J. Mater. Sci. Technol. ›› 2022, Vol. 112: 96-113.DOI: 10.1016/j.jmst.2021.09.049

• Research Article • Previous Articles     Next Articles

Effect of a weak magnetic field on ductile-brittle transition in micro-cutting of single-crystal calcium fluoride

Yunfa Guoa, Yan Jin Leea, Yu Zhanga, Anastassia Sorkina, Sergei Manzhosb,*(), Hao Wanga,*()   

  1. aDepartment of Mechanical Engineering, National University of Singapore, 9 Engineering Drive 1, Singapore 117575, Singapore
    bSchool of Materials and Chemical Technology, Tokyo Institute of Technology, Ookayama 2-12-1, Meguro-ku, Tokyo 152-8552, Japan
  • Received:2021-07-13 Revised:2021-08-25 Accepted:2021-09-23 Published:2021-12-12 Online:2021-12-12
  • Contact: Sergei Manzhos,Hao Wang
  • About author:mpewhao@nus.edu.sg (H. Wang).
    * E-mail addresses: manzhos.s.aa@m.titech.ac.jp (S. Manzhos),

Abstract:

Magneto-plasticity occurs when a weak magnetic field alters material plasticity and offers a viable solution to enhance ductile-mode cutting of brittle materials. This study demonstrates the susceptibility of non-magnetic single-crystal calcium fluoride (CaF2) to the magneto-plastic effect. The influence of magneto-plasticity on CaF2 was confirmed in micro-deformation tests under a weak magnetic field of 20 mT. The surface pile-up effect was weakened by 10–15 nm along with an enlarged plastic zone and suppressed crack propagation under the influence of the magnetic field. Micro-cutting tests along different crystal orientations on the (111) plane of CaF2 revealed an increase in the ductile–brittle transition of the machined surface with the aid of magneto-plasticity where the largest increase in ductile–brittle transition occurred along the $\left[ 11\bar{2} \right]$ orientation from 512 nm to a range of 664–806 nm. Meanwhile, the subsurface damage layer was concurrently thinner under magnetic influence. An anisotropic influence of the magnetic field relative to the single-crystal orientation and the cutting direction was also observed. An analytical model was derived to determine an orientation factor M that successfully describes the anisotropy while considering the single-crystal dislocation behaviour, material fracture toughness, and the orientation of the magnetic field. Previously suggested theoretical mechanism of magneto-plasticity via formation of non-singlet electronic states in defected configurations was confirmed with density functional theory calculations. The successful findings on the influence of a weak magnetic field on plasticity present an opportunity for the adoption of magnetic-assisted micro-cutting of non-magnetic materials.

Key words: Magneto-plasticity, Weak magnetic field, Brittle material, Ductile-brittle transition, Micro-cutting