J. Mater. Sci. Technol. ›› 2020, Vol. 45: 176-186.DOI: 10.1016/j.jmst.2019.11.020
• Research Article • Previous Articles Next Articles
Lu Zhanga, Yuanyuan Cuib, Fengli Yanga, Quan Zhanga, Juhua Zhanga, Mengting Caoa, Wei-Lin Daia,*()
Received:
2019-08-07
Revised:
2019-10-04
Accepted:
2019-11-16
Published:
2020-05-15
Online:
2020-05-27
Contact:
Wei-Lin Dai
Lu Zhang, Yuanyuan Cui, Fengli Yang, Quan Zhang, Juhua Zhang, Mengting Cao, Wei-Lin Dai. Electroless-hydrothermal construction of nickel bridged nickel sulfide@mesoporous carbon nitride hybrids for highly efficient noble metal-free photocatalytic H2 production[J]. J. Mater. Sci. Technol., 2020, 45: 176-186.
Fig. 1. (a) The effects of hydrothermal treatment temperature during loading NiS (10 wt.%) with duration fixed at 6 h on the H2 evolution performance and the yields of catalysts; (b) XRD patterns of the samples obtained under different hydrothermal temperature. (Sample yield refers to the percentage of NiS/m-CN product obtained versus the theoretical amounts).
Fig. 2. (a) The effects of hydrothermal treatment duration during loading NiS (10 wt.%) with temperature fixed at 160 °C on the H2 evolution performance and the yields of catalysts; (b) XRD patterns of the samples obtained under different hydrothermal duration.
Etching time /s | 0 | 60 | 120 | 180 | 240 | 300 | 360 | |
---|---|---|---|---|---|---|---|---|
Ni 2p | B.E/eV | -- | 853.1 | 853.2 | 853.1 | 853.0 | 853.0 | 853.0 |
Atom content/% (A) | 0 | 0.10 | 0.14 | 0.19 | 0.32 | 0.27 | 0.31 | |
S 2p | B.E/eV | 162.2 | 162.2 | 162.1 | 162.2 | 162.0 | 162.0 | 162.1 |
Atom content/% (B) | 0.09 | 0.14 | 0.15 | 0.19 | 0.16 | 0.19 | 0.21 | |
A/B | 0 | 0.71 | 0.93 | 1.00 | 2.00 | 1.42 | 1.48 |
Table 1 The relative atomic concentration (%) of Ni and S elements in the form of NiS with different sputtering time and their corresponding ratio.
Etching time /s | 0 | 60 | 120 | 180 | 240 | 300 | 360 | |
---|---|---|---|---|---|---|---|---|
Ni 2p | B.E/eV | -- | 853.1 | 853.2 | 853.1 | 853.0 | 853.0 | 853.0 |
Atom content/% (A) | 0 | 0.10 | 0.14 | 0.19 | 0.32 | 0.27 | 0.31 | |
S 2p | B.E/eV | 162.2 | 162.2 | 162.1 | 162.2 | 162.0 | 162.0 | 162.1 |
Atom content/% (B) | 0.09 | 0.14 | 0.15 | 0.19 | 0.16 | 0.19 | 0.21 | |
A/B | 0 | 0.71 | 0.93 | 1.00 | 2.00 | 1.42 | 1.48 |
Fig. 7. (a) UV-vis DRS and (d) PL spectra of NiS/m-CN (A: m-CN, B: 5% NiS/m-CN, C: 7.5% NiS/m-CN, D: 10% NiS/m-CN, E: 12.5% NiS/m-CN, F: NiS, G: 10% NiS/m-CN-D); (b) XPS valence band spectra and (c) Schematic illustration of the band positions for m-CN (g-C3N4) and 10% NiS/m-CN-160-12 (NiS/Ni/g-C3N4).
Samples | Absorption edge (nm) | Band gap energy (eV) |
---|---|---|
m-CN | 461 | 2.69 |
5% NiS/m-CN | 451 | 2.75 |
7.5% NiS/m-CN | 444 | 2.79 |
10% NiS/m-CN | 453 | 2.74 |
12.5% NiS/m-CN | 457 | 2.71 |
Table 2 Absorption edges and band gap energies of NiS/m-CN samples with different NiS loading quantity.
Samples | Absorption edge (nm) | Band gap energy (eV) |
---|---|---|
m-CN | 461 | 2.69 |
5% NiS/m-CN | 451 | 2.75 |
7.5% NiS/m-CN | 444 | 2.79 |
10% NiS/m-CN | 453 | 2.74 |
12.5% NiS/m-CN | 457 | 2.71 |
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