J. Mater. Sci. Technol. ›› 2025, Vol. 234: 71-81.DOI: 10.1016/j.jmst.2025.01.049

• Research Article • Previous Articles     Next Articles

Effect of stress-induced martensites and reverse-induced dislocations on β phase precipitation behavior in a metastable β-Ti alloy

Luyao Tanga, Puyi Gaoa,*, Jiangkun Fana,b,c,*, Wenyuan Zhanga, Ding Zhaoa, Yinfan Maa, Panpan Fana, Zhixin Zhangb, Jinshan Lia,b,c   

  1. aState Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072, China;
    bChongqing Innovation Center, Northwestern Polytechnical University, Chongqing 401135, China;
    cNational & Local Joint Engineering Research Center for Precision Thermoforming Technology of Advanced Metal Materials, Xi’an 710072, China
  • Received:2024-10-28 Revised:2025-01-01 Accepted:2025-01-09 Published:2025-11-01 Online:2025-03-21
  • Contact: *E-mail addresses: 981404099@qq.com (P. Gao), jkfan@nwpu.edu.cn (J. Fan).

Abstract: Achieving precise control over β phase precipitation is crucial for obtaining ultra-high strength in metastable β-Ti alloys. However, a comprehensive understanding of how deformation products and their reversion counterparts influence β phase precipitation behavior in these exceptional alloys remains elusive. This study explores the influence of stress-induced martensite (SIM) and its reversion-induced dislocations on the β phase precipitation behavior in a metastable β-Ti alloy. After loading and reloading, SIM laths formed, and some SIM laths subsequently reversed into the β phase, introducing band-like regions with dense and parallel arranged <110> dislocations in the β phase matrix. Such dislocations resulted in a band-like area decorated with short rod-like β phase precipitates during isothermal annealing. Meanwhile, the remaining stress-induced martensite decomposed directly into β phase, forming a long β phase with a morphology similar to the original martensite. Additionally, both sides of the original SIM laths reversed during isothermal annealing, forming {332}<113>β twins at the β/β phase interface. This divided the β phase formed in SIM laths from the β phase formed directly in the β matrix.

Key words: Titanium alloy, Stress-induced martensite, Martensite reversion, Isothermal annealing, β phase precipitation;