J. Mater. Sci. Technol. ›› 2026, Vol. 270: 68-85.DOI: 10.1016/j.jmst.2026.01.016

• Research Article • Previous Articles     Next Articles

Strain-induced microstructural and precipitation behavior of Al-Mg-Si-Mn alloys: Effects of Si content under controlled thermomechanical conditions

Oleksandr Lypchanskyia,b,*, Nikolaos Rigasc, Łukasz Rogald, Karol Januse, Lidia Litynska-Dobrzynskad, Grzegorz Korpałaf, Thomas Lampkea, Marion Merkleinc, Ulrich Prahlf   

  1. aInstitute of Materials Science and Engineering, Chemnitz University of Technology, 09107 Chemnitz, Germany;
    bFaculty of Metals Engineering and Industrial Computer Science, AGH University of Krakow, 30-059 Krakow, Poland;
    cInstitute of Manufacturing Technology, Friedrich-Alexander-Universität Erlangen-Nürnberg, 91058 Erlangen, Germany;
    dInstitute of Metallurgy and Materials Science, Polish Academy of Sciences, 30-059 Krakow, Poland;
    eFaculty of Foundry Engineering, AGH University of Krakow, 30-059 Krakow, Poland;
    fInstitute of Metal Forming, TU Bergakademie Freiberg, 09599 Freiberg, Germany
  • Received:2025-08-30 Revised:2026-01-13 Accepted:2026-01-15 Published:2026-11-01 Online:2026-01-19
  • Contact: * E-mail address: oleksandr.lypchanskyi.imf@gmail.com (O. Lypchanskyi).

Abstract: This study investigates the microstructural evolution of Al-Mg-Si-Mn alloys, focusing on the influence of Si content on mechanical properties, deformation mechanisms, and precipitate evolution during high-temperature tensile testing. Tensile tests were performed at 200, 250, 300, and 350 °C with strain rates of 0.1, 1, and 10 %/s, showing significant variations in mechanical response as a function of Si content. Microstructural characterization was performed using electron backscatter diffraction, energy-dispersive X-ray spectrometry, and a transmission electron microscope to analyze deformation mechanisms, precipitate evolution, and texture formation. The results show a progressive decrease in tensile strength and yield strength with increasing deformation temperature, with the most pronounced reduction occurring at 350 °C in alloys with higher Si content. This increased Si level promotes the strengthening of the Copper texture while progressively suppressing the Cube texture during deformation at elevated temperatures. At 200 °C, deformation bands are formed primarily by interaction with dislocations, while precipitates drive deformation band formation by effectively impeding dislocation motion. Resolved shear stress analysis indicates a direct influence on the initiation and progression of discontinuous dynamic recrystallization (DDRX), with higher Si levels promoting more pronounced DDRX. Deformation at elevated temperatures of 300 and 350 °C enhances dynamic recrystallization and accelerates continuous dynamic recrystallization, leading to increased grain boundary formation and a reduction in deformation band density. Furthermore, the evolution of β′ , B′ , and U1 phases at 300 °C and 0.1 %/s strain rate highlights the heterogeneous nucleation and growth mechanisms of precipitates. These results underscore the critical role of Si content in controlling the mechanical response and microstructural evolution of Al-Mg-Si-Mn alloys, providing valuable insights for optimizing alloy design and performance at elevated temperatures.

Key words: Recrystallization, Precipitates, Deformation mechanisms, Al-Mg-Si-Mn alloys