Water vapor effects on the oxidation resistance of modified potassium silicate coating at high temperature

doi:10.1016/j.jmst.2023.08.026

J. Mater. Sci. Technol. ›› 2024, Vol. 176: 25-35.DOI: 10.1016/j.jmst.2023.08.026

• Research article • Previous Articles Next Articles

Water vapor effects on the oxidation resistance of modified potassium silicate coating at high temperature

Yao Du^a,b, Zheng Chen^a,b, Yiliang Lu^a,b,c, Cheng Wang^b,d,*, Lanlan Yang^e, Shenglong Zhu^b,f,g,*, Fuhui Wang^f,g

^aSchool of Materials Science and Engineering, University of Science and Technology of China, Shenyang, 110016, China;
^bShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, China;
^cState Key Laboratory of Advanced Power Transmission Technology, State Grid Smart Grid Research Institute Co., Ltd., Beijing, 102209, China;
^dJiangsu JITRI Road Engineering Technology and Equipment Research Institute Co., Ltd., Xuzhou, 220005, China;
^eSchool of Materials Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang, 212003, China;
^fShenyang National Laboratory for Materials Science, Shenyang, 110016, China;
^gSchool of Materials Science and Engineering, Northeastern University, Shenyang, 110819, China

Received:2023-07-08 Revised:2023-08-02 Accepted:2023-08-02 Published:2024-03-20 Online:2024-03-15
Contact: ^*E-mail addresses: wangcheng@imr.ac.cn (C. Wang), slzhu@imr.ac.cn (S. Zhu).

Abstract

Abstract: An inorganic potassium silicate coating with pigments of alumina, aluminum phosphate, NiCrAlY and copper chromite black was prepared on CB2 stainless steel. Oxidation behavior in either ambient air or O₂+H₂O mixture at 630 °C for 2000 h was comparatively studied, and the coating exhibited excellent resistance under both test conditions. The water vapor considerably accelerated the oxidation of the uncoated CB2 steel, as the hydroxide, the main constituent of the coating, had a negligible evaporation rate at test temperature, while it had a limited effect on the coated sample. Meanwhile, the existence of coating may prolong or eliminate the incubation period in the O₂+H₂O mixture at 630 °C. After oxidation, the coating matrix is in an amorphous state and fillers as alumina and copper chromite black are stable in the coating. Leucite (KAlSi₂O₆) formed by Al from NiCrAlY and potassium silicate in the coatings was detected after tests either in O₂ or O₂+H₂O mixture.

Key words: CB2 stainless steel, Inorganic silicate coating, TEM, High-temperature corrosion, Oxidation

Yao Du, Zheng Chen, Yiliang Lu, Cheng Wang, Lanlan Yang, Shenglong Zhu, Fuhui Wang. Water vapor effects on the oxidation resistance of modified potassium silicate coating at high temperature[J]. J. Mater. Sci. Technol., 2024, 176: 25-35.

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Water vapor effects on the oxidation resistance of modified potassium silicate coating at high temperature

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