂-MIL-53(Al)] functionalized TiO₂ nanotube photoanodes for highly stable and efficient photoelectrochemical cathodic protection of nickel-coated Mg alloy

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